By looking at the H1 NMR spectra, draw the structure for the Liquid organic unknown compound and explain the process you used to determine the identity of your compound. Show all H atoms and label each equivalent set of atoms as A, B, C etc in the structure. Then, calculate the expected chemical shift for each of the equivalent set of H atoms in the structure. Clearly label your calculations Note: (Clearly list the tables used, base shift values and what correction factors were used.) 98.0368.0047.926F1: 60.201EX: c:left\HI\ACQ.ppg7.8767.5087.4807.4227.3937.3397.2717654OF1: 360.3NA: 13.161SW1: 1000PW: 14.4 usPD: 3.0 secH1- NMR | Lique'd unknown)3LB: 0.021.3271.2101.088PTS1d: 8192000 0-10 PPMUSER: DATE: 01/25/24 (15:30) The list of all the possible organic compounds are as follows:Cumene, 3-Methy-2-butanone, Phenethyl alcohol, Isopropyl Acetate, Ethel benzoate,3-phenylpropionaldehyde, isobutyl cinnamate, cyclamen aldehyde, Styrallyl acetate, Butylbutyrate, propiophenon, phenylacetylene, Cis-Hexenyl-3-Acetate, Benzyl propionate,3-(p-ethyl-phenyl)-2,2-dimethyl propionaldehyde, 2-methoxy-4-ethyl-phenol, P-ethylphenol,diphenyl amine, 4-phenyl-3-buten-2-one, Diethyl Terphthalate, glutaric acid, cinnamic acid, P-ethylbenzoic acid, Coumarin, vanillin, (2,2,2-trichloro-1-phenylethyl)acetate,4-(p-hydroxyphenyl)-2-butanone, 2-ethoxy-5-prop-1-enylphenol, t-butyl-phenol, Thymol,Calone, Syringol, Syringaldehyde. Borderline MP unknowns: Styrallyl alcohol,1,1-dimethyl-2-phenethyl acetate 1,1-dimethyl-2-phenyl ethanol.

To identify the structure based on the given 1H NMR

Answered: 6 8 7 9 S 3 0 PPM 8.036 8.004 7.926…

6 8 7 9 S 3 0 PPM 8.036 8.004 7.926 7.876 7.508 7.480 7.422 7.393 7.339 7.271 3.161 3.039 2.920 2.802 1.327 1.210 1.088 -0.000

Appl Of Ms Excel In Analytical Chemistry

2nd Edition

ISBN:9781285686691

Author:Crouch

Publisher:Crouch

Chapter2: Basic Statistical Analysis With Excel

Section: Chapter Questions

Problem 12P

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