Based on the spectra provided, draw the structure. Label each unique carbon and hydrogen with the letters A, B, C… for use in assigning NMR peaks. fill in the data table assigning peaks in each spectrum. You should assign: • All 1H NMR peaks • Significant IR peaks above 1600 cm Example of what the table should include (imagine the structure of ethanol is drawn with the CH3 hydrogens labeled as A, the CH2 hydrogens labeled as B, and the OH hydrogen labeled as C) :  hydrogen proton chemical shift  integration splitting pattern couples to.. A 1.2 3 triplet B B 3.7 2 quartet A C 2.6 1 singlet -

Chemistry
10th Edition
ISBN:9781305957404
Author:Steven S. Zumdahl, Susan A. Zumdahl, Donald J. DeCoste
Publisher:Steven S. Zumdahl, Susan A. Zumdahl, Donald J. DeCoste
Chapter1: Chemical Foundations
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Problem 1RQ: Define and explain the differences between the following terms. a. law and theory b. theory and...
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Based on the spectra provided, draw the structure. Label each unique carbon and hydrogen with the letters A, B, C… for use in assigning NMR peaks. fill in the data table assigning peaks in each spectrum. You should assign:

• All 1H NMR peaks

• Significant IR peaks above 1600 cm

Example of what the table should include (imagine the structure of ethanol is drawn with the CH3 hydrogens labeled as A, the CH2 hydrogens labeled as B, and the OH hydrogen labeled as C) : 

hydrogen proton chemical shift  integration splitting pattern couples to..
A 1.2 3 triplet B
B 3.7 2 quartet A
C 2.6 1 singlet -
Rel. Intensity
LOD
TRANSMITTANCEI
D
4000
100
80
60
40
20
0.0
10
3643 74 1993 34
3004 52 1343 79
2971 41 1243 64
2930 47 1209 46
1984 86
1164 72
1783 4
1636 86
1137 77
1081 16
3000
20
968 81
725 72
877 79
463 66
30
2000
MASS SPECTRUM
40
m/z
HAVENUMBERI-11
t
50
1500
60
1000
70
80
500
Transcribed Image Text:Rel. Intensity LOD TRANSMITTANCEI D 4000 100 80 60 40 20 0.0 10 3643 74 1993 34 3004 52 1343 79 2971 41 1243 64 2930 47 1209 46 1984 86 1164 72 1783 4 1636 86 1137 77 1081 16 3000 20 968 81 725 72 877 79 463 66 30 2000 MASS SPECTRUM 40 m/z HAVENUMBERI-11 t 50 1500 60 1000 70 80 500
CDC13
240
12
220
11
200
10
QE-300
180
9
160
8
140
7
120
6
100
5
80
4
60
3
40
2
20
1
0
0
Transcribed Image Text:CDC13 240 12 220 11 200 10 QE-300 180 9 160 8 140 7 120 6 100 5 80 4 60 3 40 2 20 1 0 0
Expert Solution
Step 1: Introduction of molecule

In the given compound three types of  1H NMR signals are present

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