Ima Chemist performed the following oxidation reaction in lab. After extracting the reaction, the 1H NMR of the crude product showed presence of impurity. One of the signal from the impurity shows as a singlet at 10 ppm. 1) Identify the functional group present in the impurity and 2) propose a detailed experiment procedure to purify product from the impure crude product. Both product and impurity are soluble in ethyl acetate solvent KMNO4 H. OH
Ima Chemist performed the following oxidation reaction in lab. After extracting the reaction, the 1H NMR of the crude product showed presence of impurity. One of the signal from the impurity shows as a singlet at 10 ppm. 1) Identify the functional group present in the impurity and 2) propose a detailed experiment procedure to purify product from the impure crude product. Both product and impurity are soluble in ethyl acetate solvent KMNO4 H. OH
Chemistry
10th Edition
ISBN:9781305957404
Author:Steven S. Zumdahl, Susan A. Zumdahl, Donald J. DeCoste
Publisher:Steven S. Zumdahl, Susan A. Zumdahl, Donald J. DeCoste
Chapter1: Chemical Foundations
Section: Chapter Questions
Problem 1RQ: Define and explain the differences between the following terms. a. law and theory b. theory and...
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Transcribed Image Text:Ima Chemist performed the following oxidation reaction in lab. After extracting the reaction, the 1H
NMR of the crude product showed presence of impurity. One of the signal from the impurity shows
as a singlet at 10 ppm. 1) Identify the functional group present in the impurity and 2) propose a
detailed experiment procedure to purify product from the impure crude product.
Both product and impurity are soluble in ethyl acetate solvent
KMNO4
H.
он
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