please draw the molecule and label it based on the data in the sheet and use the label in the data table.

Chemistry
10th Edition
ISBN:9781305957404
Author:Steven S. Zumdahl, Susan A. Zumdahl, Donald J. DeCoste
Publisher:Steven S. Zumdahl, Susan A. Zumdahl, Donald J. DeCoste
Chapter1: Chemical Foundations
Section: Chapter Questions
Problem 1RQ: Define and explain the differences between the following terms. a. law and theory b. theory and...
icon
Related questions
Question

please draw the molecule and label it based on the data in the sheet and use the label in the data table. 

Experiment 3: Williamson Ether Synthesis (Data sheet)
Setup:
4.5 g of potassium hydroxide were dissolved in 8 mL of water in a 250 mL round-bottomed
flask
2.55 g of p-cresol were added, and the mixture is swirled
The pale-yellow mixture was brought to gentle reflux and a 6.70 mL of a 50 % aqueous
solution (g/mL) of a-chloroacetic acid drop-wise using a separatory funnel
Running the reaction:
The mixture was refluxed for 10 minutes
Product isolation:
The hot mixture was transferred to a 100 mL beaker and 10 mL cold water was added
Concentrated hydrochloric acid was added dropwise until pH<2.
The yellowish mixture was placed in an ice bath for 20 minutes
The mixture was filtered using a 5 cm a Büchner funnel using a vacuum filtration setup
The crude product was recrystallized from 30 mL hot water
After filtration, the solids were placed in a drying oven at 100 °C
Product characterization:
2.30 g of a pale white solid
М.p.: 137-140 °C
Transcribed Image Text:Experiment 3: Williamson Ether Synthesis (Data sheet) Setup: 4.5 g of potassium hydroxide were dissolved in 8 mL of water in a 250 mL round-bottomed flask 2.55 g of p-cresol were added, and the mixture is swirled The pale-yellow mixture was brought to gentle reflux and a 6.70 mL of a 50 % aqueous solution (g/mL) of a-chloroacetic acid drop-wise using a separatory funnel Running the reaction: The mixture was refluxed for 10 minutes Product isolation: The hot mixture was transferred to a 100 mL beaker and 10 mL cold water was added Concentrated hydrochloric acid was added dropwise until pH<2. The yellowish mixture was placed in an ice bath for 20 minutes The mixture was filtered using a 5 cm a Büchner funnel using a vacuum filtration setup The crude product was recrystallized from 30 mL hot water After filtration, the solids were placed in a drying oven at 100 °C Product characterization: 2.30 g of a pale white solid М.p.: 137-140 °C
NMR spectra (300 MHz, DMSO-d6) ('H-NMR lower spectrum, BC-NMR upper spectrum)
DMSO-d6
220
QE-300
240
200
180
160
140
120
100
80
60
40
20
Offset: 1.2 ppm
12
11
10
6.
Transcribed Image Text:NMR spectra (300 MHz, DMSO-d6) ('H-NMR lower spectrum, BC-NMR upper spectrum) DMSO-d6 220 QE-300 240 200 180 160 140 120 100 80 60 40 20 Offset: 1.2 ppm 12 11 10 6.
Expert Solution
trending now

Trending now

This is a popular solution!

steps

Step by step

Solved in 2 steps with 1 images

Blurred answer
Similar questions
Recommended textbooks for you
Chemistry
Chemistry
Chemistry
ISBN:
9781305957404
Author:
Steven S. Zumdahl, Susan A. Zumdahl, Donald J. DeCoste
Publisher:
Cengage Learning
Chemistry
Chemistry
Chemistry
ISBN:
9781259911156
Author:
Raymond Chang Dr., Jason Overby Professor
Publisher:
McGraw-Hill Education
Principles of Instrumental Analysis
Principles of Instrumental Analysis
Chemistry
ISBN:
9781305577213
Author:
Douglas A. Skoog, F. James Holler, Stanley R. Crouch
Publisher:
Cengage Learning
Organic Chemistry
Organic Chemistry
Chemistry
ISBN:
9780078021558
Author:
Janice Gorzynski Smith Dr.
Publisher:
McGraw-Hill Education
Chemistry: Principles and Reactions
Chemistry: Principles and Reactions
Chemistry
ISBN:
9781305079373
Author:
William L. Masterton, Cecile N. Hurley
Publisher:
Cengage Learning
Elementary Principles of Chemical Processes, Bind…
Elementary Principles of Chemical Processes, Bind…
Chemistry
ISBN:
9781118431221
Author:
Richard M. Felder, Ronald W. Rousseau, Lisa G. Bullard
Publisher:
WILEY