. Answer true or false for each statement: a) A TLC analysis is sufficient to characterize the purity of a compound. b) Carboxylic acids containing six or more carbon atoms per molecule are more soluble in 2.5 M sodium hydroxide than in diethyl ether. c) Phenols containing six or more carbon atoms per molecule are more soluble in 2.5 M sodium hydroxide than in diethyl ether. d) Benzoic acid and p-nitroaniline form water-soluble salts, whereas naphthalene does not. e) TLC analysis is the method of choice to determine the type of solid phase and eluent system that is required for a column chromatography separation. f) Mineral oil is an inappropriate heating fluid for determining the boiling points of samples that exceed 200 °C (760 torr)? g) A heating bath containing mineral oil should not be used to determine the melting points of solids melting above 200 °C

EBK A SMALL SCALE APPROACH TO ORGANIC L
4th Edition
ISBN:9781305446021
Author:Lampman
Publisher:Lampman
Chapter5: Chromatography
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1. Answer true or false for each statement:

a) A TLC analysis is sufficient to characterize the purity of a compound.

b) Carboxylic acids containing six or more carbon atoms per molecule are more soluble in
2.5 M sodium hydroxide than in diethyl ether.

c) Phenols containing six or more carbon atoms per molecule are more soluble in 2.5 M sodium hydroxide
than in diethyl ether.

d) Benzoic acid and p-nitroaniline form water-soluble salts, whereas naphthalene does not.

e) TLC analysis is the method of choice to determine the type of solid phase and eluent system that is required for a column chromatography separation.

f) Mineral oil is an inappropriate heating fluid for determining the boiling points of samples that exceed 200
°C (760 torr)?

g) A heating bath containing mineral oil should not be used to determine the melting points of solids melting
above 200 °C

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