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counts counts counts **Provide the values on each x-axis (be especially clear about the position of all signals). Label EVERY signal with the structure(s) that is/are responsible for >1% of each signal (for both GC-FID and GC-MS). Include isotope signals that result from any atom that has a natural abundance of 1% or greater. Information such as area under the curve, signal intensity, and signal width should be accurately depicted. This is just a template, depending on the assignment some MS spectra below may not be needed. Additional instructions are often provided in the assignment question. If a discrepancy should arise, the assignment instructions supersede the template instructions. FID MS at 5.13 minutes MS at 7.61 minutes MS at 10.43 minutes m/z m/z m/z minutes

counts counts counts **Provide the values on each x-axis (be especially clear about the position of all signals). Label EVERY signal with the structure(s) that is/are responsible for >1% of each signal (for both GC-FID and GC-MS). Include isotope signals that result from any atom that has a natural abundance of 1% or greater. Information such as area under the curve, signal intensity, and signal width should be accurately depicted. This is just a template, depending on the assignment some MS spectra below may not be needed. Additional instructions are often provided in the assignment question. If a discrepancy should arise, the assignment instructions supersede the template instructions. FID MS at 5.13 minutes MS at 7.61 minutes MS at 10.43 minutes m/z m/z m/z minutes

Physical Chemistry
Physical Chemistry
2nd Edition
ISBN:9781133958437
Author:Ball, David W. (david Warren), BAER, Tomas
Publisher:Ball, David W. (david Warren), BAER, Tomas
Chapter16: Introduction To Magnetic Spectroscopy
Section: Chapter Questions
Problem 16.46E: a The structure of 2 chloroethanol is usually staggered, as shown in this Newman projection: How...
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use template attached please to show how to draw, thank you!
 
Imagine that you analyzed the original distillation mixture from Exp #3 using a Gas Chromatography instrument that is equipped with both a Flame Ionization Detector (FID) and a Mass Spectrometer (MS). Use the “GC-FID/MS Template” provided in the Experiment folder (if you cannot print it or annotate it, then you may hand-draw the template and your answers on a piece of paper). For this question, and this question only, you may very neatly hand-
draw or use ChemDraw to add structures to the spectra
 
i) On the “GC-FID/MS Template,” draw the FID spectrum for the Exp #5 original mixture. Assume that the compounds elute from the column at 5.13 minutes, 7.61 minutes, and 10.43 minutes. Clearly label each signal with the corresponding compound name. Signals should not be drawn as more than “30 seconds wide.” Each signal should include a retention time below the signal (as described above).
counts counts counts **Provide the values on each x-axis (be especially clear about the position of all signals). Label EVERY signal with the structure(s) that is/are responsible for >1% of each signal (for both GC-FID and GC-MS). Include isotope signals that result from any atom that has a natural abundance of 1% or greater. Information such as area under the curve, signal intensity, and signal width should be accurately depicted. This is just a template, depending on the assignment some MS spectra below may not be needed. Additional instructions are often provided in the assignment question. If a discrepancy should arise, the assignment instructions supersede the template instructions. FID MS at 5.13 minutes MS at 7.61 minutes MS at 10.43 minutes m/z m/z m/z minutes
Transcribed Image Text:counts counts counts **Provide the values on each x-axis (be especially clear about the position of all signals). Label EVERY signal with the structure(s) that is/are responsible for >1% of each signal (for both GC-FID and GC-MS). Include isotope signals that result from any atom that has a natural abundance of 1% or greater. Information such as area under the curve, signal intensity, and signal width should be accurately depicted. This is just a template, depending on the assignment some MS spectra below may not be needed. Additional instructions are often provided in the assignment question. If a discrepancy should arise, the assignment instructions supersede the template instructions. FID MS at 5.13 minutes MS at 7.61 minutes MS at 10.43 minutes m/z m/z m/z minutes
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