8. In real life, NMR samples often contain impurities, so extra signals will appear on yourspectrum that are not related to your product. The document "Common NMR impurities"lists some common impurities and their NMR data. Here are some instructions for readingthis document:o Use Table 1 on page 2 of the document, focusing on the column for CDCI3. (Thisis the NMR solvent we are using.)o The impurities are listed in the first column.o The "mult" column tells you the multiplicities those signals should have.• s = singlet, d = doublet, t = triplet, q = quartet, etc.o The numbers in the table are the chemical shifts that certain impurities appear at.o For example, if diethyl ether is present in your sample, you should see two signals:a triplet at 1.21 ppm and a quartet at 3.48 ppm. Complete this table for some of the possible impurities that could appear in NMR spectrumexperiment.Chemical shifts (ppm) and multiplicitiesof impurity peaksIdentity of impurity1.56, singletacetone3.21, singlet; 1.19 singlet2.45, quartet; 2.14, singlet; 1.06, tripletNote: tert-butyl methyl ether and butanone are two solvents we will use in this experiment that arenot included in the "Common NMR impurities" document. The spectrum of each is shown below.Determine which 'H NMR spectrum is of tert-butyl methyl ether and which is of butanone, then fillin the last two rows in the table above.11106.4107543ppmppmHOP-3-535HP-00-105

Structure of butanone- It contains 3 types of protons. Structure of tert-butyl methyl ether.…

Complete this table for some of the possible impurities that could appear in NMR spectrum experiment. Chemical shifts (ppm) and multiplicities of impurity peaks Identity of impurity 1.56, singlet acetone 3.21, singlet; 1.19 singlet 2.45, quartet; 2.14, singlet; 1.06, triplet Note: tert-butyl methyl ether and butanone are two solvents we will use in this experiment that are not included in the "Common NMR impurities" document. The spectrum of each is shown below. Determine which 'H NMR spectrum is of tert-butyl methyl ether and which is of butanone, then fill in the last two rows in the table above. 11 10 5. pom Ppm

Complete this table for some of the possible impurities that could appear in NMR spectrum experiment. Chemical shifts (ppm) and multiplicities of impurity peaks Identity of impurity 1.56, singlet acetone 3.21, singlet; 1.19 singlet 2.45, quartet; 2.14, singlet; 1.06, triplet Note: tert-butyl methyl ether and butanone are two solvents we will use in this experiment that are not included in the "Common NMR impurities" document. The spectrum of each is shown below. Determine which 'H NMR spectrum is of tert-butyl methyl ether and which is of butanone, then fill in the last two rows in the table above. 11 10 5. pom Ppm

Chemistry

10th Edition

ISBN:9781305957404

Author:Steven S. Zumdahl, Susan A. Zumdahl, Donald J. DeCoste

Publisher:Steven S. Zumdahl, Susan A. Zumdahl, Donald J. DeCoste

Chapter1: Chemical Foundations

Section: Chapter Questions

Problem 1RQ: Define and explain the differences between the following terms. a. law and theory b. theory and...

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