(a) Interpretation: The synthesis route for the preparation of 2- bromobenzoic acid from o- toluidine ( o- methylaniline) is to be drawn. Concept introduction: The formation of diazonium salt from aromatic amines takes place using sodium nitrite and hydrochloric acid at low temperatures. This process is known as diazotization. The diazonium salts can be converted to aryl halides using copper halides or aryl cyanides using copper cyanides

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Answer 1

Question

Chapter 23, Problem 23.29P

Interpretation Introduction

(a)

Interpretation:

The synthesis route for the preparation of 2- bromobenzoic acid from o-toluidine (o-methylaniline) is to be drawn.

Concept introduction:

The formation of diazonium salt from aromatic amines takes place using sodium nitrite and hydrochloric acid at low temperatures. This process is known as diazotization. The diazonium salts can be converted to aryl halides using copper halides or aryl cyanides using copper cyanides

Interpretation Introduction

(b)

Interpretation:

The synthesis route for the preparation of 2, 4, 6- tribromobenzoic acid from aniline is to be drawn.

Concept introduction:

The formation of diazonium salt from aromatic amines takes place using sodium nitrite and hydrochloric acid at low temperatures. This process is known as diazotization. The diazonium salts can be converted to aryl halides using copper halides or aryl cyanides using copper cyanides

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Transmitance 3. Which one of the following compounds corresponds to this IR spectrum? Point out the absorption band(s) that helped you decide. OH H3C OH H₂C CH3 H3C CH3 H3C INFRARED SPECTRUM 0.8- 0.6 0.4- 0.2 3000 2000 1000 Wavenumber (cm-1) 4. Consider this compound: H3C On the structure above, label the different types of H's as A, B, C, etc. In table form, list the labeled signals, and for each one state the number of hydrogens, their shifts, and the splitting you would observe for these hydrogens in the ¹H NMR spectrum. Label # of hydrogens splitting Shift (2)

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Answer 2

Question

Chapter 23, Problem 23.29P

Interpretation Introduction

(a)

Interpretation:

The synthesis route for the preparation of 2- bromobenzoic acid from o-toluidine (o-methylaniline) is to be drawn.

Concept introduction:

The formation of diazonium salt from aromatic amines takes place using sodium nitrite and hydrochloric acid at low temperatures. This process is known as diazotization. The diazonium salts can be converted to aryl halides using copper halides or aryl cyanides using copper cyanides

Interpretation Introduction

(b)

Interpretation:

The synthesis route for the preparation of 2, 4, 6- tribromobenzoic acid from aniline is to be drawn.

Concept introduction:

The formation of diazonium salt from aromatic amines takes place using sodium nitrite and hydrochloric acid at low temperatures. This process is known as diazotization. The diazonium salts can be converted to aryl halides using copper halides or aryl cyanides using copper cyanides

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Answer 3

Question

Chapter 23, Problem 23.29P

Interpretation Introduction

(a)

Interpretation:

The synthesis route for the preparation of 2- bromobenzoic acid from o-toluidine (o-methylaniline) is to be drawn.

Concept introduction:

The formation of diazonium salt from aromatic amines takes place using sodium nitrite and hydrochloric acid at low temperatures. This process is known as diazotization. The diazonium salts can be converted to aryl halides using copper halides or aryl cyanides using copper cyanides

Interpretation Introduction

(b)

Interpretation:

The synthesis route for the preparation of 2, 4, 6- tribromobenzoic acid from aniline is to be drawn.

Concept introduction:

The formation of diazonium salt from aromatic amines takes place using sodium nitrite and hydrochloric acid at low temperatures. This process is known as diazotization. The diazonium salts can be converted to aryl halides using copper halides or aryl cyanides using copper cyanides

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Answer 4

Question

Chapter 23, Problem 23.29P

Interpretation Introduction

(a)

Interpretation:

The synthesis route for the preparation of 2- bromobenzoic acid from o-toluidine (o-methylaniline) is to be drawn.

Concept introduction:

The formation of diazonium salt from aromatic amines takes place using sodium nitrite and hydrochloric acid at low temperatures. This process is known as diazotization. The diazonium salts can be converted to aryl halides using copper halides or aryl cyanides using copper cyanides

Interpretation Introduction

(b)

Interpretation:

The synthesis route for the preparation of 2, 4, 6- tribromobenzoic acid from aniline is to be drawn.

Concept introduction:

The formation of diazonium salt from aromatic amines takes place using sodium nitrite and hydrochloric acid at low temperatures. This process is known as diazotization. The diazonium salts can be converted to aryl halides using copper halides or aryl cyanides using copper cyanides

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Answer 5

Chapter 23, Problem 23.29P

Interpretation Introduction

(a)

Interpretation:

The synthesis route for the preparation of 2- bromobenzoic acid from o-toluidine (o-methylaniline) is to be drawn.

Concept introduction:

The formation of diazonium salt from aromatic amines takes place using sodium nitrite and hydrochloric acid at low temperatures. This process is known as diazotization. The diazonium salts can be converted to aryl halides using copper halides or aryl cyanides using copper cyanides

Interpretation Introduction

(b)

Interpretation:

The synthesis route for the preparation of 2, 4, 6- tribromobenzoic acid from aniline is to be drawn.

Concept introduction:

The formation of diazonium salt from aromatic amines takes place using sodium nitrite and hydrochloric acid at low temperatures. This process is known as diazotization. The diazonium salts can be converted to aryl halides using copper halides or aryl cyanides using copper cyanides

Answer 6

Chapter 23, Problem 23.29P

Interpretation Introduction

(a)

Interpretation:

The synthesis route for the preparation of 2- bromobenzoic acid from o-toluidine (o-methylaniline) is to be drawn.

Concept introduction:

The formation of diazonium salt from aromatic amines takes place using sodium nitrite and hydrochloric acid at low temperatures. This process is known as diazotization. The diazonium salts can be converted to aryl halides using copper halides or aryl cyanides using copper cyanides

Answer 7

Chapter 23, Problem 23.29P

Interpretation Introduction

(a)

Interpretation:

The synthesis route for the preparation of 2- bromobenzoic acid from o-toluidine (o-methylaniline) is to be drawn.

Concept introduction:

The formation of diazonium salt from aromatic amines takes place using sodium nitrite and hydrochloric acid at low temperatures. This process is known as diazotization. The diazonium salts can be converted to aryl halides using copper halides or aryl cyanides using copper cyanides

Answer 8

Interpretation Introduction

(b)

Interpretation:

The synthesis route for the preparation of 2, 4, 6- tribromobenzoic acid from aniline is to be drawn.

Concept introduction:

The formation of diazonium salt from aromatic amines takes place using sodium nitrite and hydrochloric acid at low temperatures. This process is known as diazotization. The diazonium salts can be converted to aryl halides using copper halides or aryl cyanides using copper cyanides

Answer 9

Interpretation Introduction

(b)

Interpretation:

The synthesis route for the preparation of 2, 4, 6- tribromobenzoic acid from aniline is to be drawn.

Concept introduction:

The formation of diazonium salt from aromatic amines takes place using sodium nitrite and hydrochloric acid at low temperatures. This process is known as diazotization. The diazonium salts can be converted to aryl halides using copper halides or aryl cyanides using copper cyanides

Answer 10

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Answer 11

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Answer 12

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Answer 13

Ch. 23 - Prob. 23.1P Ch. 23 - Prob. 23.2P Ch. 23 - Prob. 23.3P Ch. 23 - Prob. 23.4P Ch. 23 - Prob. 23.5P Ch. 23 - Prob. 23.6P Ch. 23 - Prob. 23.7P Ch. 23 - Prob. 23.8P Ch. 23 - Prob. 23.9P Ch. 23 - Prob. 23.10P

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Chapter 23 Solutions