(c) Preparation of hexaamminenickel(II) chloride, [Ni(NH3)6] Cl2 USE THE FUME HOOD. Dissolve 6.0 g of nickel chloride hexahydrate in about 6 mL of hot distilled H2O. Add about 12 mL of concentrated aqueous ammonia slowly to the rapidly stirred solution until the green precipitate of nickel hydroxide has dissolved. Allow the mixture to stand at room temperature for 10 min (use an ice bath if crystallization does not occur spontaneously) and then remove the crystals of hexaamminenickel(II) chloride by filtration on a Buchner funnel in the fume hood. Wash the precipitate with about 25 mL of concentrated ammonia, then wash t with acetone and allow the product to dry at room temperature in air. Record the yield. prod = 1.75 و рогре
(c) Preparation of hexaamminenickel(II) chloride, [Ni(NH3)6] Cl2 USE THE FUME HOOD. Dissolve 6.0 g of nickel chloride hexahydrate in about 6 mL of hot distilled H2O. Add about 12 mL of concentrated aqueous ammonia slowly to the rapidly stirred solution until the green precipitate of nickel hydroxide has dissolved. Allow the mixture to stand at room temperature for 10 min (use an ice bath if crystallization does not occur spontaneously) and then remove the crystals of hexaamminenickel(II) chloride by filtration on a Buchner funnel in the fume hood. Wash the precipitate with about 25 mL of concentrated ammonia, then wash t with acetone and allow the product to dry at room temperature in air. Record the yield. prod = 1.75 و рогре
Chapter1: Taking Risks And Making Profits Within The Dynamic Business Environment
Section: Chapter Questions
Problem 1CE
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