lab 10 report

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Mechanical Engineering

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Jan 9, 2024

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Objective As in laboratory experiment #2 (Tensile test in metals) the objective of this experiment is to study the effect of temperature and displacement rate on polymers when put under tensile force. And compare results with those obtained in experiment #2. Materials and equipment Instron tensile testing machine. Environmental chamber. Test specimens: - Acrylic /PMMA (Poly (methyl methacrylate)) Nylon 6.6 (Polyamide) or PE (Polyethylene) - Experimental Procedure Take the initial measurements of the specimens (gage length, diameter). Record them in table 2. Use a permanent marker to mark the middle 2- inch span of the specimen’s narrow section to specify where to mount the arms of the extensometer. Input the data (material name, displacement rate, gage length, diameter, and geometry of the specimen) of the test into Merlin software. Follow the tensile testing matrix shown in Table1. Mount the specimen into the threaded grips enclosed by the environmental chamber. Keep the acrylic specimen at 60°C in the environmental chamber for 1 hour.
1 Remove the fractured test specimen from the grips and measure the final gage length on the specimen. Also, measure the diameter of the specimen at the fracture (the neck). Record the final measurements (gage length, diameter) in table 2. Follow the same procedure described above for Nylon 6.6 (Polyamide) & PE (Polyethylene) without using environmental chamber and utilize the extensometer. Results Table 1: Measurements for the specimens tested Specimen Young’s Modulus/MPa Yield Strength/MPa Yield Strain Ultimate Tensile/MPa PMMA (60 °C) 700.6 35.09 0.05 52.73 PMMA (low rate) 2236.9 43.01 0.03 79.82 PMMA (high rate) 2380.6 57.03 0.03 73.02 PE (low rate) 810.82 12.48 0.05 17.67 PE (high rate) 1143 22.10 0.05 27.58 Nylon (low rate) 2976.1 16.16 0.05 22.51
2 Nylon (high rate) 3247.5 69.99 0.05 78.98 Table 2: A comparison of the mechanical properties of the specimens. The values are obtained from MIcrosoft Excel Specimen Failure Tensile Stress Failure Tensile Strain Elongation (%) Area Reduction (%) Poisson’s Ratio PMMA (60°C) 43.69 0.63 53.57 61.32 0.71 PMMA (low rate) 79.78 0.08 1.72 0.44 0.13 PMMA (high rate) 73.01 0.05 1.67 0.44 0.13 PE (low rate) 17.56 1.78 46.03 73.4 1.19 PE (high rate) 14.01 2.15 86.15 70.65 0.74 Nylon (low rate) 19.31 0.33 33.85 79.58 1.43 Nylon (high rate) 28.11 0.68 31.75 87.06 1.44 Table 3: A comparison of the mechanical properties of the specimens. The values are obtained from MIcrosoft Excel Following are the engineering stress vs engineering strain graphs for all the specimens tested
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3 Discussion The data obtained at room temperature for Acrylic in low displacement and plexiglass in high displacement is incoherent because we did not have enough data points to work with, which lead to inadequate leading curves. Based on the plots, we see that acrylic at room temperature in low displacement has the second highest yield strength and ultimate strength. The difference between low and high displacement rate is the change in strain. Nylon at room temperature has less yield strength in low displacement rate compared to
4 the high displacement rate. The plots of Nylon in low & high displacement rate are similar but after 1-strain units, the graph of the high rate decreases and has a greater ultimate strength than the low rate. Nevertheless, the Stress vs. Strain curve for plexiglass demonstrates that strain is more apparent at room temperature than in high displacement rate at 60 °C. The yield strength is also greater at room temperature than at 60°C. Since there is more deformation going on in the higher temperature, the failure occurs faster (at low strain) at room temperature than at 60°C. Review Questions 1. Determine the yield, maximum, and failure values of load and displacement from the load displacement data provided by the machine. - Refer to the “Results” section 2. Plots of Engineering Stress vs Strain are required for each specimen. Overplot stress strain data of the tested specimens in a figure. - Refer to the “Results” section. 3. Determine the mechanical properties of each tested specimen (Young’s Modulus, yield stress, yield strain, Poisson’s ratio, failure stress, failure strain, ductility (%EL)), and show your calculations explicitly. Compare your calculations with the literature and compute the percentage error. - Refer to the “Results” section. 4. Did fracture occur at the neck for the nylon or PE? - The Facture did not take place at the necking of Nylon at low displacement rate and PE in both cases the specimens were only stretched and elongated. 5. After necking of the nylon or PE specimen, did further deformation occur at the neck area?
5 - After necking further deformation took place at the neck area, it can only be drawn a similarity with PMMA at high temperature. 6. Were similar phenomena observed when testing the PMMA specimen? - PMMA specimens tested at room temperature have a brittle mode of failure while PMMA at high temperature the largest plastic deformation. The strain of PMMA at high temperature showed the largest ductility compared to the other PMMA specimens. 7. Are the modes of failure of the PMMA and nylon or PE specimens similar? Why? - The failure modes of PMMA and nylon are similar because high strain rate leads to greater yield strength and ultimate strength but decreases ductility. 8. What are the effects of high strain rate on the failure mode and on the mechanical properties of each of the PMMA and nylon or PE specimen? Did you observe a similar phenomenon for metals you tested at lab 2? - In the nylon material, greater strain rate causes the plastic deformation rate to increase. The mode of failure was around the same for acrylic at high strain rate. 9. Does the failure mode of polymers differ from that of metals? Explain in detail. - Failure more in polymers are different from metals as they have weak intermolecular interactions. The reversible deformation in the material causes the modulus of elasticity to be less. Nonetheless, polymers experience additional strain in the elastic region than metals. 10. What is the elastic deformation mechanism for nylon or PE? Is it different from that of metals? In what way? - Nylon has more reversible deformation and can experience more strain than metals because the material has more necking and went through crazing.
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6 11. What is the plastic deformation mechanism for nylon? How does it affect the shape of the engineering stress-strain curve? - In Nylon, the necking spreads which causes a lot of crazing. The strain is also increased in the plastic region of the stress-strain curve. 12. Discuss how the microstructures of polymers and metals make their behavior under mechanical loading different. - Metals do not go through crazing because their microstructure is not composed of chains that can be straightened into units. The microstructure of metals is not very ductile compared to polymers. This is because the interior of metals is constructed of crystal material. However, polymers contain lower tensile strength. 13. What is the temperature effect on stress-strain curves on PMMA? Do you expect to have similar effects on aluminum or steel you tested at lab 2? - The stress-strain curve for PMMA is greatly impacted by temperature. According to the plots, strain varies with temperature. 14. What effect does temperature have on the rupture stress? - Higher temperatures decrease rupture stress. 15. What effect does temperature have on the rupture strain? - Higher temperatures increase the rupture strain. Conclusions
7 The experiment allowed us to analyze and compare the properties of different polymers under tensile loading at different displacement rates and temperatures. A further goal achieved was to compare the results with those of metals. It was observed that displacement rate and temperatures affect Young’s modulus, yield strength and strain, as well as modes of failure of the materials tested. References Callister, William D. Rethwisch, David G. “Materials Science & Engineering”. 2010 edition. Li, J. Lab Manuals . CUNY Blackboard Website.