a) Interpreted the analytical data reported, you should include reference to theIR, and NMR chemical shifts, integration and observed splitting patterns Question 4.You are asked to identify an unknown compound, which has the following analyticaldata:PPMChemical ShiftIntegration1Multiplicity8.287.9517.486.9911d4.1122.811.343tThe peak at 8.28 ppm is found to disappear when the NMR sample is treated withD20The IR spectrum of the unknown has the following key peaks;a sharp strong peak at 1680 cm-1a broad signal at 3250 cm-1The compound has a molecular weight of 213.66You have been provided with 9 possible structures of the unknown compound.

Answered: Image /qna-images/answer/d716a419-5625-4e1b-b934-1241e5a7df6d.jpg

Question 4. You are asked to identify an unknown compound, which has the following analytical data: PPM Chemical Shift Integration 1 Multiplicity 8.28 7.95 1 d 7.48 1 6.99 4.11 1 d. 2 2.81 1.34 3 The peak at 8.28 ppm is found to disappear when the NMR sample is treated with

Question 4. You are asked to identify an unknown compound, which has the following analytical data: PPM Chemical Shift Integration 1 Multiplicity 8.28 7.95 1 d 7.48 1 6.99 4.11 1 d. 2 2.81 1.34 3 The peak at 8.28 ppm is found to disappear when the NMR sample is treated with

Organic Chemistry

9th Edition

ISBN:9781305080485

Author:John E. McMurry

Publisher:John E. McMurry

Chapter13: Structure Determination: Nuclear Magnetic Resonance Spectroscopy

Section13.12: Dept 13c Nmr Spectroscopy

Problem 21P

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Concept explainers

NMR Spectroscopy

NMR stands for Nuclear Magnetic Resonance in which the study of different molecules is done based on the interaction of radiofrequency electromagnetic radiations with the nuclei of molecules placed in a strong magnetic field. A precise study of spectra of visible light and all bands of electromagnetic radiation is called spectroscopy.

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a) Interpreted the analytical data reported, you should include reference to the
IR, and NMR chemical shifts, integration and observed splitting patterns

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