Introduction to Chemistry
4th Edition
ISBN: 9781259288722
Author: BAUER
Publisher: MCG
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Question
Chapter 9, Problem 158QP
(a)
Interpretation Introduction
Interpretation:
The correct statement is to be identified.
(b)
Interpretation Introduction
Interpretation:
The correct statement is to be identified.
(c)
Interpretation Introduction
Interpretation:
The correct statement is to be identified.
(d)
Interpretation Introduction
Interpretation:
The correct statement is to be identified.
(e)
Interpretation Introduction
Interpretation:
The correct statement is to be identified.
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You have now performed a liquid-liquid extraction protocol in Experiment 4. In doing so, you
manipulated and exploited the acid-base chemistry of one or more of the compounds in your
mixture to facilitate their separation into different phases. The key to understanding how liquid-
liquid extractions work is by knowing which layer a compound is in, and in what protonation state.
The following liquid-liquid extraction is different from the one you performed in Experiment
4, but it uses the same type of logic. Your task is to show how to separate apart Compound
A and Compound B.
. Complete the following flowchart of a liquid-liquid extraction. Handwritten work is
encouraged.
•
Draw by hand (neatly) only the appropriate organic compound(s) in the boxes.
.
Specify the reagent(s)/chemicals (name is fine) and concentration as required in Boxes 4
and 5.
•
Box 7a requires the solvent (name is fine).
•
Box 7b requires one inorganic compound.
• You can neatly complete this assignment by hand and…
b) Elucidate compound D w) mt at 170 nd shows c-1 stretch at 550cm;'
The compound has the ff electronic transitions: 0%o* and no a*
1H NMR Spectrum
(CDCl3, 400 MHz)
3.5
3.0
2.5
2.0
1.5
1.0
0.5 ppm
13C{H} NMR Spectrum
(CDCl3, 100 MHz)
Solvent
80
70
60
50
40
30
20
10
0 ppm
ppm
¹H-13C me-HSQC Spectrum
ppm
(CDCl3, 400 MHz)
5
¹H-¹H COSY Spectrum
(CDCl3, 400 MHz)
0.5
10
3.5
3.0
2.5
2.0
1.5 1.0
10
15
20
20
25
30
30
-35
-1.0
1.5
-2.0
-2.5
3.0
-3.5
0.5
ppm
3.5
3.0
2.5
2.0
1.5
1.0
0.5
ppm
Show work with explanation. don't give Ai generated solution
Chapter 9 Solutions
Introduction to Chemistry
Ch. 9 - Prob. 1QCCh. 9 - Prob. 2QCCh. 9 - Prob. 3QCCh. 9 - Prob. 4QCCh. 9 - Prob. 5QCCh. 9 - Prob. 1PPCh. 9 - Prob. 2PPCh. 9 - What pressure is needed to compress 455 mL of...Ch. 9 - Prob. 4PPCh. 9 - Prob. 5PP
Ch. 9 - Prob. 6PPCh. 9 - Prob. 7PPCh. 9 - Prob. 8PPCh. 9 - Prob. 9PPCh. 9 - Prob. 10PPCh. 9 - Prob. 11PPCh. 9 - Prob. 12PPCh. 9 - Prob. 13PPCh. 9 - Prob. 14PPCh. 9 - Prob. 15PPCh. 9 - Prob. 16PPCh. 9 - Prob. 17PPCh. 9 - Prob. 18PPCh. 9 - Prob. 1QPCh. 9 - Prob. 2QPCh. 9 - Prob. 3QPCh. 9 - Prob. 4QPCh. 9 - A series of organic compounds called the alkanes...Ch. 9 - Prob. 6QPCh. 9 - Prob. 7QPCh. 9 - Prob. 8QPCh. 9 - Prob. 9QPCh. 9 - Prob. 10QPCh. 9 - Prob. 11QPCh. 9 - Prob. 12QPCh. 9 - Prob. 13QPCh. 9 - Prob. 14QPCh. 9 - Prob. 15QPCh. 9 - Prob. 16QPCh. 9 - Prob. 17QPCh. 9 - Prob. 18QPCh. 9 - Prob. 19QPCh. 9 - Prob. 20QPCh. 9 - Prob. 21QPCh. 9 - Prob. 22QPCh. 9 - Prob. 23QPCh. 9 - Prob. 24QPCh. 9 - Prob. 25QPCh. 9 - Prob. 26QPCh. 9 - Prob. 27QPCh. 9 - Prob. 28QPCh. 9 - Prob. 29QPCh. 9 - Prob. 30QPCh. 9 - Prob. 31QPCh. 9 - Prob. 32QPCh. 9 - Prob. 33QPCh. 9 - Prob. 34QPCh. 9 - Prob. 35QPCh. 9 - Prob. 36QPCh. 9 - Prob. 37QPCh. 9 - Prob. 38QPCh. 9 - Prob. 39QPCh. 9 - Prob. 40QPCh. 9 - Prob. 41QPCh. 9 - Prob. 42QPCh. 9 - Prob. 43QPCh. 9 - Prob. 44QPCh. 9 - Prob. 45QPCh. 9 - Prob. 46QPCh. 9 - Prob. 47QPCh. 9 - Prob. 48QPCh. 9 - Prob. 49QPCh. 9 - Prob. 50QPCh. 9 - Prob. 51QPCh. 9 - Prob. 52QPCh. 9 - Prob. 53QPCh. 9 - Prob. 54QPCh. 9 - Prob. 55QPCh. 9 - Prob. 56QPCh. 9 - Prob. 57QPCh. 9 - Prob. 58QPCh. 9 - Prob. 59QPCh. 9 - Prob. 60QPCh. 9 - Prob. 61QPCh. 9 - Prob. 62QPCh. 9 - Prob. 63QPCh. 9 - Prob. 64QPCh. 9 - Prob. 65QPCh. 9 - Prob. 66QPCh. 9 - Prob. 67QPCh. 9 - Prob. 68QPCh. 9 - Prob. 69QPCh. 9 - Prob. 70QPCh. 9 - Prob. 71QPCh. 9 - Prob. 72QPCh. 9 - Prob. 73QPCh. 9 - Prob. 74QPCh. 9 - Prob. 75QPCh. 9 - Prob. 76QPCh. 9 - Prob. 77QPCh. 9 - Prob. 78QPCh. 9 - Prob. 79QPCh. 9 - Prob. 80QPCh. 9 - Prob. 81QPCh. 9 - Prob. 82QPCh. 9 - Prob. 83QPCh. 9 - Prob. 84QPCh. 9 - Prob. 85QPCh. 9 - Prob. 86QPCh. 9 - Prob. 87QPCh. 9 - Prob. 88QPCh. 9 - Prob. 89QPCh. 9 - Prob. 90QPCh. 9 - Prob. 91QPCh. 9 - Prob. 92QPCh. 9 - Prob. 93QPCh. 9 - Prob. 94QPCh. 9 - Prob. 95QPCh. 9 - Prob. 96QPCh. 9 - Prob. 97QPCh. 9 - Prob. 98QPCh. 9 - Prob. 99QPCh. 9 - Prob. 100QPCh. 9 - Prob. 101QPCh. 9 - Prob. 102QPCh. 9 - Prob. 103QPCh. 9 - Prob. 104QPCh. 9 - Prob. 105QPCh. 9 - Prob. 106QPCh. 9 - Prob. 107QPCh. 9 - Prob. 108QPCh. 9 - Prob. 109QPCh. 9 - Prob. 110QPCh. 9 - Prob. 111QPCh. 9 - Prob. 112QPCh. 9 - Prob. 113QPCh. 9 - Prob. 114QPCh. 9 - Prob. 115QPCh. 9 - Prob. 116QPCh. 9 - Prob. 117QPCh. 9 - Prob. 118QPCh. 9 - Prob. 119QPCh. 9 - Prob. 120QPCh. 9 - Prob. 121QPCh. 9 - Prob. 122QPCh. 9 - Prob. 123QPCh. 9 - Prob. 124QPCh. 9 - Prob. 125QPCh. 9 - Prob. 126QPCh. 9 - Prob. 127QPCh. 9 - Prob. 128QPCh. 9 - Prob. 129QPCh. 9 - Prob. 130QPCh. 9 - Prob. 131QPCh. 9 - Prob. 132QPCh. 9 - Prob. 133QPCh. 9 - Prob. 134QPCh. 9 - Prob. 135QPCh. 9 - Prob. 136QPCh. 9 - Prob. 137QPCh. 9 - Prob. 138QPCh. 9 - Prob. 139QPCh. 9 - Prob. 140QPCh. 9 - Prob. 141QPCh. 9 - Prob. 142QPCh. 9 - Prob. 143QPCh. 9 - Prob. 144QPCh. 9 - Prob. 145QPCh. 9 - Prob. 146QPCh. 9 - Prob. 147QPCh. 9 - Prob. 148QPCh. 9 - Prob. 149QPCh. 9 - Prob. 150QPCh. 9 - Prob. 151QPCh. 9 - Prob. 152QPCh. 9 - Prob. 153QPCh. 9 - Prob. 154QPCh. 9 - Prob. 155QPCh. 9 - Prob. 156QPCh. 9 - Prob. 157QPCh. 9 - Prob. 158QPCh. 9 - Prob. 159QPCh. 9 - Prob. 160QPCh. 9 - Prob. 161QPCh. 9 - Prob. 162QPCh. 9 - Prob. 163QPCh. 9 - Prob. 164QPCh. 9 - Prob. 165QPCh. 9 - Butane burns with oxygen according to the...Ch. 9 - Prob. 167QP
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- Redraw the flowchartarrow_forwardredraw the flowchart with boxes and molecules written in themarrow_forwardPart I. a) Elucidate the structure of compound A using the following information. • mass spectrum: m+ = 102, m/2=57 312=29 • IR spectrum: 1002.5 % TRANSMITTANCE Ngg 50 40 30 20 90 80 70 60 MICRONS 5 8 9 10 12 13 14 15 16 19 1740 cm M 10 0 4000 3600 3200 2800 2400 2000 1800 1600 13 • CNMR 'H -NMR Peak 8 ppm (H) Integration multiplicity a 1.5 (3H) triplet b 1.3 1.5 (3H) triplet C 2.3 1 (2H) quartet d 4.1 1 (2H) quartet & ppm (c) 10 15 28 60 177 (C=0) b) Elucidate the structure of compound B using the following information 13C/DEPT NMR 150.9 MHz IIL 1400 WAVENUMBERS (CM-1) DEPT-90 DEPT-135 85 80 75 70 65 60 55 50 45 40 35 30 25 20 ppm 1200 1000 800 600 400arrow_forward
- • Part II. a) Elucidate The structure of compound c w/ molecular formula C10 11202 and the following data below: • IR spectra % TRANSMITTANCE 1002.5 90 80 70 60 50 40 30 20 10 0 4000 3600 3200 2800 2400 2000 1800 1600 • Information from 'HAMR MICRONS 8 9 10 11 14 15 16 19 25 1400 WAVENUMBERS (CM-1) 1200 1000 800 600 400 peak 8 ppm Integration multiplicity a 2.1 1.5 (3H) Singlet b 3.6 1 (2H) singlet с 3.8 1.5 (3H) Singlet d 6.8 1(2H) doublet 7.1 1(2H) doublet Information from 13C-nmR Normal carbon 29ppm Dept 135 Dept -90 + NO peak NO peak 50 ppm 55 ppm + NO peak 114 ppm t 126 ppm No peak NO peak 130 ppm t + 159 ppm No peak NO peak 207 ppm по реак NO peakarrow_forwardCould you redraw these and also explain how to solve them for me pleasarrow_forwardNonearrow_forward
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