Functional group present in 9-fluorenone (6) other than the aromatic rings should be identified. Concept Introduction : Column chromatography is a large scale solid-liquid adsorption chromatographic technique that can separate multi-gram amounts of mixtures. This is a preparative version of thin layer chromatography that permits separation and isolation of products by a collection of eluted fractions.

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Answer 1

Question

Chapter 6.3, Problem 15E

(a)

Interpretation Introduction

Interpretation:

Functional group present in 9-fluorenone (6) other than the aromatic rings should be identified.

Concept Introduction :

Column chromatography is a large scale solid-liquid adsorption chromatographic technique that can separate multi-gram amounts of mixtures. This is a preparative version of thin layer chromatography that permits separation and isolation of products by a collection of eluted fractions.

(b)

Interpretation Introduction

Interpretation:

More polar compounds from fluorine and 9-fluorenone should be identified and explained.

Concept Introduction :

Column chromatography is a large scale solid-liquid adsorption chromatographic technique that can separate multi-gram amounts of mixtures. This is a preparative version of thin layer chromatography that permits separation and isolation of products by a collection of eluted fractions.

(c)

Interpretation Introduction

Interpretation:

From fluorine and 9-fluorenone, first eluting compound that expects from a normal − phase column chromatography should be identified and the reason should be explained

Concept Introduction :

Column chromatography is a large scale solid-liquid adsorption chromatographic technique that can separate multi-gram amounts of mixtures. This is a preparative version of thin layer chromatography that permits separation and isolation of products by the collection of eluted fractions.

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A mixture of the two compounds shown below is dissolved in ether. Using the information given in the experiment, select all the correct statements regarding the extraction and isolation of the two compounds. lose 0000 X OH A. X can be extracted from the organic layer using sodium hydroxide. B. Y can precipitate out of the aqueous layer by the addition of sodium hydroxide to the salt of Y. C. X can precipitate out of the aqueous layer by the addition of sodium hydroxide to the salt of X. D. Y can be extracted from the organic layer using sodium hydroxide.

Please help me with this, I am trying to prepare for my final exam next week and I am just completely lost

1. What effect will the following factors have on a chromatographic separation? (a) Too strong an adsorbent (b) Collection of large elution fractions

Answer 2

Question

Chapter 6.3, Problem 15E

(a)

Interpretation Introduction

Interpretation:

Functional group present in 9-fluorenone (6) other than the aromatic rings should be identified.

Concept Introduction :

Column chromatography is a large scale solid-liquid adsorption chromatographic technique that can separate multi-gram amounts of mixtures. This is a preparative version of thin layer chromatography that permits separation and isolation of products by a collection of eluted fractions.

(b)

Interpretation Introduction

Interpretation:

More polar compounds from fluorine and 9-fluorenone should be identified and explained.

Concept Introduction :

Column chromatography is a large scale solid-liquid adsorption chromatographic technique that can separate multi-gram amounts of mixtures. This is a preparative version of thin layer chromatography that permits separation and isolation of products by a collection of eluted fractions.

(c)

Interpretation Introduction

Interpretation:

From fluorine and 9-fluorenone, first eluting compound that expects from a normal − phase column chromatography should be identified and the reason should be explained

Concept Introduction :

Column chromatography is a large scale solid-liquid adsorption chromatographic technique that can separate multi-gram amounts of mixtures. This is a preparative version of thin layer chromatography that permits separation and isolation of products by the collection of eluted fractions.

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Answer 3

Question

Chapter 6.3, Problem 15E

(a)

Interpretation Introduction

Interpretation:

Functional group present in 9-fluorenone (6) other than the aromatic rings should be identified.

Concept Introduction :

Column chromatography is a large scale solid-liquid adsorption chromatographic technique that can separate multi-gram amounts of mixtures. This is a preparative version of thin layer chromatography that permits separation and isolation of products by a collection of eluted fractions.

(b)

Interpretation Introduction

Interpretation:

More polar compounds from fluorine and 9-fluorenone should be identified and explained.

Concept Introduction :

Column chromatography is a large scale solid-liquid adsorption chromatographic technique that can separate multi-gram amounts of mixtures. This is a preparative version of thin layer chromatography that permits separation and isolation of products by a collection of eluted fractions.

(c)

Interpretation Introduction

Interpretation:

From fluorine and 9-fluorenone, first eluting compound that expects from a normal − phase column chromatography should be identified and the reason should be explained

Concept Introduction :

Column chromatography is a large scale solid-liquid adsorption chromatographic technique that can separate multi-gram amounts of mixtures. This is a preparative version of thin layer chromatography that permits separation and isolation of products by the collection of eluted fractions.

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Answer 4

Question

Chapter 6.3, Problem 15E

(a)

Interpretation Introduction

Interpretation:

Functional group present in 9-fluorenone (6) other than the aromatic rings should be identified.

Concept Introduction :

Column chromatography is a large scale solid-liquid adsorption chromatographic technique that can separate multi-gram amounts of mixtures. This is a preparative version of thin layer chromatography that permits separation and isolation of products by a collection of eluted fractions.

(b)

Interpretation Introduction

Interpretation:

More polar compounds from fluorine and 9-fluorenone should be identified and explained.

Concept Introduction :

Column chromatography is a large scale solid-liquid adsorption chromatographic technique that can separate multi-gram amounts of mixtures. This is a preparative version of thin layer chromatography that permits separation and isolation of products by a collection of eluted fractions.

(c)

Interpretation Introduction

Interpretation:

From fluorine and 9-fluorenone, first eluting compound that expects from a normal − phase column chromatography should be identified and the reason should be explained

Concept Introduction :

Column chromatography is a large scale solid-liquid adsorption chromatographic technique that can separate multi-gram amounts of mixtures. This is a preparative version of thin layer chromatography that permits separation and isolation of products by the collection of eluted fractions.

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Answer 5

Chapter 6.3, Problem 15E

(a)

Interpretation Introduction

Interpretation:

Functional group present in 9-fluorenone (6) other than the aromatic rings should be identified.

Concept Introduction :

Column chromatography is a large scale solid-liquid adsorption chromatographic technique that can separate multi-gram amounts of mixtures. This is a preparative version of thin layer chromatography that permits separation and isolation of products by a collection of eluted fractions.

(b)

Interpretation Introduction

Interpretation:

More polar compounds from fluorine and 9-fluorenone should be identified and explained.

Concept Introduction :

Column chromatography is a large scale solid-liquid adsorption chromatographic technique that can separate multi-gram amounts of mixtures. This is a preparative version of thin layer chromatography that permits separation and isolation of products by a collection of eluted fractions.

(c)

Interpretation Introduction

Interpretation:

From fluorine and 9-fluorenone, first eluting compound that expects from a normal − phase column chromatography should be identified and the reason should be explained

Concept Introduction :

Column chromatography is a large scale solid-liquid adsorption chromatographic technique that can separate multi-gram amounts of mixtures. This is a preparative version of thin layer chromatography that permits separation and isolation of products by the collection of eluted fractions.

Answer 6

Chapter 6.3, Problem 15E

(a)

Interpretation Introduction

Interpretation:

Functional group present in 9-fluorenone (6) other than the aromatic rings should be identified.

Concept Introduction :

Column chromatography is a large scale solid-liquid adsorption chromatographic technique that can separate multi-gram amounts of mixtures. This is a preparative version of thin layer chromatography that permits separation and isolation of products by a collection of eluted fractions.

Answer 7

Chapter 6.3, Problem 15E

(a)

Interpretation Introduction

Interpretation:

Functional group present in 9-fluorenone (6) other than the aromatic rings should be identified.

Concept Introduction :

Column chromatography is a large scale solid-liquid adsorption chromatographic technique that can separate multi-gram amounts of mixtures. This is a preparative version of thin layer chromatography that permits separation and isolation of products by a collection of eluted fractions.

Answer 8

(b)

Interpretation Introduction

Interpretation:

More polar compounds from fluorine and 9-fluorenone should be identified and explained.

Concept Introduction :

Column chromatography is a large scale solid-liquid adsorption chromatographic technique that can separate multi-gram amounts of mixtures. This is a preparative version of thin layer chromatography that permits separation and isolation of products by a collection of eluted fractions.

Answer 9

(b)

Interpretation Introduction

Interpretation:

More polar compounds from fluorine and 9-fluorenone should be identified and explained.

Concept Introduction :

Column chromatography is a large scale solid-liquid adsorption chromatographic technique that can separate multi-gram amounts of mixtures. This is a preparative version of thin layer chromatography that permits separation and isolation of products by a collection of eluted fractions.

Answer 10

(c)

Interpretation Introduction

Interpretation:

From fluorine and 9-fluorenone, first eluting compound that expects from a normal − phase column chromatography should be identified and the reason should be explained

Concept Introduction :

Column chromatography is a large scale solid-liquid adsorption chromatographic technique that can separate multi-gram amounts of mixtures. This is a preparative version of thin layer chromatography that permits separation and isolation of products by the collection of eluted fractions.

Answer 11

(c)

Interpretation Introduction

Interpretation:

From fluorine and 9-fluorenone, first eluting compound that expects from a normal − phase column chromatography should be identified and the reason should be explained

Concept Introduction :

Column chromatography is a large scale solid-liquid adsorption chromatographic technique that can separate multi-gram amounts of mixtures. This is a preparative version of thin layer chromatography that permits separation and isolation of products by the collection of eluted fractions.

Answer 12

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Answer 13

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Answer 14

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Answer 15

Ch. 6.2 - Prob. 1E Ch. 6.2 - Prob. 2E Ch. 6.2 - Prob. 3E Ch. 6.2 - Prob. 4E Ch. 6.2 - Prob. 5E Ch. 6.2 - Prob. 6E Ch. 6.2 - Prob. 7E Ch. 6.2 - Prob. 8E Ch. 6.2 - Prob. 9E Ch. 6.3 - Prob. 1E

Solution Summary: The author explains that polar compounds from fluorine and 9-fluorenone should be identified and explained.

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