Principles of Instrumental Analysis, 6th Edition
6th Edition
ISBN: 9788131525579
Author: Douglas A. Skoog, F. James Holler, Stanley R. Crouch
Publisher: Cenage Learning
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Question
Chapter 19, Problem 19.9QAP
Interpretation Introduction
(a)
Interpretation:
The frequency difference at 4.69 T should be predicted.
Concept introduction:
Nuclear magnetic resonance is a technique that is used to predict the structural formula of the compound. NMR spectroscopy involves the examination of the nucleus under the external magnetic field.
Interpretation Introduction
(b)
Interpretation:
The frequency difference at 7.05 T should be predicted.
Concept introduction:
Nuclear magnetic resonance is a technique that is used to predict the structural formula of the compound. NMR spectroscopy involves the examination of the nucleus under the external magnetic field.
Interpretation Introduction
(c)
Interpretation:
The frequency difference at 18.8 T should be predicted. v
Concept introduction:
Nuclear magnetic resonance is a technique that is used to predict the structural formula of the compound. NMR spectroscopy involves the examination of the nucleus under the external magnetic field.
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4. (2 pts) Draw the structure of the major component of the Limonene isolated. Explain how
you confirmed the structure.
5. (2 pts) Draw the fragment corresponding to the base peak in the Mass spectrum of
Limonene.
6. (1 pts) Predict the 1H NMR spectral data of R-Limonene.
Proton NMR: 5.3 pon multiplet (H Ring
Chapter 19 Solutions
Principles of Instrumental Analysis, 6th Edition
Ch. 19 - Prob. 19.1QAPCh. 19 - Prob. 19.2QAPCh. 19 - Prob. 19.3QAPCh. 19 - Prob. 19.4QAPCh. 19 - Prob. 19.5QAPCh. 19 - A nucleus has a spin quantum number of 7/2. How...Ch. 19 - Prob. 19.7QAPCh. 19 - Prob. 19.8QAPCh. 19 - Prob. 19.9QAPCh. 19 - Why is 133C-133C spin-spin splitting not observed...
Ch. 19 - Prob. 19.11QAPCh. 19 - Prob. 19.12QAPCh. 19 - Prob. 19.13QAPCh. 19 - What is a rotating frame of reference?Ch. 19 - How will E for an isolated 13C nucleus compare...Ch. 19 - Prob. 19.16QAPCh. 19 - Prob. 19.17QAPCh. 19 - Prob. 19.18QAPCh. 19 - Prob. 19.19QAPCh. 19 - Prob. 19.20QAPCh. 19 - Prob. 19.21QAPCh. 19 - Prob. 19.22QAPCh. 19 - Prob. 19.23QAPCh. 19 - Prob. 19.24QAPCh. 19 - Prob. 19.25QAPCh. 19 - Prob. 19.26QAPCh. 19 - Prob. 19.27QAPCh. 19 - Prob. 19.28QAPCh. 19 - Prob. 19.29QAPCh. 19 - Prob. 19.30QAPCh. 19 - The proton NMR spectrum in Figure 19.39 is for an...Ch. 19 - The proton NMR spectrum in Figure 19-40 is for a...Ch. 19 - Prob. 19.33QAPCh. 19 - Prob. 19.34QAPCh. 19 - Prob. 19.35QAPCh. 19 - From the proton NMR spectrum in Figure 19-44,...Ch. 19 - From the proton spectrum given in Figure 19-45,...Ch. 19 - Prob. 19.38QAPCh. 19 - Prob. 19.39QAPCh. 19 - Prob. 19.40QAPCh. 19 - Prob. 19.41QAPCh. 19 - Prob. 19.42QAP
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