The following data were obtained by gas-liquid chromatography using a 40.0 cm packed column: Air i. Compound Methylcyclohexane Methylcyclohexene Toluene Solve the following: V. vi. tR (min) 1.9 10.1 10.8 1. If a resolution of 1.5 was desired in resolving methylcyclohexene and toluene, calculate 13.3 How many plates would be required? Set up Stationary phase Mobile phase Result Separation Analysis time wb (min) ii. How long would the column if the same packing were employed? 0.77 0.81 1.05 2. What are the main distinctions between gas chromatography (GC) and thin layer chromatography (TLC) in terms of the basis of separation: i. ii. iii. iv.

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The following data were obtained by gas-liquid chromatography using a 40.0 cm
packed column:
i.
Air
Solve the following:
iv.
Compound
Methylcyclohexane
Methylcyclohexene
Toluene
V.
vi.
tR (min)
1.9
10.1
10.8
Set up
Stationary phase
Mobile phase
Result
13.3
1. If a resolution of 1.5 was desired in resolving methylcyclohexene and toluene,
calculate
How many plates would be required?
Separation
Analysis time
wb (min)
-
0.77
0.81
2. What are the main distinctions between gas chromatography (GC) and thin
layer chromatography (TLC) in terms of the basis of separation:
i.
ii.
1.05
How long would the column if the same packing were employed?
Transcribed Image Text:The following data were obtained by gas-liquid chromatography using a 40.0 cm packed column: i. Air Solve the following: iv. Compound Methylcyclohexane Methylcyclohexene Toluene V. vi. tR (min) 1.9 10.1 10.8 Set up Stationary phase Mobile phase Result 13.3 1. If a resolution of 1.5 was desired in resolving methylcyclohexene and toluene, calculate How many plates would be required? Separation Analysis time wb (min) - 0.77 0.81 2. What are the main distinctions between gas chromatography (GC) and thin layer chromatography (TLC) in terms of the basis of separation: i. ii. 1.05 How long would the column if the same packing were employed?
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