In a test tube with 0.3 mL of N,N-dimethylaniline, 5 mL of 10% NaOH, 0.4 mL of benzene sulfonyl chloride. Add a few drops of 4M KOH to make sure it is alkaline and use a litmus paper. Let it stand for 10 minutes. Pour 6M HCl dropwise until it acidify. Explain what happens to the mixture before and after adding HCl. If a precipitate is formed, collect it by filtration or decantation. Test for solubility of the precipitate in 3 mL of 2.5M NaOH. Heat to 50 OC. Shake the tube well for 3 minutes. Explain what happens to the mixture after adding NAOH. N-methylaniline
In a test tube with 0.3 mL of N,N-dimethylaniline, 5 mL of 10% NaOH, 0.4 mL of benzene sulfonyl chloride. Add a few drops of 4M KOH to make sure it is alkaline and use a litmus paper. Let it stand for 10 minutes. Pour 6M HCl dropwise until it acidify. Explain what happens to the mixture before and after adding HCl. If a precipitate is formed, collect it by filtration or decantation. Test for solubility of the precipitate in 3 mL of 2.5M NaOH. Heat to 50 OC. Shake the tube well for 3 minutes. Explain what happens to the mixture after adding NAOH. N-methylaniline
Chemistry
10th Edition
ISBN:9781305957404
Author:Steven S. Zumdahl, Susan A. Zumdahl, Donald J. DeCoste
Publisher:Steven S. Zumdahl, Susan A. Zumdahl, Donald J. DeCoste
Chapter1: Chemical Foundations
Section: Chapter Questions
Problem 1RQ: Define and explain the differences between the following terms. a. law and theory b. theory and...
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In a test tube with 0.3 mL of N,N-dimethylaniline, 5 mL of 10% NaOH, 0.4 mL of benzene sulfonyl chloride.
Add a few drops of 4M KOH to make sure it is alkaline and use a litmus paper. Let it stand for 10 minutes.
Pour 6M HCl dropwise until it acidify.
Explain what happens to the mixture before and after adding HCl.
If a precipitate is formed, collect it by filtration or decantation. Test for solubility of the precipitate in 3 mL of 2.5M NaOH. Heat to 50 OC. Shake the tube well for 3 minutes.
Explain what happens to the mixture after adding NAOH.
N-methylaniline
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