35- 40 40- 45- 2980.65 4000 3500 3000 2500 2000 1500 1000 500 Wavenumbers (cm-1) 00 50- 55 59 %Transmittance 99 60 99 65- 2889.03 88 80- 95 85- 3657.47 3854.47 3752.13 1496.34 1473.06 1382.11 1135.85 1452.27 1251.24 1072.73 955.08 00 90- 2045.26 1030.49 811.05 762.19 689.35 626.06 596.85 550.97 500.48 480.70 455.36 426.77 417.04 407.47 Tue Oct 22 16:14:00 2024 (GMT-04:00) 10 8 10.5644 Figure 2. 1H NMR spectrum in CDCl3 of meso-stilbene dibromide. 2.0000 3.7702 Figure 1. 1H NMR spectrum in CDCl3 of d/-stilbene dibromide, 8 5.0-8.0 ppm region. 6 4 2 0 [ppm] .2598 5.4826 (1R, 2R)-1,2-dibromo-1,2-diphenylethane 1H NMR in CDC13 with SiMed (27/09/08] 7.26 7.18 T . 7.8 7.6 7.14 7.2 7.0 6.8 6.6 6.1 6.2 6.0 5.8 5.6 5.4 ppm 4.5599 -0.0005 enantiomer -5.48

35- 40 40- 45- 2980.65 4000 3500 3000 2500 2000 1500 1000 500 Wavenumbers (cm-1) 00 50- 55 59 %Transmittance 99 60 99 65- 2889.03 88 80- 95 85- 3657.47 3854.47 3752.13 1496.34 1473.06 1382.11 1135.85 1452.27 1251.24 1072.73 955.08 00 90- 2045.26 1030.49 811.05 762.19 689.35 626.06 596.85 550.97 500.48 480.70 455.36 426.77 417.04 407.47 Tue Oct 22 16:14:00 2024 (GMT-04:00) 10 8 10.5644 Figure 2. 1H NMR spectrum in CDCl3 of meso-stilbene dibromide. 2.0000 3.7702 Figure 1. 1H NMR spectrum in CDCl3 of d/-stilbene dibromide, 8 5.0-8.0 ppm region. 6 4 2 0 [ppm] .2598 5.4826 (1R, 2R)-1,2-dibromo-1,2-diphenylethane 1H NMR in CDC13 with SiMed (27/09/08] 7.26 7.18 T . 7.8 7.6 7.14 7.2 7.0 6.8 6.6 6.1 6.2 6.0 5.8 5.6 5.4 ppm 4.5599 -0.0005 enantiomer -5.48

Macroscale and Microscale Organic Experiments

7th Edition

ISBN:9781305577190

Author:Kenneth L. Williamson, Katherine M. Masters

Publisher:Kenneth L. Williamson, Katherine M. Masters

Chapter45: Synthesis And Bioassay Of Sulfanilamide And Derivatives

Section: Chapter Questions

Problem 5Q

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