Lab Report-2-Matter and Phase Changes Distil Ethanol
docx
keyboard_arrow_up
School
Madisonville Community College *
*We aren’t endorsed by this school
Course
130
Subject
Chemistry
Date
Jun 18, 2024
Type
docx
Pages
4
Uploaded by JusticeFogGuanaco38
Matter and Phase Changes: Distil Ethanol
Exp. No. 2
I. Purpose
The purpose of this lab simulation was to learn about the three states of matter: solid, liquid and gas. The experiment performed was the distillation of ethanol while modifying the conditions in order to observe the process of phase changes.
A sample of ethanol (C2H5OH) 80% and water 20% (v/v) was obtained in order to produce a bioethanol. II. Experimental Method
A heating curve for H20 was created using a 500 mL beaker of ice, a heating plate set at -50 degrees C. and a temperature probe. Creation of the heating curve of H20 helped
establish the evaporation and melting point of ethanol (C2H5OH). 78 degrees C and -
115 degrees C, respectively. A 500 mL suction flask of C2H5OH was used. The distillation apparatus was set to 78 degrees C to separate the homogenous sample of C2H5OH 80% and H20 20% (v/v). The 100 mL collecting flask showed the first attempt was unsuccessful with the results paralleled the original sample of C2H5OH 80% and H20 20% (v/v). The realization that the atmospheric pressure varied from the highlands,
the atm needed to be mimicked in the lab. A suction flask of 500 Ml of ice on a heat plate, a vacuum pump to a suction flask using a vacuum hose. A reduced pressure was produced showing a change in evaporation and melting points. This recreates the 0.53 atm, showing a boiling point of 62.21 degrees C. for C2H5OH and H20. These changes produced a purer form of C2H5OH.
III. Data and Calculations
Materials used: Suction flask 500 mL (Contains: Ice)
Suction flask 500 mL (Contains: Ethanol)
Heating mantle
Distilling flask
Condensor Collecting flask
Vacuum hose
Cooling water in
Cooling water out
Heat plate
Temperature probe
Sates of Matter
Solid
Rigid It has both a fixed shape and volume.
Liquid Assumes the shape of its container. It has a distinct volume but has no specific forms.
Gas
Also known as vapor. Takes the volume and shape of its container.
It has no definite shape and volume.
Phase Changes Melting
energy required to break the intermolecular forces and increase the motion of the particles during solid to liquid transition
Vaporization particle movement keeps increasing as the temperature rises. The motion of the particles becomes more rapid and spread apart as the particles move into gaseous states
Sublimination
Some solids can skip the liquid phase and change to the gaseous state directly. Classification of Matter
Pure Substance
is a matter that has a constant composition.
Element is a type of substance that cannot be broken into a simpler substance by chemical change. Each element is composed of only one kind of atom. Compound
is two or more different kinds of elements can combine.
Mixture
combination of different substances. Homogenous Mixture
mixtures that are uniform throughout.
Heterogeneous Mixture
mixture that varies in composition, properties and appearance throughout.
IV. Results The results of this experiment showed that by adjusting the melting, boiling and atm, it was possible to achieve the goal of bioethanol.
V. Conclusion
The lab simulation elaborated on the three states of matter by giving visuals, definitions and showing that there is kinetic energy and intermolecular forces between the molecules. The lab taught how essential it is a knowing how to read and determine the heating curve of a given substance in order to achieve the desired results. A combination of these fundamentals helped in performing the distillation technique to successfully produce bioethanol. Reference:
150+ virtual labs for universities and high schools
. Labster. (n.d.). https://www.labster.com/. FEEDBACK
Great job, keep it up!
Lab 2
+1/1 formatting
DO NOT USE PERSONAL PRONOUNS (I, you, we, etc.) IN LAB REPORTS!
Purpose
+2/2 purpose mentions purifying/distilling ethanol to extend gasoline supply
Methods
+2/3 Mentions 3 of 5: heat water to produce heating curve, heat ethanol to produce heating curve, distil ethanol at 78
°
C, heat water at lower pressure to produce heating curve, distil ethanol at lower temperature
Data and Calcs
+0/1 boiling point of ethanol 78
°
C
+0/1 result of distillation 80% H2O/20% EtOH
+0/1 distillation at 0.53 atm
+0/1 distillation at 61.21
°
C
+0/1 result of distillation 44% H2O/56% EtOH
Results
Temperature (
°
C
)
Pressure (atm)
%v/v
Normal BP
78
1
80% H2O/20% EtOH
Reduced Pressure
61.21
0.53
44% H2O/56% EtOH
+5
No table of data, only qualitative
REPORT THESE DATA IN A TABLE!
Conclusions
+2/4 Conclusions section does not include purpose
Your preview ends here
Eager to read complete document? Join bartleby learn and gain access to the full version
- Access to all documents
- Unlimited textbook solutions
- 24/7 expert homework help
FEEDBACK
Use the feedback and grading key to keep improving your reports!
Related Documents
Related Questions
Heating a solid until it passes directly from the solid phase into the gaseous phase.
Separating a liquid from an insoluble solid sediment by carefully pouring the liquid from the
solid without disturbing the solid.
The process of vapor returning to the solid phase without a liquid phase in between.
Heating a mixture to vaporize a volatile liquid component to make the remaining component dry.
Separating a solid from a liquid using a porous material, such as paper, charcoal, or sand, as
a filter.
Using a solvent to selectively dissolve one or more components from a solid mixture.
Answer Bank
extraction
filtration
decantation
deposition
sublimation
evaporation
arrow_forward
A certain liquid X has a normal boiling point of 93.90 °℃ and a boiling point elevation constant K₁ = 1.14 °C-kg-mol¯¹. Calculate the boiling point of a solution
made of 40.1g of zinc chloride (ZnCl₂) dissolved in 350. g of X.
Round you answer to 4 significant digits.
°C
x10
X
1
Ś
arrow_forward
5. Chemical Xis a solid with white color that forms large crystals. The solubility of
chemical X in water at different temperatures is shown below.
Solubility of X in H20
124
10-
8-
6-
2-
0+
Ó 10 20 30 40 50 60 70 80 90100
Temperature (°C)
Irina wants to dissolve 30 grams of Xin 1 liter of water. She does so by stirring
30 grams of the large crystals into 1 liter of water at 45°C. How could Irina change
her method to dissolve all the X faster?
Solubility (g/100 g H,O)
4-
arrow_forward
Why is fractional distillation more efficient than simple distillation when purifying liquid mixtures?
arrow_forward
Balance
arrow_forward
ed
The boiling point of water is 100.00 °C at 1 atmosphere.
A student dissolves 12.63 grams of sodium sulfide, Na₂S (78.05 g/mol), in 163.3 grams of water. Use the table of
boiling and freezing point constants to answer the questions below.
Solvent
Water
Ethanol
Chloroform
Benzene
Formula
H₂O
CH3CH₂OH
CHCI 3
соно
Diethyl ether CH3CH₂CH₂CH3
The molality of the solution is
The boiling point of the solution is
Kb (°C/m) Kf (°C/m)
0.512
1.86
1.22
1.99
3.67
2.53
2.02
m.
°C.
5.12
arrow_forward
The boiling point of water is 100.00 °C at 1 atmosphere.
A student dissolves 14.52 grams of calcium acetate, Ca(CH3COO)2 (158.2 g/mol), in 156.5 grams of water. Use the table of boiling and freezing point constants to answer the questions below.
Solvent
Formula
Kh (°C/m) Kf (°C/m)
Water
H20
0.512
1.86
Ethanol
CH3CH2OH
1.22
1.99
Chloroform
CHCI3
3.67
Benzene
C6H6
2.53
5.12
Diethyl ether CH3CH2OCH2CH3
2.02
The molality of the solution is
m.
The boiling point of the solution is
°C.
arrow_forward
Only typed solution.
arrow_forward
Part B
The solvent for an organic reaction is prepared by mixing 70.0 mL of acetone (C3H6O) with 64.0 mL of ethyl acetate (C4H8O2). This mixture is stored at
25.0 °C. The vapor pressure and the densities for the two pure components at 25.0 °C are given in the following table. What is the vapor pressure of the
stored mixture?
Vapor pressure Density
Compound
(mmHg) (g/mL)
230.0
0.791
95.38
0.900
acetone
ethyl acetate
Express your answer to three significant figures and include the appropriate units.
▸ View Available Hint(s)
Psoln:
HÅ
Units
Value
?
arrow_forward
Part E
Write balanced complete ionic equation for NaOH(aq)+ HC,H,O2 (aq)→H,O(1) + NaC, H,O2 (aq).
Express your answer as a chemical equation. Identify all of the phases in your answer.
ΑΣΦ
x"
O That's not quite right. Please check your formatting and try again
No credit lost. Try again.
Submit
Previous Answers Request Answer
Part F
Write balanced net ionic equation for NAOH(aq) | HC,H,O, (aq) H,O(1) i NaC, H,O, (aq).
Express your answer as a chemical equation. Identify all of the phases in your answer.
arrow_forward
The boiling point of water is 100.00 °C at 1 atmosphere.
A student dissolves 14.27 grams of magnesium acetate,
Mg(CH3COO)2 (142.4 g/mol), in 201.2 grams of water. Use the table of
boiling and freezing point constants to answer the questions below.
Solvent
Formula
Kb (°C/m) Kf (°C/m)
Water
H₂O
0.512
1.86
Ethanol
CH3CH2OH
1.22
1.99
Chloroform
CHCl3
3.67
Benzene
C6H6
2.53
5.12
Diethyl ether CH3CH2OCH2CH3
2.02
The molality of the solution is
The boiling point of the solution is
m.
°C.
arrow_forward
302
301
300
299
298
297
(K)
296
295
294
293
292
0.2
0.4
0.6
0.8
XA
According to the phase diagram shown for mixtures of A and B shown above, if xA
0.2, solid
A (enter A or B) will start to precipitate from a
homogeneous solution when the temperature reaches
A K (enter
the temperature to zero decimal places).
arrow_forward
Submit
Previous Answers
A solid mixture consists of 25.5 g of KNO (potassium nitrate) and
4.5 g of K2SO4 (potassium sulfate). The mixture is added to 130. g
of water
v Correct
Use this solubility curve (Eigure 1) to answer the questions.
Crystallization
Crystallization is the opposite of dissolution. Since solids tend to dissolve better at higher temperatures, we can cause them to crystallize (i.e., undissolve) from a solution
by lowering the temperature.
Part B
If the solution described in the introduction is cooled to 0 °C, what mass of KNO, should crystallize?
Enter your answer numerically in grams.
• View Available Hint(s)
Figure
< 1 of 1
29.65
KNO, / NH,CI
Previous Answers
Submit
50-
Nac
X Incorrect; Try Again; 6 attempts remaining
40
30
LiSO,
Part C Complete previous part(s)
20 -
K,SO,
10-
Part D
KCIO,
10
20
30
40
50
60
For which salt, K2SO,, LişSO,. KCIO,, or NH,C1, will increasing the temperature of the water have the greatest change in solubility per 100 g solvent?…
arrow_forward
Part A
H2 SO4 (aq) and LİOH(ag)
Express your answer as a chemical equation. Identify all of the phases in your answer.
ΑΣφ
?
Submit
Request Answer
Part B
HCl(aq) and Al(OH)3 (s)
Express your answer as a chemical equation. Identify all of the phases in your answer.
ΑΣφ
?
Submit
Request Answer
Part C
H2 SO3 (ag) and Mg(OH)2(s)
Express your answer as a chemical equation. Identify all of the phases in your answer.
arrow_forward
In addition to the separation techniques used in this lab (magnetism, evaporation, and filtering), there are other commonly used separation techniques. Some of these techniques are:Distillation – this process is used to separate components that have significantly different boiling points. The solution is heated and the lower boiling point substance is vaporized first. The vapor can be collected and condensed and the component recovered as a pure liquid. If the temperature of the mixture is then raised, the next higher boiling component will come off and be collected. Eventually only non-volatile components will be left in the original solution.Centrifugation – a centrifuge will separate mixtures based on their mass. The mixture is placed in a centrifuge tube which is then spun at a high speed. Heavier components will settle at the bottom of the tube while lighter components will be at the top. This is the technique used to separate red blood cells from blood plasma.Sieving – this is…
arrow_forward
SylvanPrep
edx edX| Free Online...
C Coursera| Online...
= College Algebra B..
an...
- Calcworkshop
Resources
O Hint
Check Answer
45.9%
Assignment Score:
Question 32 of 41
A new linear temperature scale, degrees Zunzol (°Z), is based on the freezing point and boiling point of a newly discovered
compound zunzol. The freezing point of zunzol, -141.5 °C, is defined as 0 °Z, and the boiling point of zunzol, -24.8 °C, is
defined as 100 °Z. What is the freezing point of water in degrees Zunzol?
|
freezing point:
What is the boiling point of water in degrees Zunzol?
boiling point:
1037
10
A stv
P.
2.
arrow_forward
The 50:50 (by mass) mix of water and ethylene glycol (antifreeze) contains 16 moles
of ethylene glycol per 1 kg of water.
Given than K₁ for water is 0.5 °C/m, what is the boiling point of the mixture?
100.5°C
108 °C
92°C
100°C
99.5°C
arrow_forward
Solvent
Formula
Diethyl
ether
Water
Ethanol
Chloroform CHCl3
Benzene C6H6
H₂O
CH3 CH₂ OH
Kb (°C/m) K(°C/m)
0.512
The molality of the solution is
The freezing point of the solution is
1.22
3.67
2.53
CH3 CH₂ OCH₂ CH3 2.02
m.
1.86
1.99
5.12
°C.
arrow_forward
Petroleum chemistry
arrow_forward
A certain liquid X has a normal boiling point of 105.30 °C and a boiling point elevation constant K₁ = 1.74 °C-kg-mol¯¹. Calculate the boiling point of a
solution made of 8.59g of ammonium chloride (NHCl) dissolved in 150. g of X.
Round you answer to 5 significant digits.
пос
x10
X
arrow_forward
Acrylonitrile and ethyl acetate have the same boiling point: 77.20C. Which
statement explains the outcome you would expect if a mixture of these
two substances were distilled? *
The acrylonitrile would vaporize first and the ethyl acetate would be left behinc
O The ethyl acetate would vaporize first and the acrylonitrile would be left behind
Both substances would vaporize at the same time so distillation would not be h
Ethyl acetate is a solid so distillation would involve allowing the acrylonitrile to
evaporate.
Which statement best explains why structural formulas are good for
depicting polymers?
arrow_forward
4. Why is fractional distillation more "efficient" than simple distillation?
During boiling point determination the temperature of the vapors is be
E
arrow_forward
SEE MORE QUESTIONS
Recommended textbooks for you

Chemistry: The Molecular Science
Chemistry
ISBN:9781285199047
Author:John W. Moore, Conrad L. Stanitski
Publisher:Cengage Learning
Related Questions
- Heating a solid until it passes directly from the solid phase into the gaseous phase. Separating a liquid from an insoluble solid sediment by carefully pouring the liquid from the solid without disturbing the solid. The process of vapor returning to the solid phase without a liquid phase in between. Heating a mixture to vaporize a volatile liquid component to make the remaining component dry. Separating a solid from a liquid using a porous material, such as paper, charcoal, or sand, as a filter. Using a solvent to selectively dissolve one or more components from a solid mixture. Answer Bank extraction filtration decantation deposition sublimation evaporationarrow_forwardA certain liquid X has a normal boiling point of 93.90 °℃ and a boiling point elevation constant K₁ = 1.14 °C-kg-mol¯¹. Calculate the boiling point of a solution made of 40.1g of zinc chloride (ZnCl₂) dissolved in 350. g of X. Round you answer to 4 significant digits. °C x10 X 1 Śarrow_forward5. Chemical Xis a solid with white color that forms large crystals. The solubility of chemical X in water at different temperatures is shown below. Solubility of X in H20 124 10- 8- 6- 2- 0+ Ó 10 20 30 40 50 60 70 80 90100 Temperature (°C) Irina wants to dissolve 30 grams of Xin 1 liter of water. She does so by stirring 30 grams of the large crystals into 1 liter of water at 45°C. How could Irina change her method to dissolve all the X faster? Solubility (g/100 g H,O) 4-arrow_forward
- Why is fractional distillation more efficient than simple distillation when purifying liquid mixtures?arrow_forwardBalancearrow_forwarded The boiling point of water is 100.00 °C at 1 atmosphere. A student dissolves 12.63 grams of sodium sulfide, Na₂S (78.05 g/mol), in 163.3 grams of water. Use the table of boiling and freezing point constants to answer the questions below. Solvent Water Ethanol Chloroform Benzene Formula H₂O CH3CH₂OH CHCI 3 соно Diethyl ether CH3CH₂CH₂CH3 The molality of the solution is The boiling point of the solution is Kb (°C/m) Kf (°C/m) 0.512 1.86 1.22 1.99 3.67 2.53 2.02 m. °C. 5.12arrow_forward
- The boiling point of water is 100.00 °C at 1 atmosphere. A student dissolves 14.52 grams of calcium acetate, Ca(CH3COO)2 (158.2 g/mol), in 156.5 grams of water. Use the table of boiling and freezing point constants to answer the questions below. Solvent Formula Kh (°C/m) Kf (°C/m) Water H20 0.512 1.86 Ethanol CH3CH2OH 1.22 1.99 Chloroform CHCI3 3.67 Benzene C6H6 2.53 5.12 Diethyl ether CH3CH2OCH2CH3 2.02 The molality of the solution is m. The boiling point of the solution is °C.arrow_forwardOnly typed solution.arrow_forwardPart B The solvent for an organic reaction is prepared by mixing 70.0 mL of acetone (C3H6O) with 64.0 mL of ethyl acetate (C4H8O2). This mixture is stored at 25.0 °C. The vapor pressure and the densities for the two pure components at 25.0 °C are given in the following table. What is the vapor pressure of the stored mixture? Vapor pressure Density Compound (mmHg) (g/mL) 230.0 0.791 95.38 0.900 acetone ethyl acetate Express your answer to three significant figures and include the appropriate units. ▸ View Available Hint(s) Psoln: HÅ Units Value ?arrow_forward
- Part E Write balanced complete ionic equation for NaOH(aq)+ HC,H,O2 (aq)→H,O(1) + NaC, H,O2 (aq). Express your answer as a chemical equation. Identify all of the phases in your answer. ΑΣΦ x" O That's not quite right. Please check your formatting and try again No credit lost. Try again. Submit Previous Answers Request Answer Part F Write balanced net ionic equation for NAOH(aq) | HC,H,O, (aq) H,O(1) i NaC, H,O, (aq). Express your answer as a chemical equation. Identify all of the phases in your answer.arrow_forwardThe boiling point of water is 100.00 °C at 1 atmosphere. A student dissolves 14.27 grams of magnesium acetate, Mg(CH3COO)2 (142.4 g/mol), in 201.2 grams of water. Use the table of boiling and freezing point constants to answer the questions below. Solvent Formula Kb (°C/m) Kf (°C/m) Water H₂O 0.512 1.86 Ethanol CH3CH2OH 1.22 1.99 Chloroform CHCl3 3.67 Benzene C6H6 2.53 5.12 Diethyl ether CH3CH2OCH2CH3 2.02 The molality of the solution is The boiling point of the solution is m. °C.arrow_forward302 301 300 299 298 297 (K) 296 295 294 293 292 0.2 0.4 0.6 0.8 XA According to the phase diagram shown for mixtures of A and B shown above, if xA 0.2, solid A (enter A or B) will start to precipitate from a homogeneous solution when the temperature reaches A K (enter the temperature to zero decimal places).arrow_forward
arrow_back_ios
SEE MORE QUESTIONS
arrow_forward_ios
Recommended textbooks for you
- Chemistry: The Molecular ScienceChemistryISBN:9781285199047Author:John W. Moore, Conrad L. StanitskiPublisher:Cengage Learning

Chemistry: The Molecular Science
Chemistry
ISBN:9781285199047
Author:John W. Moore, Conrad L. Stanitski
Publisher:Cengage Learning