Step 1: Calculate the Index of Hydrogen Deficiency (IHD). Step 2: Use IR to determine obvious functional groups. Step 3: Use 1H-NMR to determine structural details. Step 4: Confirm the final structure using 13C-NMR. Find and draw the structure and give supporting data.
Step 1: Calculate the Index of Hydrogen Deficiency (IHD). Step 2: Use IR to determine obvious functional groups. Step 3: Use 1H-NMR to determine structural details. Step 4: Confirm the final structure using 13C-NMR. Find and draw the structure and give supporting data.
Chemistry
10th Edition
ISBN:9781305957404
Author:Steven S. Zumdahl, Susan A. Zumdahl, Donald J. DeCoste
Publisher:Steven S. Zumdahl, Susan A. Zumdahl, Donald J. DeCoste
Chapter1: Chemical Foundations
Section: Chapter Questions
Problem 1RQ: Define and explain the differences between the following terms. a. law and theory b. theory and...
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Step 1: Calculate the Index of Hydrogen Deficiency (IHD).
Step 2: Use IR to determine obvious
Step 3: Use 1H-NMR to determine structural details.
Step 4: Confirm the final structure using 13C-NMR.
Find and draw the structure and give supporting data.
Transcribed Image Text:TRRNGMETTRNCEI
8-
3) C;H,Br
13C NMR
IR
LOD
ppm
139.93
120.88
29.56
25.76
17.51
200
180
160
140
120
100
80
60
40
20
4D00
3000
2000
1500
1000
CDS-04-223
ppm
HAVENUMB ERI -l
1Η NMR
Assign. Shift(ppm)
A
5.52
В
4.015
1.78
D
1.74
2
Impurity
1
8
7
6
2
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