100 80 60 40 20 3373 3025 IR Spectrum (liquid film) 4000 3000 2000 1600 1200 800 v (cm) % of base peak 30 45 M 149 91 104 Mass Spectrum C10H15N 40 80 120 160 200 240 280 m/e 13C NMR Spectrum (100 MHz, CDC, solution) expansion DEPT CH: CH3CH ↑ 128 127 126 proton decoupled expansion 128 127 126. Problem 162 solvent 200 160 120 80 40 0 8 (ppm) 1H NMR Spectrum (400 MHz, CDCl solution) expansion expansions 7.3 7.2 7.1 2.7 2.6 2.5 1.7 1.6 1.5 1.4 1.3 10 9 8 7 6 5 4 3 2 1 exchanges with D₂O TMS 0 8 (ppm)

100 80 60 40 20 3373 3025 IR Spectrum (liquid film) 4000 3000 2000 1600 1200 800 v (cm) % of base peak 30 45 M 149 91 104 Mass Spectrum C10H15N 40 80 120 160 200 240 280 m/e 13C NMR Spectrum (100 MHz, CDC, solution) expansion DEPT CH: CH3CH ↑ 128 127 126 proton decoupled expansion 128 127 126. Problem 162 solvent 200 160 120 80 40 0 8 (ppm) 1H NMR Spectrum (400 MHz, CDCl solution) expansion expansions 7.3 7.2 7.1 2.7 2.6 2.5 1.7 1.6 1.5 1.4 1.3 10 9 8 7 6 5 4 3 2 1 exchanges with D₂O TMS 0 8 (ppm)

Principles of Instrumental Analysis

7th Edition

ISBN:9781305577213

Author:Douglas A. Skoog, F. James Holler, Stanley R. Crouch

Publisher:Douglas A. Skoog, F. James Holler, Stanley R. Crouch

Chapter9: Atomic Absorption And Atomic Fluorescence Spectrometry

Section: Chapter Questions

Problem 9.8QAP

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