An unknown compound was given and following data was given. Identify what the compound is based on the 1H NMR, FT-IR and melting point data.   Table 1. Data for Melting Point Sample mp range (°C) Lit mp (°C) Correction Factor (°C) Corrected mp (°C) Unknown #9 123.7-125.2         124.0-125.2       Standard 123.8-125.3       Benzoic Acid 124.1-125.5

Chemistry
10th Edition
ISBN:9781305957404
Author:Steven S. Zumdahl, Susan A. Zumdahl, Donald J. DeCoste
Publisher:Steven S. Zumdahl, Susan A. Zumdahl, Donald J. DeCoste
Chapter1: Chemical Foundations
Section: Chapter Questions
Problem 1RQ: Define and explain the differences between the following terms. a. law and theory b. theory and...
icon
Related questions
Question

An unknown compound was given and following data was given. Identify what the compound is based on the 1H NMR, FT-IR and melting point data.

 

Table 1. Data for Melting Point

Sample

mp range (°C)

Lit mp (°C)

Correction Factor (°C)

Corrected mp (°C)

Unknown #9

123.7-125.2

 

 

 

 

124.0-125.2

 

 

 

Standard

123.8-125.3

 

 

 

Benzoic Acid

124.1-125.5

 

 

 

Unknown 9 in CDCI,
offset: 0.9 ppm.
11
10
3
33 →peak splits
Transcribed Image Text:Unknown 9 in CDCI, offset: 0.9 ppm. 11 10 3 33 →peak splits
80-
75
70
65-
60
55-
50-
45-
40
35
30-
25-
20-
15-
10-
5-
4000
3500
3000
2500
2000
1500
1000
500
Wavenumbers (cm-1)
%Transmittance
Transcribed Image Text:80- 75 70 65- 60 55- 50- 45- 40 35 30- 25- 20- 15- 10- 5- 4000 3500 3000 2500 2000 1500 1000 500 Wavenumbers (cm-1) %Transmittance
Expert Solution
steps

Step by step

Solved in 2 steps with 1 images

Blurred answer
Similar questions
  • SEE MORE QUESTIONS
Recommended textbooks for you
Chemistry
Chemistry
Chemistry
ISBN:
9781305957404
Author:
Steven S. Zumdahl, Susan A. Zumdahl, Donald J. DeCoste
Publisher:
Cengage Learning
Chemistry
Chemistry
Chemistry
ISBN:
9781259911156
Author:
Raymond Chang Dr., Jason Overby Professor
Publisher:
McGraw-Hill Education
Principles of Instrumental Analysis
Principles of Instrumental Analysis
Chemistry
ISBN:
9781305577213
Author:
Douglas A. Skoog, F. James Holler, Stanley R. Crouch
Publisher:
Cengage Learning
Organic Chemistry
Organic Chemistry
Chemistry
ISBN:
9780078021558
Author:
Janice Gorzynski Smith Dr.
Publisher:
McGraw-Hill Education
Chemistry: Principles and Reactions
Chemistry: Principles and Reactions
Chemistry
ISBN:
9781305079373
Author:
William L. Masterton, Cecile N. Hurley
Publisher:
Cengage Learning
Elementary Principles of Chemical Processes, Bind…
Elementary Principles of Chemical Processes, Bind…
Chemistry
ISBN:
9781118431221
Author:
Richard M. Felder, Ronald W. Rousseau, Lisa G. Bullard
Publisher:
WILEY