What are replicates in Analytical Chemistry? O The component of a sample that repeats over different assays. Similar assays done to different samples A sample that contains exactly the same amount of analytes than the original sample similar samples that are analyzed at the same time and in the same way

What are replicates in Analytical Chemistry? O The component of a sample that repeats over different assays. Similar assays done to different samples A sample that contains exactly the same amount of analytes than the original sample similar samples that are analyzed at the same time and in the same way

Chemistry

10th Edition

ISBN:9781305957404

Author:Steven S. Zumdahl, Susan A. Zumdahl, Donald J. DeCoste

Publisher:Steven S. Zumdahl, Susan A. Zumdahl, Donald J. DeCoste

Chapter1: Chemical Foundations

Section: Chapter Questions

Problem 1RQ: Define and explain the differences between the following terms. a. law and theory b. theory and...

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QUESTION 16 Match the correct choices with the given. For gravimetric analysis, use this data to answer the questions. |Trial 1 0.6020 g 24.8405 g 24.8451 g 24.8422 Trial 2 0.5021 g 22.8165 g 22.8165 g Trial 3 0.5018 g 22.8169 g 22.8169 g |Weight of Sample Weight of Crucible and Ba$O, 8 24.8422 g Constant Weight of Crucible & Sample 24.8422 g 22.8165 g 22.8169 g Weight of Crucible 24.3181 22.3593 g 22.3641 g 24.3160 g 24.3142 g 24.3142 g 24.3142 g 24.3142 g 22.3523 g 22.3534 g 22.3532 g 22.3532 g 22.3612 g 22.3605 g 22.3605 g 22.3605 g Constant Weight of Crucible 22.3532 g 22.3605 g Weight of BaSo, |% so,2- Average Standard deviation Relative standard deviation A. 2.65 Average of the % (w/w) SO42- B. to decompose the solid and form a compound of known composition and to remove the solvent and any non-volatile species Standard deviation of the % (w/w) So2- Relative standard deviation of the C. reprecipitation % (w/w) SO42- D. formation of small crystals This is a drastic but effective…
In a standardization experiment, a student titrates a 0.250g sample of pure Na,CO, with her HOa solution. This first titration required 37.94 mL of her prepared HCl solution. She then used 37.56 ml of the now-standardized acid to titrate a 0.330 g sample of impure soda ash (mostly sodium carbonate). Find the % Na CO, in the unknown Report your answer to two places past the decimal leg. 43.45).
1. Develop a detailed separation scheme for the separation and determination of the percent composition of your sample which will be a mixture of NaCl, NH.CL, and sand. You are expected to use the properties of the components listed below and some of the techniques listed in the table in the pre-lab queries (and used in Separations I). Keep in mind that any chemistry student should be able to pick up your scheme, understand it, and use it to complete the separation and calculation of % composition. Place the scheme on a separate sheet of paper. Component Solubility (@25°C) Melting Point Hardness sodium chloride, NaCl 35 g/100 mL water 801°C soft ammonium chloride, NH&Cl 37 g/100 mL water sublimes 350°C soft sand, SIQ2 insoluble 1600°C hard Example of compounds in a container. Naci NH.CI sio2 Exploring the Chemical World, PGCC, 2003 4 RESULTS Show all calculations with units in this space.
> In a typical quantitative analysis, which step is the most crucial? What part will make or break the result? Why?
Data obtained: Chips # of extractions Chips' weight (g) Fat weight (g) Regular 3 20.043 6.745 3 20.187 6.438 3 20.198 7.451 Low fat 3 19.456 3.982 3 20.072 4.547 3 20.192 4.589 Mass percent is a method of expressing the concentration of a substance in a mixture or element in a compound. It is calculated as the mass of the component divided by the total mass of the mixture and then multiplied by 100 to get the percent. The formula is: mass % of component= (mass of component / total mass) x 100% 1) Reproduce the following table, and use the data to determine the mass % of fat in the chips for each trial. 2) Show one example calculation. Chips Trial % by mass of fat Regular 1 2 3 Lowfat 1 2 3
Which of the following statements is false? * Chromatographic analysis is independent of film thickness Thick films are used with highly volatile analytes because such films retain solutes for a longer time, thus providing a greater time for separation to take place. Thin films are useful for separating species of low volatility in a reasonable length of time. Which of the following is true about a chromatogram? * The signal is plotted as a function of time or volume of the added mobile phase The position of the peak can be used to quantitatively identify the components of the sample The area under the peak provides qualitative measure of the amount of each component The following are characteristics of an ideal GC detector except-* A temperature range from room temperature to at least 400°C. A long response time independent of flow rate. Adequate sensitivity
Errors of different varieties may arise throughout the course of an experiment. Below, match the different types of errors with their corresponding definitions. Group of answer choices Errors that have an equal chance to be positive or negative. These errors will arise because it is impossible to make any measurement completely exact. Errors that will have a consistent directional bias every time the experiment is carried out. These errors tend to always be positive or negative, meaning over or underestimating, respectively, the true value of the measurement due to experimental limitations. An error that is within the direct control and/or caused by a mistake from the chemist. Options Random error Systematic error Human mistake
alculate the approximate volume of the vinegar sample needed for the analyses (Part A.1). Brand of vinegar or unknown no. Colauita tof White Wine Trial 1 1122809 Trial 2 Trial 1 Trial 2 e Guia 112.280g (12.822g 112.796 115 565 lis.9 1. Mass of flask (g) l15.603 2. Mass of flask + vinegar (g) 2.496 3.323 2,743 2,749 3. Mass of vinegar (g) B. Analysis of Vinegar Sample 2mL 7.5 23mL 32.コ 1. Buret reading of NaOH, initial (mL) 5.25mL 13ML amL 2. Buret reading of NaOH, final (mL) 33,3 31.2 1. Volume of NaOH used (mL) 2! mL a7.45 me 20.3 32.2 o i135 • 004 1 Molar concentration of NaOH (mol/L) Oi135 • 00 3 1003 , 063 5. Moles of NaOH added (mol) 6. Moles of CH,COOH in vinegar (mol) 7. Mass of CH,COOH in vinegar (g) 8. Percent by mass of CH,COOH in vinegar (%) 9. Average percent by mass of CH,COOH in vinegar (%) Calculations for Trial 1 of the first vinegar sample on next page. Experiment 10 137
Saved Normal BIIIU fxl Ix Actual mass used in solution prep (g) Volume solution prepared Measured conductivity (uS/cm) Substance 0.1 g Naci 0.1003 100 mL 1149 0.1 g Nal 0.10 100 ml 419 Calculate the mass of Nal that would be necessary to yield the same conductivity as the NaCl solution. Clearly show these calculations in your lab notebook. Saved T BII U X X + fr Normal
A student determined fluoride in a toothpaste sample using ion chromatography. A toothpaste sample of mass 0.100 g was dissolved in type I water and then quantitatively filtered through a Whatman #1 filter paper into a clean 100 ml volumetric flask. The flask was then made up to volume with type I water and mixed thoroughly.A portion of the solution was filtered through a 0.45 um filter into a sample vial for analysis. Analysis of the sample gave a fluoride concentration of 1.60 mg/l Calculate the % w/w fluoride in the original toothpaste sample. (Give your answer to 3 decimal places please)
The following volumes of 0.000300 M SCN are diluted to 15.00 mL. Determine the concentration of SCN in each sample after dilution. These values will be used during the experiment. To enter exponential values, use the format 1.0e-5. Sample 0.000300 M SCN (mL) [SCN'] (M) 1 1.50 3.50 7.00 4 10.00 3.
Now, look for the description of these techniques and identify which can separate the following mixtures. Two colorless liquids A non-dissolving solid mixed with a liquid Red and blue marbles of the same size and mass