Part D: A Multi-step Synthesis making (2-methyl-2-hexanol to 2-hexenes)1) IR: discuss the IR, specifically how you can tell the dehydration was successful. Label and discuss key peaks on your spectrum.2) Discuss/analyze NMR; focus your discussion on the peaks arising from the vinylic protons.3) Was the product successfully made? How can you tell? 4000350030002500Wavenumbers (cm-1)2000150010005007072742960.542928.25767880822862.32%Transmittance1454.851376.95886.7984870.3190-825.5892941078.331117.72961649.95983.95790.00 772.48730 842154.19666.91 656.00 647 38 640.97629.65 611.96 605.10 593.89 585.86 579.99 573.78562.20 555.78 549 38 543.93 538.25 531.18 524.96 512.7298673 13623.52505.70102 part D/E ZG.ppg1210SWI: 1015PW:9.7 us8PD: 3.0 sec5.2395.1255.0064.67760.670 29OF1:357.0INA: 12.1122.0161.901LB: 0.01.6951.6011.5181.4111.3902801.2042PTS1d: 81920.8890.7660.5060.000-0.006-0.038PPMUSER: DATE: 11/27/23 (13:46)

Given is a synthesis of 2-hexene from 2-methyl-2-hexanol.Discuss:The IR spectrumAnalyze the NMR…

Part D: A Multi-step Synthesis making (2-methyl-2-hexanol to 2-hexenes) 1) IR: discuss the IR, specifically how you can tell the dehydration was successful. Label and discuss key peaks on your spectrum. 2) Discuss/analyze NMR; focus your discussion on the peaks arising from the vinylic protons. 3) Was the product successfully made? How can you tell?

Part D: A Multi-step Synthesis making (2-methyl-2-hexanol to 2-hexenes) 1) IR: discuss the IR, specifically how you can tell the dehydration was successful. Label and discuss key peaks on your spectrum. 2) Discuss/analyze NMR; focus your discussion on the peaks arising from the vinylic protons. 3) Was the product successfully made? How can you tell?

Principles of Instrumental Analysis

7th Edition

ISBN:9781305577213

Author:Douglas A. Skoog, F. James Holler, Stanley R. Crouch

Publisher:Douglas A. Skoog, F. James Holler, Stanley R. Crouch

Chapter19: Nuclear Magnetic Resonance Spectroscopy

Section: Chapter Questions

Problem 19.14QAP: What is a rotating frame of reference?

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4000 3500 3000 2500 Wavenumbers (cm-1) 2000 20 1500 1000 500 1705.32 1354.36 1135.21 1476.83 997.91 2969.16 %Transmittance 1274.53 832.71 1427.75 953.40 553.28 790.43 1218.83 1585.98 894.05 671.73 780.29 463.73 100 C
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