Ahmed Chishti_Course Orientation Scan
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Michigan State University *
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Course
162
Subject
Chemistry
Date
Feb 20, 2024
Type
Pages
12
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COURSE ORIENTATION LABORATORY SCAVE
N
GER HU
N
T Before you can effectively use a laboratory space, you must be familiar with the location of materials and equipment. Identify the location of the items listed within the floor plan below. These items may be available inside the lab or in the hallways outside the lab room. JBr" Dispensing fume hood K Waste fume hood Jej(sink @' DI/RO water tap Safety shower Eyewash station Fire extinguisher Team power outlets Team lab air nozzles Dustpan and broom Balance areas Broken glassware box ,A-
Equipment shelves Gloves Markers & labeling tape IR Spectrometer ,,d} Paper towels Centrifuge Storage area for personal belongings Emergency response ICE bucket flyer Oven . Spill kit .....
Team vacuum nozzles ICE machine* Team natural gas .,.,.,.,,, nozzles ',u-' First aid supplies* * Ibten
1
1
s st0red near Chemistry Stockroom. Mark the direction of the Chemistry Stockroom relative to your map e ow. ,,
~
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otebook Submission (Ind" 'd I A . . iv1 ua ss1gnment) 19
-
l Within the following images
, fill in the blanks for the laboratory equipment stored on each shelf. Throughout the semester your course section will be responsible for returning all equipment in good condition
, to the proper location
. Any lab section that fails to keep the laboratory clean and organized, will receive a deduction of Contribution points
. (10) Plastic Beakers (20) Metal Beakers -
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LABORATORY ACCIDE
N
TS Fill in the table below pe
rtamm
g to the lab accid
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oves
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cy shower
, etc.) u~ iC-ew
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EFFECTIVE PROCEDURE DESIG
N
niroughout the seme
st
er
,_ y~u will ~ork with your team to plan original experimental investigations to ~swer s~icnt
1
fi_c q_uesllons
, solve problems
, and/or design solutions associated with project scenanos
. ~hile designing your experiments
, it is critical to effectively communicate your procedural p~ans with you~ te~ates as well as your lab instructor(s)
. Listed below are some important guidelines for designing comprehensive procedures
; keep these ideas in mind throughout the semester as your team designs procedures for each Jab project. Procedure Design Guidelines • Safety First!! Indicate anr hazards and important chemical waste disposal, at each applicable step. • Detailed directions for each step, with indications of appropriate order of operations. o Instructions must be clear enough that someone unfamiliar with the project and goals could carry out your procedure on their own. o Use an appropriate balance between thorough documentation and over-explanation. For example
, it is not necessary to instruct readers to remove a reagent cap before pipetting, but you should indicate exactly how much solution to pipet. • Use illustrations (pictures, diagrams, etc.) to help the reader interpret the procedure. Remember, a picture is worth 1000 words! • Provide more than a recipe. Explain the science and goals behind procedural steps so there is some basis of knowledge for knowing how to adapt and improvise to resolve unforeseen issues. • What data to record and how to record data. Expected units of measurement that are explicit, including the appropriate number of significant figures. • Cleaning up after yourself is not glamourous, but it is important to include steps within your procedures for handling waste and cleaning/returning used equipment. Cleanup takes time and your team must plan so you can finish and leave the lab in good condition on time
. PROCEDURE DESIG
N
I
N
G PRACTICE For this activity, your team has been assigned the following task
. Your lab instructor will provide a preliminary procedure to complete the task. Please do your best in giving this a try! This exercise is meant to be a memorable experience to demonstrate the importance of writing comprehensive procedures, not an exercise in flawlessness. Assigned Task Create a rainbow-colored column using the following materials, in addition to the elementary lab materials that are always available in the lab
. The values listed below are the maximum total amounts available for your team to use. Your team is NOT required to use all the materials listed. • (2 g) Sodium Chloride • FD&C Red #40 dye • FD&C Blue #1 dye • FD&C Yell ow #5 dye Include this page with your N
otebook Submission. (Individual Assignment)
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[ PART 1: Attempt the provided pr d _ oce ure. Refer
e
ncing the procedure provided by your lab instructor
, create a r . Use th
e space below to record data and work out any ideas yo t a,_nbow~olored column. Be prepared to report out your team
's progress (question 1
.t e;m discovers ~Ion? the way. in art 2) when time 1s up
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PART 2: Reflect on the challenges of using the provided procedure. I. What did you focus on to begin? Were there any context-clues your team used? What inferences or assumptions did you make? Did you refer to any outside resources? wt. f-oc-
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l PART 3: Design a thorough procedure. . r t
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m to des
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mpr
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: I : When completed, use a camera-equipped mobile device and scanning application of your choice (i.e., the Genius Scan app), to upload a PDF copy of your completed Course Orientation pages to the appropriate assignment Dropbox in D2L. This is an I
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U...
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A chemist working as a safety inspector finds an unmarked bottle in a lab cabinet. A note on the door of the cabinet says the cabinet is used to store bottles of
diethylamine, pentane, acetone, carbon tetrachloride, and tetrahydrofuran.
The chemist plans to try to identify the unknown liquid by measuring the density and comparing to known densities. First, from her collection of Material Safety
Data Sheets (MSDS), the chemist finds the following information:
liquid
density
g
0.71
mL
diethylamine
olo
Ar
pentane
0.63
mL
g
0.79
mL
acetone
g
1.6
mL
carbon tetrachloride
g
0.89
mL
tetrahydrofuran
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1. For each field, which problem is being addressed by the consumer product?
2. What are some chemical components of the consumer products?
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Suppose you accidentally drop a glass bowl full of sugar onto the floor, causing the bowl to shatter into pieces.
Which of the procedures would be the most effective way to separate the sugar from the tiny pieces of glass?
Collect all of the sugar and glass pieces into a pot and heat the mixture to melt the sugar. Then, pour the liquid sugar through a filter to separate the glass from the sugar.
Collect all of the sugar and glass pieces into a bucket of water. Allow the water to dissolve the sugar, then remove the water and sugar solution, leaving the glass behind in the bucket. The solution is then heated to evaporate the water, leaving the sugar behind.
Use a magnifying glass and tweezers to safely remove the glass particles from the mixture.
Sweep a magnet across the spill to attract the glass particles and remove them from the mixture.
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During a laboratory experiment, a student mixed two homogeneous aqueous solutions. After mixing a solid precipitate was formed. What is the best way for the solid to be separated from the solution?
Put it in a beaker and heat it.
Filter it using a Buchner funnel, filter flask and vacuum pump.
Use a pipette to remove the solid from the liquid.
Scoop it out with a spatula.
The solid cannot be isolated.
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On a dry day, your hair flies apart when you brush it. How would you explain this?Match the words in the left column to the appropriate blanks in the sentences on the right.
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Emily attempts to separate a mixture of iodine crystals, table sugar, and iron powder. First, she weighs out an empty beaker, weighs it empty, transfers her mixture to the beaker, and then reweighs it. She then gently heats the mixture under a vacuum to sublime all of the iodine. After the sample has cooled, she reweighs the dry sample containing only iron and sugar. She then takes the remaining sample and adds some distilled water to dissolve the sugar but not the iron. She places a strong rare earth magnet beneath the flask to attract all of the iron particles and pours out (decants) the sugar solution into a new beaker (beaker #2). She also rinses the iron particles once or twice more to make sure all of the sugar is dissolved and decants the rinse water into the beaker with the sugar solution. She then gently warms the iron powder to dry it and reweighs it in the original beaker. Finally, she takes the sugar solution and heats it to evaporate off all the water to obtain dry sugar…
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