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- Give an overview of the method of mass spectrometry and how it works.Discuss the following general steps in gravimetric analysis. Sample solution Preparation Precipitation Digestion Filtration and Washing Drying and igniting Weighing and then calculation.*(iii) The reaction of ethene with aqueous potassium manganate(VII), KMNO., produces ethane-1,2-diol, CH,OHCH,OH. Data: molar mass of ethane-1,2-diol = 62 g mol In an experiment, KMNO, containing only "O reacts with ethene. Suggest how the mass spectrum of ethane-1,2-diol data could be used to decide whether the oxygen atoms in ethane-1,2-diol came from the manganate(VII) ion, water, or a combination of the two. (2)
- 2. The solubility of aspirin in water is 1 g per 300 mL at 25 °C. Assuming that your crystallization and washing with water were done at this temperature, what weight of aspirin did you lose in the filtrate and washings? How much was your percent yield lowered by this loss?student found a bottle of unknown origin in the basement of an "CAUTION—contains С₁H₁O.” No other A old house. The bottle was labelled information was given, but inside the bottle were some white crystals. The student took the bottle to a chemistry laboratory, where she analyzed the crystals with the help of the laboratory staff. C₁2H₁6O reacted with Br₂ in CCl4 adding one mole of Br, and forming C₁₂H₁OB2₂. When a sample of C₁₂H₂O was reacted with O3 followed by Zn/H₂O, two different samples, J and K, were obtained. Compound J had a molecular formula of C.HgO₂, and its NMR is shown below. Compound K had a molecular formula of C₂H₂O, and it could be oxidized to compound L, with a molecular formula of C₂H₂O₂. The IR spectrum of L showed a very wide, strong band centred around 3000 cm*¹. The NMR spectrum of L showed only two different absorptions: a doublet (6H) at 0.9 ppm and a septet (1H) at 3.6 ppm. There was also a singlet (1H) off the scale at 11.8 ppm. students, deduce possible…(a) Using NO2(g) as an example, show with dimensional analysis that the molecular mass and molar mass of a substance are numerically equal but have different units.(b) The number of atoms of oxygen in a 0.01800-g sample of O3(g) is equal to the number of molecules in a 0.06085-g sample of CxH6. Determine the value of x. (c) Vitamin C contains carbon, hydrogen and oxygen only. It is 4.579% by mass of hydrogen. One molecule of vitamin C contains 6 oxygen atoms and 8 hydrogen atoms.Determine the molecular formula of vitamin C.
- Please can you complete answer for b an cIn 1961, scientists agreed that the atomic mass unit (amu)would be defined as the mass of an atom of 12C. Before then,it was defined as the average mass of an atom of naturally occurring oxygen (a mixture of 16O, 17O, and 18O). The current atomic mass of oxygen is 15.9994 amu. (a) Did Avogadro’snumber change after the definition of an amu changed and, if so,in what direction? (b) Did the definition of the mole change?(c) Did the mass of a mole of a substance change? (d) Before1961, was Avogadro’s number 6.021023(when considered tothree significant figures), as it is today?14. Shown below are the mass spectra (without data tables) of four molecules. (The structure of each molecule is shown on the spectrum.) Mark the [M] peak for each, and indicate the molecular weight of the molecule. Relative Intensity Relative Intensity 100 80 60 40- 20 0-mm 10 100- 80 a. 20- 115-14-5501 0-mm 10 20 b. =0 20 30 30 40 40 50 50 60 m/z 60 m/z 70 70 80 80 90 100 90 100 Relative Intensity Relative Intensity 100- 80 40 20 0 100 80 40 10 20- 15-NU-5580 15 20 25 115--555 ont 10 20 30 30 35 40 45 50 55 m/z 40 50 m/z 60 60 70 65 70 75 80 Based on the five mass spectra you have seen, describe how one might identify the [M]* peak (molecular ion peak) on the mass spectrum of an unknown compound.
- The first two steps in the industrial synthesis of nitric acid produce nitrogen dioxide from ammonia: 4 NH3(g) +50₂ (g) = 4 NO(g) + 6H₂O(g) K₁ K2 2 NO(g) + O₂(g) 2 NO₂ (g) = The net reaction is: K 4 NH3(g) +70₂ (g) 4NO₂(g) + 6H₂O(g) Write an equation that gives the overall equilibrium constant K in terms of the equilibrium constants K, and K₂. If you need to include any physical constants, be sure you use their standard symbols, which you'll find in the ALEKS Calculator. K = 0 0.0 00 09 ? olo X GExplain the advantages and disadvantages of mass spectrometry?1. Provide the chemical formula (including brackets where appropriate) or systematic name for the following compounds. (a) gold(I) hypoiodite (b) HI(aq): (f) Ca(ClO4)2·4H2O: 2. What mass (in g) of chlorine atoms are there in a sample that consists of 5e+23 molecules of molecular chlorine? INSTRUCTIONS: Report your answer to 3 significant figures in scientific notation unless stated otherwise. DO NOT include the units in your answer.
