Decide what H and C atoms in your final product should fit the reported chemical shifts and answer any additional questions. The literature data are for the free base fluoxetine product not the oxalate product. 1HNMR (60 MHz, CDCI3) d 1.9-2.2 (10H, m), 5.2 (1H, t), 6.8-7.4 (9H, m). 1°C NMR (91 MHz, CDCI3) d 160.5, 141.0, 128.6, 127.6, 126.5, 125.7, 122.8, 124.3 (q. J = 267 Hz), 122.5 (q. J = 30 Hz), 115.7, 78.5, 55.7, 45.5, 36.8. %3D 1. For the 13C spectrum: notice the signals at 124.3 and 122.5 are split into quartets. This is unusual for the 13C NMR of many organic compounds. Why is this observed in the spectrum for fluoxetine.
Analyzing Infrared Spectra
The electromagnetic radiation or frequency is classified into radio-waves, micro-waves, infrared, visible, ultraviolet, X-rays and gamma rays. The infrared spectra emission refers to the portion between the visible and the microwave areas of electromagnetic spectrum. This spectral area is usually divided into three parts, near infrared (14,290 – 4000 cm-1), mid infrared (4000 – 400 cm-1), and far infrared (700 – 200 cm-1), respectively. The number set is the number of the wave (cm-1).
IR Spectrum Of Cyclohexanone
It is the analysis of the structure of cyclohexaone using IR data interpretation.
IR Spectrum Of Anisole
Interpretation of anisole using IR spectrum obtained from IR analysis.
IR Spectroscopy
Infrared (IR) or vibrational spectroscopy is a method used for analyzing the particle's vibratory transformations. This is one of the very popular spectroscopic approaches employed by inorganic as well as organic laboratories because it is helpful in evaluating and distinguishing the frameworks of the molecules. The infra-red spectroscopy process or procedure is carried out using a tool called an infrared spectrometer to obtain an infrared spectral (or spectrophotometer).
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