ompounds 2,4 Dinitrophenylhydrazones Mix 2.5 mL of 2,4-dinitrophenylhydrazine in phosphoric acid and 25 mg of the unknown. Warm in a water bath for 5 min and let crystallization proceed. Collect the product by suction filtration and wash the crystals with cold water. Recrystallize from ethanol and let it dry until next time. NHÁNH, N-NH- -NO₂ R☑ R✗ R' NO₂ R' O₂N
ompounds 2,4 Dinitrophenylhydrazones Mix 2.5 mL of 2,4-dinitrophenylhydrazine in phosphoric acid and 25 mg of the unknown. Warm in a water bath for 5 min and let crystallization proceed. Collect the product by suction filtration and wash the crystals with cold water. Recrystallize from ethanol and let it dry until next time. NHÁNH, N-NH- -NO₂ R☑ R✗ R' NO₂ R' O₂N
Chapter12: Isopentyl Acetate (banana Oil)
Section: Chapter Questions
Problem 2Q
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Question
Please provide a mechanism for 2,4 dinitrophenylhydrazones reaction. The unknown is 3-pentanone. Please provide a mechanism for the reagents being added 3-pentanone.

Transcribed Image Text:ompounds
2,4 Dinitrophenylhydrazones
Mix 2.5 mL of 2,4-dinitrophenylhydrazine in phosphoric
acid and 25 mg of the unknown. Warm in a water bath for 5
min and let crystallization proceed. Collect the product by
suction filtration and wash the crystals with cold water.
Recrystallize from ethanol and let it dry until next time.
NHÁNH,
N-NH-
-NO₂
R☑
R✗
R'
NO₂
R' O₂N
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