Attached 1st Reaction was performed in the Synthesis of Dihydrosafrole via Friedel-Crafts Acylation & Reduction Experiment resulting in following IR spectra. Can you analyze it and fill the following table? Are their any impurities found? Peak Position cm-1 Bond Type Functional Group
Attached 1st Reaction was performed in the Synthesis of Dihydrosafrole via Friedel-Crafts Acylation & Reduction Experiment resulting in following IR spectra. Can you analyze it and fill the following table? Are their any impurities found? Peak Position cm-1 Bond Type Functional Group
Principles of Instrumental Analysis
7th Edition
ISBN:9781305577213
Author:Douglas A. Skoog, F. James Holler, Stanley R. Crouch
Publisher:Douglas A. Skoog, F. James Holler, Stanley R. Crouch
Chapter6: An Introduction To Spectrometric Methods
Section: Chapter Questions
Problem 6.1QAP
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Question
Attached 1st Reaction was performed in the Synthesis of Dihydrosafrole via Friedel-Crafts Acylation & Reduction Experiment resulting in following IR spectra. Can you analyze it and fill the following table? Are their any impurities found?
Peak Position cm-1 |
Bond Type |
|
![Wavenumbers (cm-1)
4000
3500
3000
2500
2000
1500
1000
500
-2
0
$34.97
N
4
6
1248.08
8
10
12-
14-
16
18
20
22-
24
26
1678.11
1503.63
1487.15
1440.18
%Transmittance
1038.47
2977.99
2905.83
1604.99
1359.44
1140.00
1112.25
933.58
877.83
794.48
1460.69
1765.04
3077.21
3344.59
966.30
3224.27
2784.35
2717.68
2673.35
2616.36
2480.21
1859.63
1818.47
1308.71
1071.24
744.04 718.36](/v2/_next/image?url=https%3A%2F%2Fcontent.bartleby.com%2Fqna-images%2Fquestion%2Fc4436f5f-01e3-4d46-baa5-3f23cf388ae7%2Fee7f34f2-952c-4302-b261-f7d46e70bd25%2Flkrq3eg_processed.jpeg&w=3840&q=75)
Transcribed Image Text:Wavenumbers (cm-1)
4000
3500
3000
2500
2000
1500
1000
500
-2
0
$34.97
N
4
6
1248.08
8
10
12-
14-
16
18
20
22-
24
26
1678.11
1503.63
1487.15
1440.18
%Transmittance
1038.47
2977.99
2905.83
1604.99
1359.44
1140.00
1112.25
933.58
877.83
794.48
1460.69
1765.04
3077.21
3344.59
966.30
3224.27
2784.35
2717.68
2673.35
2616.36
2480.21
1859.63
1818.47
1308.71
1071.24
744.04 718.36
![Reaction 1
da
CH₁
ZnO (nanoparticles)
Heat
ol
CH₂](/v2/_next/image?url=https%3A%2F%2Fcontent.bartleby.com%2Fqna-images%2Fquestion%2Fc4436f5f-01e3-4d46-baa5-3f23cf388ae7%2Fee7f34f2-952c-4302-b261-f7d46e70bd25%2F2xt6yu7_processed.png&w=3840&q=75)
Transcribed Image Text:Reaction 1
da
CH₁
ZnO (nanoparticles)
Heat
ol
CH₂
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