3372 IR Spectrum (liquid film) 4000 3000 2000 1600 1200 800 V (cm) 100 80 60 40 20 % of base peak 106 148 Mass Spectrum M 149 C10H15N 40 80 120 160 200 240 280 m/e 13C NMR Spectrum (100 MHz, CDCl, solution) DEPT CH2CH3CH proton decoupled expansion 130 125 expansion 130 125 solvent 200 160 120 80 1H NMR Spectrum (400 MHz, CDCl3 solution) expansion (not to scale) 7.2 7.1 Problem 163 40 0 8 (ppm) expansion (not to scale) 2.9 2.8 expansion (not to scale) exchanges with D₂O 1.3 1.2 TMS 10 9 8 7 6 5 4 3 2 1 0 8 (ppm)
3372 IR Spectrum (liquid film) 4000 3000 2000 1600 1200 800 V (cm) 100 80 60 40 20 % of base peak 106 148 Mass Spectrum M 149 C10H15N 40 80 120 160 200 240 280 m/e 13C NMR Spectrum (100 MHz, CDCl, solution) DEPT CH2CH3CH proton decoupled expansion 130 125 expansion 130 125 solvent 200 160 120 80 1H NMR Spectrum (400 MHz, CDCl3 solution) expansion (not to scale) 7.2 7.1 Problem 163 40 0 8 (ppm) expansion (not to scale) 2.9 2.8 expansion (not to scale) exchanges with D₂O 1.3 1.2 TMS 10 9 8 7 6 5 4 3 2 1 0 8 (ppm)
Chapter13: Structure Determination: Nuclear Magnetic Resonance Spectroscopy
Section13.SE: Something Extra
Problem 29AP
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please provide the structure for this problem, thank you!
Transcribed Image Text:3372
IR Spectrum
(liquid film)
4000
3000
2000
1600
1200
800
V (cm)
100
80
60
40
20
% of base peak
106
148
Mass Spectrum
M
149
C10H15N
40
80
120
160
200
240
280
m/e
13C NMR Spectrum
(100 MHz, CDCl, solution)
DEPT CH2CH3CH
proton decoupled
expansion
130
125
expansion
130
125
solvent
200
160
120
80
1H NMR Spectrum
(400 MHz, CDCl3 solution)
expansion
(not to scale)
7.2 7.1
Problem 163
40
0
8 (ppm)
expansion
(not to scale)
2.9 2.8
expansion
(not to scale)
exchanges
with D₂O
1.3 1.2
TMS
10 9
8
7
6
5
4
3
2
1
0
8 (ppm)
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