QUESTION: Provide a reasonable curved-arrow mechanism for the conversion of your starting material into product. Aldol Condensation Reaction of an Unknown C15H13CIO2 Procedure: Protocol for Synthesizing Unknown WHIM Identify the correct starting material for this reaction. FYI the acetophenone is incorporated into the product. In a 150 x 18 mm test tube containing a stir bar, dissolve 2 mmoles of benzaldehyde and 2 mmoles of acetophenone in 1 ml of 95% ethanol. Add 5 drops of 10% sodium hydroxide solution, stir the mixture until it becomes homogeneous and then let it stir at room temperature for another 20 min. Cool the mixture in an ice bath, collect the crystals in a Hirsch funnel and wash the crystals with a little ice-cold 95% ethanol. Recrystallize the solid from 95% ethanol. Dry the resulting crystals by pressing them between filter paper and by spreading them out on a watch glass. H -CH3 Proposed Structure of Starting Material: C-CH2-CH- -CI OH Proposed Structure of Product:

Chemistry
10th Edition
ISBN:9781305957404
Author:Steven S. Zumdahl, Susan A. Zumdahl, Donald J. DeCoste
Publisher:Steven S. Zumdahl, Susan A. Zumdahl, Donald J. DeCoste
Chapter1: Chemical Foundations
Section: Chapter Questions
Problem 1RQ: Define and explain the differences between the following terms. a. law and theory b. theory and...
icon
Related questions
Question
QUESTION: Provide a reasonable curved-arrow mechanism for the conversion of your starting material into product.
Aldol Condensation Reaction of an Unknown C15H13CIO2
Procedure: Protocol for Synthesizing Unknown WHIM
Identify the correct starting material for this reaction. FYI the acetophenone is incorporated into the product.
In a 150 x 18 mm test tube containing a stir bar, dissolve 2 mmoles of benzaldehyde and 2 mmoles of acetophenone in 1 ml
of 95% ethanol. Add 5 drops of 10% sodium hydroxide solution, stir the mixture until it becomes homogeneous and then let
it stir at room temperature for another 20 min.
Cool the mixture in an ice bath, collect the crystals in a Hirsch funnel and wash the crystals with a little ice-cold 95% ethanol.
Recrystallize the solid from 95% ethanol. Dry the resulting crystals by pressing them between filter paper and by spreading
them out on a watch glass.
H
-C-CH3
Proposed Structure of Starting Material:
Opang
-CH,-CH
-CI
Proposed Structure of Product:
Transcribed Image Text:QUESTION: Provide a reasonable curved-arrow mechanism for the conversion of your starting material into product. Aldol Condensation Reaction of an Unknown C15H13CIO2 Procedure: Protocol for Synthesizing Unknown WHIM Identify the correct starting material for this reaction. FYI the acetophenone is incorporated into the product. In a 150 x 18 mm test tube containing a stir bar, dissolve 2 mmoles of benzaldehyde and 2 mmoles of acetophenone in 1 ml of 95% ethanol. Add 5 drops of 10% sodium hydroxide solution, stir the mixture until it becomes homogeneous and then let it stir at room temperature for another 20 min. Cool the mixture in an ice bath, collect the crystals in a Hirsch funnel and wash the crystals with a little ice-cold 95% ethanol. Recrystallize the solid from 95% ethanol. Dry the resulting crystals by pressing them between filter paper and by spreading them out on a watch glass. H -C-CH3 Proposed Structure of Starting Material: Opang -CH,-CH -CI Proposed Structure of Product:
Expert Solution
steps

Step by step

Solved in 2 steps with 2 images

Blurred answer
Knowledge Booster
Alkynes
Learn more about
Need a deep-dive on the concept behind this application? Look no further. Learn more about this topic, chemistry and related others by exploring similar questions and additional content below.
Recommended textbooks for you
Chemistry
Chemistry
Chemistry
ISBN:
9781305957404
Author:
Steven S. Zumdahl, Susan A. Zumdahl, Donald J. DeCoste
Publisher:
Cengage Learning
Chemistry
Chemistry
Chemistry
ISBN:
9781259911156
Author:
Raymond Chang Dr., Jason Overby Professor
Publisher:
McGraw-Hill Education
Principles of Instrumental Analysis
Principles of Instrumental Analysis
Chemistry
ISBN:
9781305577213
Author:
Douglas A. Skoog, F. James Holler, Stanley R. Crouch
Publisher:
Cengage Learning
Organic Chemistry
Organic Chemistry
Chemistry
ISBN:
9780078021558
Author:
Janice Gorzynski Smith Dr.
Publisher:
McGraw-Hill Education
Chemistry: Principles and Reactions
Chemistry: Principles and Reactions
Chemistry
ISBN:
9781305079373
Author:
William L. Masterton, Cecile N. Hurley
Publisher:
Cengage Learning
Elementary Principles of Chemical Processes, Bind…
Elementary Principles of Chemical Processes, Bind…
Chemistry
ISBN:
9781118431221
Author:
Richard M. Felder, Ronald W. Rousseau, Lisa G. Bullard
Publisher:
WILEY