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Suggest possible crystallization solvents for the following compounds. Use IMF to predict the type of solvent each compound should be soluble in. Then, find the melting point and solubility of compounds in the handbook, and choose s recrystallization solvent

Suggest possible crystallization solvents for the following compounds. Use IMF to predict the type of solvent each compound should be soluble in. Then, find the melting point and solubility of compounds in the handbook, and choose s recrystallization solvent

Chemistry
Chemistry
10th Edition
ISBN:9781305957404
Author:Steven S. Zumdahl, Susan A. Zumdahl, Donald J. DeCoste
Publisher:Steven S. Zumdahl, Susan A. Zumdahl, Donald J. DeCoste
Chapter1: Chemical Foundations
Section: Chapter Questions
Problem 1RQ: Define and explain the differences between the following terms. a. law and theory b. theory and...
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Suggest possible crystallization solvents for the following compounds. Use IMF to predict the type of solvent each compound should be soluble in. Then, find the melting point and solubility of compounds in the handbook, and choose s recrystallization solvent
naphthale ne 0 4-phenylcyclohexanone 18. 2-inda nol H₂CO₂C phenylacetic acid H CO₂H *$HOOO dimethylfumarate
Transcribed Image Text:naphthale ne 0 4-phenylcyclohexanone 18. 2-inda nol H₂CO₂C phenylacetic acid H CO₂H *$HOOO dimethylfumarate
Solvent 6 Petroleum ether Pentane Hexane Heptane Ligroin Heptane Octane Nonane Cyclohexane 1,4-Dioxane Tolnene Diethyl ether Chloroform Ethyl acetate Tetrahydrofuran Dichloromethane Acetone Ethanol (95%) Methanol Water CH3CH₂CH₂CH₂CH₂ pentane CHỊCH,-O-CH;CH diethyl ether CH₂ CH₂ acetone F7 Y Table 1. Common solvents, Dielectric Boiling Point Freezing Point Constant (8) °C (760 Torr) & 7 1.9 1.84 1.89 FB 1.9 1.9 E 1.9 1.9 1.965 2.21 2.38 4.34 4.81 6.02 7.60 9.08 8 20.7 24,6 32.6 78.5 CH₂-C ********** **38 30-80 * 8 80-120 Ở–CH,CH, ethyl acetate CH₂CH₂-OH ethanol 366 JOUL H|J "C 885 55 85 233 553- -130 F10 ( 9 95 -91 91 -57 -SI 6.6 118 95 CH₂CH₂CH₂CH₂CH₂CH₂CH₂CH₂ octane -116 -63-5 -84 -109 295 -95 -11 94 10 Density g/mL. 0.63 0.66 F11 T-PAD 0.68 18 19 ) 0.68 0 -0.70 0.72 0.78 1.03 0.87 ALIENWARE 0.71 1.48 0.90 0.89 1.33 0.79 0,79 0.79 8-8-8 1.00 CH₂-OH methanol Water Soluble 22222222 222 2222 9098 No No No No No No Yes No Slightly Yes Yes Yes na Página < F12 ALIENT Flammable K L : || Yes Yes Yes الشالشال Yes Yes Yes Yes Yes Ves cyclohexane 1,4-dioxane toluene Yes Yes CH₂Cl₂ CHCI tetrahydrocuran dichloromethane chloroform Yes No Yes Yes No Yes Yes Yes No H₂O water 9 HOME { CH₂ + = 3
Transcribed Image Text:Solvent 6 Petroleum ether Pentane Hexane Heptane Ligroin Heptane Octane Nonane Cyclohexane 1,4-Dioxane Tolnene Diethyl ether Chloroform Ethyl acetate Tetrahydrofuran Dichloromethane Acetone Ethanol (95%) Methanol Water CH3CH₂CH₂CH₂CH₂ pentane CHỊCH,-O-CH;CH diethyl ether CH₂ CH₂ acetone F7 Y Table 1. Common solvents, Dielectric Boiling Point Freezing Point Constant (8) °C (760 Torr) & 7 1.9 1.84 1.89 FB 1.9 1.9 E 1.9 1.9 1.965 2.21 2.38 4.34 4.81 6.02 7.60 9.08 8 20.7 24,6 32.6 78.5 CH₂-C ********** **38 30-80 * 8 80-120 Ở–CH,CH, ethyl acetate CH₂CH₂-OH ethanol 366 JOUL H|J "C 885 55 85 233 553- -130 F10 ( 9 95 -91 91 -57 -SI 6.6 118 95 CH₂CH₂CH₂CH₂CH₂CH₂CH₂CH₂ octane -116 -63-5 -84 -109 295 -95 -11 94 10 Density g/mL. 0.63 0.66 F11 T-PAD 0.68 18 19 ) 0.68 0 -0.70 0.72 0.78 1.03 0.87 ALIENWARE 0.71 1.48 0.90 0.89 1.33 0.79 0,79 0.79 8-8-8 1.00 CH₂-OH methanol Water Soluble 22222222 222 2222 9098 No No No No No No Yes No Slightly Yes Yes Yes na Página < F12 ALIENT Flammable K L : || Yes Yes Yes الشالشال Yes Yes Yes Yes Yes Ves cyclohexane 1,4-dioxane toluene Yes Yes CH₂Cl₂ CHCI tetrahydrocuran dichloromethane chloroform Yes No Yes Yes No Yes Yes Yes No H₂O water 9 HOME { CH₂ + = 3
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