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- In the technique of high performance liquid chromatography (HPLC) the peak area response for a particular analyte is directly proportional to concentration Analgesic tablets typically consist of aspirin and caffeine as the active ingredients, the remainder made up of inert binding material. The concentrations of aspirin and caffeine may be routinely monitored using HPLC, whereby the peak areas obtained from a solution of the tablet are compared with those obtained from standard solutions of the analytes. In an analysis to determine the concentration of caffeine in such a tablet, the following data were recorded: Solutions Analysed: Tablet Sample: Mass of tablet (dissolved in 250 cm methano): 0.523 g Caffeine Standard: Mass of caffeine (diessolved in 500 cm methanol) 0.105 g HPLC results: Solution Peak Area (catfeine) 1. Tablet Sample 325 2. Caffeine Std. 865 The concentration of caffeine in the tablet (expressed as a mass (w/wl percentage) was Oa 1.89 Ob 13.4 O 3.77 Od. 267 Oe 7.54 You…49 measurements of a variable have been made, resulting in a mean of 9.491 and a population standard deviation, σ, of 1.212. Indicate whether any of the following values can be rejected using the 2sm criterion: 9.357; 9.399; 9.577; 9.605?(A). Yes, 9.357 and 9.605 can be rejected(B). Yes, 9.357 can be rejected(C). Yes, 9.605 can be rejected(D). No, none should be rejectedIn a survey of 1000 large corporations, 250 said that, given a choice between a job candidate who smokes and an equally qualified nonsmoker, the nonsmoker would get the job (USA Today).(a) Let p represent the proportion of all corporations preferring a nonsmoking candidate. Find a point estimate for p.(b) Find a 0.95 confidence interval for p.(c) As a news writer, how would you report the survey results regarding the proportion of corporations that hire the equally qualified nonsmoker? What is the margin of error based on a 95% confidence interval?
- A chemist obtained the following data for percent lindane in the triplicate analysis of an insecticide preparation: 7.23, 6.95, and 7.53. Calculate the 95% confidence interval for the mean of the three data, assuming the following criteria. (a) the only information about the precision of the method is the precision for the three data Confidence interval = ± % lindane (b) on the basis of long experience with the method, it is believed that s --> o = 0.26% lindane Confidence interval = ± % lindaneQuestion: Using a method for the determination of % CaO in limestone the following results were obtained for a NIST Certified Reference Sample (CRM): % Cao 50.38, 50.20, 50.31, 50.22 50.41 Five samples were obtained from a railcar of limestone. The analysis of the samples gave the following results: % CaO 55.01, 59.61, 58.82, 64.39, 62.49 a) Determine the variance due to sampling. b) If the samples taken from the railcar had a mass of 0.500 g, what mass5
- Calculate the mean and 90% confidence interval for the data set. Sample Value 1 8.0626 8.0650 3 8.0583 4 8.0564 8.0571 6. 8.0600 mean: étv A A hulu 2. 5.A titrimetric method for the determination of calcium in limestone was tested by analysis of an NIST limestone containing 30.15% CaO. The mean result of four analyses was 30.26% CaO, with a standard deviation of 0.085%. By pooling data from several analyses, it was established that s = 0.094% CaO.a. Do the data indicate the presence of a systematic error at the 95% confidence level?b. Do the data indicate the presence of systematic error at the 95% confidence level if no pooled value for s was available?Icalate Hi BeHot)+6el2( +2Bels() +oHel(②) using Hess Law Bel310+3H2O→H2B/23(g) +3=-122.5K) B2H6(+6H2O(P)→2HB+6H2(火) →トニ-4734人) Male B₂ HO H2(+244145) Siven +3HP Im Belz
