It should be identified for the unprepared compounds by using the Heck reaction. Concept introduction: Suzuki reaction: A reaction that couples an aryl halide or vinyl halide with an Organoboron reagent . Heck reaction: A reaction that breaks the double bond of an alkene and then joins the fragments .

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Answer 1

Question

Chapter 11, Problem 42P

(a)

Interpretation Introduction

Interpretation:

It should be identified for the unprepared compounds by using the Heck reaction.

Concept introduction:

Suzuki reaction:

A reaction that couples an aryl halide or vinyl halide with an Organoboron reagent.

Heck reaction:

A reaction that breaks the double bond of an alkene and then joins the fragments.

(b)

Interpretation Introduction

Interpretation:

The starting material and the suitable compound should be identified which can be prepared from Heck reaction.

Concept introduction:

Suzuki reaction:

A reaction that couples an aryl halide or vinyl halide with an Organoboron reagent.

Heck reaction:

A reaction that breaks the double bond of an alkene and then joins the fragments.

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5. Use the MS data to answer the questions on the next page. 14.0 1.4 15.0 8.1 100- MS-IW-5644 26.0 2.8 27.0 6.7 28.0 1.8 29.0 80 4.4 38.0 1.0 39.0 1.5 41.0 1.2 42.0 11.2 43.0 100.0 44.0 4.3 79.0 1.9 80.0 2.6 Relative Intensity 40 81.0 1.9 82.0 2.5 93.0 8.7 20- 95.0 8.2 121.0 2.0 123.0 2.0 136.0 11.8 0 138.0 11.5 20 40 8. 60 a. Br - 0 80 100 120 140 160 180 200 220 m/z Identify the m/z of the base peak and molecular ion. 2 b. Draw structures for each of the following fragments (include electrons and charges): 43.0, 93.0, 95.0, 136.0, and 138.0 m/z. C. Draw a reasonable a-fragmentation mechanism for the fragmentation of the molecular ion to fragment 43.0 m/z. Be sure to include all electrons and formal charges. 6. Using the values provided in Appendix E of your lab manual, calculate the monoisotopic mass for the pyridinium ion (CsH6N) and show your work.

Answer 2

Question

Chapter 11, Problem 42P

(a)

Interpretation Introduction

Interpretation:

It should be identified for the unprepared compounds by using the Heck reaction.

Concept introduction:

Suzuki reaction:

A reaction that couples an aryl halide or vinyl halide with an Organoboron reagent.

Heck reaction:

A reaction that breaks the double bond of an alkene and then joins the fragments.

(b)

Interpretation Introduction

Interpretation:

The starting material and the suitable compound should be identified which can be prepared from Heck reaction.

Concept introduction:

Suzuki reaction:

A reaction that couples an aryl halide or vinyl halide with an Organoboron reagent.

Heck reaction:

A reaction that breaks the double bond of an alkene and then joins the fragments.

Expert Solution & Answer

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Answer 3

Question

Chapter 11, Problem 42P

(a)

Interpretation Introduction

Interpretation:

It should be identified for the unprepared compounds by using the Heck reaction.

Concept introduction:

Suzuki reaction:

A reaction that couples an aryl halide or vinyl halide with an Organoboron reagent.

Heck reaction:

A reaction that breaks the double bond of an alkene and then joins the fragments.

(b)

Interpretation Introduction

Interpretation:

The starting material and the suitable compound should be identified which can be prepared from Heck reaction.

Concept introduction:

Suzuki reaction:

A reaction that couples an aryl halide or vinyl halide with an Organoboron reagent.

Heck reaction:

A reaction that breaks the double bond of an alkene and then joins the fragments.

Expert Solution & Answer

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See solution

Answer 4

Question

Chapter 11, Problem 42P

(a)

Interpretation Introduction

Interpretation:

It should be identified for the unprepared compounds by using the Heck reaction.

Concept introduction:

Suzuki reaction:

A reaction that couples an aryl halide or vinyl halide with an Organoboron reagent.

Heck reaction:

A reaction that breaks the double bond of an alkene and then joins the fragments.

(b)

Interpretation Introduction

Interpretation:

The starting material and the suitable compound should be identified which can be prepared from Heck reaction.

Concept introduction:

Suzuki reaction:

A reaction that couples an aryl halide or vinyl halide with an Organoboron reagent.

Heck reaction:

A reaction that breaks the double bond of an alkene and then joins the fragments.

Expert Solution & Answer

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Answer 5

Chapter 11, Problem 42P

(a)

Interpretation Introduction

Interpretation:

It should be identified for the unprepared compounds by using the Heck reaction.

Concept introduction:

Suzuki reaction:

A reaction that couples an aryl halide or vinyl halide with an Organoboron reagent.

Heck reaction:

A reaction that breaks the double bond of an alkene and then joins the fragments.

(b)

Interpretation Introduction

Interpretation:

The starting material and the suitable compound should be identified which can be prepared from Heck reaction.

Concept introduction:

Suzuki reaction:

A reaction that couples an aryl halide or vinyl halide with an Organoboron reagent.

Heck reaction:

A reaction that breaks the double bond of an alkene and then joins the fragments.

Answer 6

Chapter 11, Problem 42P

(a)

Interpretation Introduction

Interpretation:

It should be identified for the unprepared compounds by using the Heck reaction.

Concept introduction:

Suzuki reaction:

A reaction that couples an aryl halide or vinyl halide with an Organoboron reagent.

Heck reaction:

A reaction that breaks the double bond of an alkene and then joins the fragments.

Answer 7

Chapter 11, Problem 42P

(a)

Interpretation Introduction

Interpretation:

It should be identified for the unprepared compounds by using the Heck reaction.

Concept introduction:

Suzuki reaction:

A reaction that couples an aryl halide or vinyl halide with an Organoboron reagent.

Heck reaction:

A reaction that breaks the double bond of an alkene and then joins the fragments.

Answer 8

(b)

Interpretation Introduction

Interpretation:

The starting material and the suitable compound should be identified which can be prepared from Heck reaction.

Concept introduction:

Suzuki reaction:

A reaction that couples an aryl halide or vinyl halide with an Organoboron reagent.

Heck reaction:

A reaction that breaks the double bond of an alkene and then joins the fragments.

Answer 9

(b)

Interpretation Introduction

Interpretation:

The starting material and the suitable compound should be identified which can be prepared from Heck reaction.

Concept introduction:

Suzuki reaction:

A reaction that couples an aryl halide or vinyl halide with an Organoboron reagent.

Heck reaction:

A reaction that breaks the double bond of an alkene and then joins the fragments.

Answer 10

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Answer 11

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Answer 12

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Answer 13

Ch. 11.1 - Prob. 1P Ch. 11.2 - Which is more reactive an organolithium compound...Ch. 11.2 - Prob. 3P Ch. 11.3 - Muscalure is the sex attractant of the common...Ch. 11.3 - Prob. 7P Ch. 11.3 - Prob. 8P Ch. 11.3 - Prob. 9P Ch. 11.3 - Prob. 10P Ch. 11.4 - Prob. 13P Ch. 11.4 - Prob. 14P

Solution Summary: The author explains that Suzuki reaction couples an aryl halide with an Organoboron reagent. Heck reaction breaks the double bond of an alkene and joins the fragments.

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Chapter 11 Solutions