Based on the general procedure and reaction scheme, how much of every reagent would be needed to produce this reaction

Chemistry
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ISBN:9781305957404
Author:Steven S. Zumdahl, Susan A. Zumdahl, Donald J. DeCoste
Publisher:Steven S. Zumdahl, Susan A. Zumdahl, Donald J. DeCoste
Chapter1: Chemical Foundations
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Based on the general procedure and reaction scheme, how much of every reagent would be needed to produce this reaction?

1
OH
+
Ar
2
H
H₂N
3
p-TSA
OMe H₂O, 80 °C, 3h
O
Ar
H
Transcribed Image Text:1 OH + Ar 2 H H₂N 3 p-TSA OMe H₂O, 80 °C, 3h O Ar H
General procedure
A mixture of 4-hydroxycoumarin (1 mmol), aromatic aldehyde
(1 mmol), methyl carbamate (1.5 mmol) and p-TSA (0.1 mmol) was
suspended in water (10 mL) and stirred at 80 °C for 3 h. The reaction
was monitored by TLC. After completion, the reaction mixture was
allowed to cool to room temperature. The solid was collected by
filtration and washed with water (15 mL) to give a pure product.
Transcribed Image Text:General procedure A mixture of 4-hydroxycoumarin (1 mmol), aromatic aldehyde (1 mmol), methyl carbamate (1.5 mmol) and p-TSA (0.1 mmol) was suspended in water (10 mL) and stirred at 80 °C for 3 h. The reaction was monitored by TLC. After completion, the reaction mixture was allowed to cool to room temperature. The solid was collected by filtration and washed with water (15 mL) to give a pure product.
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