Principles of Instrumental Analysis
7th Edition
ISBN: 9781305577213
Author: Douglas A. Skoog, F. James Holler, Stanley R. Crouch
Publisher: Cengage Learning
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Question
Chapter A1, Problem A1.16QAP
Interpretation Introduction
Interpretation:
In a NIST reference steel sample the certified percentage of nickel is 1.12% and the standard deviation related to this 0.03%. The determination of percentage produce for the nickel using new spectrometric method is − 1.10, 1.08, 1.09, 1.12 and 1.09. The indication of the bias in the method at the 95% level is to be determined.
Concept introduction:
The formula that will be used-
Here,
N = degree of freedom
s = standard deviation
t = constant
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In the Thermo Fisher application note about wine analysis (Lesson 3), the following
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MAU
300
200
T
34
5
100-
1 2
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6
7
8
9
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2.6
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3.0 3.2 3.4
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4.4
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5.2
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1.04
O 1.24
The diagram shows two
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1000°C and 1400°C. State the
weight percentage of the
primary constituent (grains of
C) that would be obtained by
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1000°C
a+L
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12
α
a+C
45
1200 C
L+y
140096
C+Y
a+ß
800°C
700°C
C+B
96
92
a+B
0
10
20
30
40
50
60
70 80 90 100
A
% peso B
B
8.
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protons.
2
4
3
ō (ppm)
OH
4
6 6
СОН
2
1
0
Chapter A1 Solutions
Principles of Instrumental Analysis
Ch. A1 - Prob. A1.1QAPCh. A1 - Prob. A1.2QAPCh. A1 - Prob. A1.3QAPCh. A1 - Prob. A1.4QAPCh. A1 - Prob. A1.5QAPCh. A1 - Prob. A1.6QAPCh. A1 - Prob. A1.7QAPCh. A1 - Prob. A1.8QAPCh. A1 - Prob. A1.9QAPCh. A1 - Prob. A1.10QAP
Ch. A1 - Prob. A1.11QAPCh. A1 - Prob. A1.12QAPCh. A1 - Prob. A1.13QAPCh. A1 - Prob. A1.14QAPCh. A1 - Prob. A1.15QAPCh. A1 - Prob. A1.16QAPCh. A1 - Prob. A1.17QAPCh. A1 - Prob. A1.18QAPCh. A1 - Prob. A1.19QAPCh. A1 - Prob. A1.20QAPCh. A1 - Prob. A1.21QAPCh. A1 - Prob. A1.22QAPCh. A1 - Prob. A1.23QAPCh. A1 - Prob. A1.24QAP
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