The concentration of the pesticide Imazalil should be determined in an apple sample. Outline how you will proceed to analyze Imazalil in the apple sample: Extraction and purification, concentration and analysis (chromatographic technique, column, detector, mobile phase, etc.). Imazalil is a thermally stable substance with a melting point of 50 ° C. The compound is sparingly water soluble (1.4 g/ L) with LogP = 3.8. The compound is further weakly basic with a pka value equal to 6.5 The structure of Imazalil (C14H14CI2N2O). The compound is weakly basic, pKa (NH +) = 6.5.

The concentration of the pesticide Imazalil should be determined in an apple sample. Outline how you will proceed to analyze Imazalil in the apple sample: Extraction and purification, concentration and analysis (chromatographic technique, column, detector, mobile phase, etc.). Imazalil is a thermally stable substance with a melting point of 50 ° C. The compound is sparingly water soluble (1.4 g/ L) with LogP = 3.8. The compound is further weakly basic with a pka value equal to 6.5 The structure of Imazalil (C14H14CI2N2O). The compound is weakly basic, pKa (NH +) = 6.5.

Chemistry

10th Edition

ISBN:9781305957404

Author:Steven S. Zumdahl, Susan A. Zumdahl, Donald J. DeCoste

Publisher:Steven S. Zumdahl, Susan A. Zumdahl, Donald J. DeCoste

Chapter1: Chemical Foundations

Section: Chapter Questions

Problem 1RQ: Define and explain the differences between the following terms. a. law and theory b. theory and...

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A piece of Gold weighing 12,359 Kg is suspected of being contaminated with Iron. To perform an instrumental analysis and To confirm whether or not it contains Fe, a portion of the sample (0.954 g) is taken from the piece and dissolved with 25 mL of aqua regia. Heats up For its complete dissolution, it is cooled and made up to 100 mL. A 10 mL aliquot is taken from this solution and made up to 50 mL. From This last solution is given the appropriate treatment to visualize Fe+2, for which the 1,10-phenanthroline reagent is added. (it forms a complex that is red in color) and is taken to a visible spectrophotometer and with a 12 mm cell a absorbance of 0.45. Previously, a calibration curve of Fe+2 was obtained under the same instrumental conditions obtaining the following data: (view table) Calculate the purity of the gold piece, assuming impurities only due to Fe.
Consider Table 1, which lists the volumes of the Fe3+ and SCN- solutions used for the continuous variation method. Note that each of the stock solutions is 0.002 M before mixing. What are the initial concentrations of Fe3+ and SCN- for solution 4, where the volumes are both 5 mL? [Initial meaning after they are mixed, but before]they reach equilibrium)
ASAP: Please help me solve for Average Molarity of EDTA Standard Solution and Ca Titer (mg Ca/mL of EDTA Solution). Show step by step solution. This is the data. Please explain thoroughly as well.
A 100 ml bottle of metronidazole 100 mg/ml suspension is available in your pharmacy. Calculate the volume of this suspension needed to be diluted with cherry syrup to prepare 60 ml of a 4% metronidazole suspension. 1 ml of a 1:1000 epinephrine injection was mixed with 20 ml of 1% lidocaine injection. Calculate the new ratio strength of epinephrine in the admixture. (IGNORE ANY VOLUME CHANGES AFTER ADMIXTURE) Instead of preparing 4 grams of tetracaine hydrochloride 4% gel an 8% gel was compounded by mistake. How many grams of the 8% gel and gel base must be mixed to get 4 grams of a 4% gel? How many milliliters of 70% ethanol and 20% ethanol must be mixed to prepare 500 ml of 30% ethanol? A diphenhydramine elixir contains 12.5 mg drug in one teaspoon. The volume of oral vehicle that is to be added to 100 ml of this elixir to reduce its strength by one half its original strength is; 6. 90 capsules of Liothyronine (T3) 15 micrograms are to be prepared. The formula calls for a 1:10000…
250.0 ml of the mineral water sample was precipitated with potassium sodium tetraphenyl bromate: K+ + B(C6H5)4-  KB(C6H5)(s). The precipitate was filtered, washed and dissolved in an organic solvent. An excess of HgY2- was added to the solution: 4 HgY2- + B(C6H5)4- +4H2O  H3BO3 + 4C6H5Hg+ + 4HY3- + OH-. The liberated EDTA was titrated with 0.05581 M Mg 2+ solution, which consumed 29.64 mL. Calculate the potassium concentration [mg/l] in the sample.
PRESTUDY 3. Using the physical properties you entered in the table and the outlined experimental procedure, complete the flow chart. In the oval spaces, name the reagents and/or conditions necessary to affect each indicated separation step. In the rectangular boxes, write the names of the separated components. Mixture of NaCl, SiO₂, Fe ces SiO₂2 and NaCl magnet Aironeme EREO2 PPps 0-281 Fe Taxo ==puritas = $ PRES PRC.E 08-0-41
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Transfer 3-4 drops or a pinch of the test compound (Acetanilide) to 3 ml of the solvents, 5% NaOH and 5% HCL Shake the mixture thoroughly. The time required for the solute to dissolve in the solvent should not be more than 2 minutes. Indicate with (+) or (-) if the test compound is soluble or insoluble in the solvent. Is Acetanilide solube or insolube in 5% NaOH? _______ Is Acetanilde soluble or insolube in 5% HCL? _______
A solution contains 0.10 M Sr(NO3)₂ and 0.20 M Bi(NO₂). When solid Na AsO is added to the solution a precipitate forms. What concentration of AsO ³ maintains maximum separation of Sr²+ and Bi³+? Ksp of Sr₂(AsO₂)₂ = 4.29 x 10-1⁹ and BIASO = 4.43 x 10-1⁰ 4 4/2
MAKE A METHODOLOGY : MATERIALS/ REAGENTS WITH SCHEMATIC DIAGRAM . THE PICTURE UPLOADED SERVES AS A GUIDE, DO THE SAME THING BASED FROM THE PIC. Procedure: Place 20 drops of each of 0.2M CuSO4 in a centrifuge tube. Then add 5 drops of freshly prepared 6M (NH4)2S to each centrifuge tube. Record your observation. Centrifuge the mixtures for 3 mins. and decant the supernatant liquid. Add 10 drops of DI water and 10 drops of 6M HNO3. Stir and boil the mixture in a hot water bath for 5 mins. centrifuge the mixture for 3 mins. Decant the supernatant solution from procedure 3. Discard the To each of the supernatant liquid, add 6 drops of 6M H2SO4. Allow themixtures to cool and 5 drops of DI water. To the mixtures in procedure 4, add few drops of concentrated NH3 until the solution becomes basic. Confirm using a litmus paper. Record your observation. Add 1 drop of 5M NaOH and 1 drop of 0.1 M SnCl2 to the centrifuge tube containing Bi3+ ion , centrifuge and decant the supernatant liquid. To…