Exactly 5.00-mL aliquots of a methanol solution containing an unknown amount of methamphetamine were measured into 50.00-mL volumetric flasks. The following volumes of a standard methanol solution of methamphetamine containing 2.000 ug/mL of methamphetamine were then introduced into each flask and the mixture was diluted to volume with 0.000, 0.500, 1.00, 1.50 and 2.00 mL of methanol. 1 uL of these solutions was then injected into a gas chromatograph and the following respective peak areas were measured: 326, 480, 641, 802, and 956 (all peak areas were x 103).   Plot the data Using the plot from (a), calculate the concentration of methamphetamine in the unknown. Derive a least squares equation from the data. Calculate the concentration of methamphetamine from the equation in (c).

Introduction to General, Organic and Biochemistry
11th Edition
ISBN:9781285869759
Author:Frederick A. Bettelheim, William H. Brown, Mary K. Campbell, Shawn O. Farrell, Omar Torres
Publisher:Frederick A. Bettelheim, William H. Brown, Mary K. Campbell, Shawn O. Farrell, Omar Torres
Chapter6: Solutions And Colloids
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  1. Exactly 5.00-mL aliquots of a methanol solution containing an unknown amount of methamphetamine were measured into 50.00-mL volumetric flasks. The following volumes of a standard methanol solution of methamphetamine containing 2.000 ug/mL of methamphetamine were then introduced into each flask and the mixture was diluted to volume with 0.000, 0.500, 1.00, 1.50 and 2.00 mL of methanol. 1 uL of these solutions was then injected into a gas chromatograph and the following respective peak areas were measured: 326, 480, 641, 802, and 956 (all peak areas were x 103).

 

  1. Plot the data
  2. Using the plot from (a), calculate the concentration of methamphetamine in the unknown.
  3. Derive a least squares equation from the data.
  4. Calculate the concentration of methamphetamine from the equation in (c).

 

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