120L Ex2 Identification of a solid acid report sheets - CHEM 120L - Spring 2022

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School

University of Waterloo *

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Course

120L

Subject

Chemistry

Date

May 24, 2024

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pdf

Pages

4

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Report
Experiment 2: Identification of an Unknown Solid Acid Post-lab Report Sheets Name: Student ID #: Submission date: TA: Partner: Experimental objectives: * To gain experience in the techniques of weighing by difference, quantitative transfer and standardization titrations * To prepare a primary standard solution, use this solution to determine the concentration of a sodium hydroxide standard * To use an NaOH standard to titrate against an unknown solid acid in order to determine the molar mass and thus identity of the unknown from the set of possible unknowns * To develop skill in the use of unit analysis for calculations Results Part A: NOTE: Marks are deducted each time 1-2 line unit analysis is not used AND each time significant figures are incorrect. Use care in all calculations! Mass of oxalic acid used: Sample calculation for determining the concentration of oxalic acid, using unit analysis: Concentration of oxalic acid:
Sample calculation for determining the concentration of NaOH, using unit analysis: Titration Volume of oxalic acid Volume of NaOH Concentration of NaOH # (mL) (mL) ™) 1 2 3 Average Concentration of NaOH from Part A: Results Part B: Unknown #: Titration # Mass of Unknown (8) Volume of NaOH (mL)
Sample calculation of unknown molar mass assuming the acid is monoprotic, using unit analysis: Sample calculation of unknown molar mass assuming the acid is diprotic, using unit analysis: Sample calculation of unknown molar mass assuming the acid is triprotic, using unit analysis: Sample calculation for determination of the average molar mass:
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Molar Mass Sample Monoprotic Diprotic Triprotic 3 Average Molar Mass: Conclusion: Write a formal lab report conclusion for this experiment and attach it as the next page in these report sheets. Refer to LEARN - Content - Lab reports for information on writing formal lab report conclusions. Maximum length for this conclusion is one page, double spaced. Be sure to summarize the results from all the experimental objectives outlined in this report and include both the identity and # of your unknown. References: If you use any resources in preparing this report, you must provide reference information for them here: Attachments to your report: * Your experimental procedure summary will be graded as part of your lab report. Attach it behind the report sheets. * Your Data Sheet must be submitted with your report as proof that you performed the experiment, attach it as the last page of your report.