5:18 PM (()) 32.9 Vo 4G K/S LTE 1 Reaction between 24 dihydroxy benzoic acid and copper acetate And After this reaction with dabco Yes Solvemt methanol ||| = 5 4G 93
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- Nitration of methyl benzoate: Weight of filler paper: 0.682g Mp product: 76-77 C Nitration of Acetanilide: Weight of filler paper: 0.691g Weight of filler paper product: 1.232g Mp product: 212-214 C Compound MM (g/mol) ortho mp (oC) meta mp (oC) para mp (oC) Nitroacetanilide 180.16 94 155 214-217 Methyl nitrobenzoate 181.15 -13 78-80 94-96 Theoretical yield of acetanilde: 0.6664g Theoretical yield of methyl benzoate: 0.7317g find theoretical yield of methyl nitrobenzoate percent yield of your methyl nitrobenzoate and melting point of your methyl nitrobenzoateA Studen t is Purformad the falliwing reaction and atter Com plet ing the work-up Step and isulating be cnde Aridunet iP was detenmined they t The starting matunal Was still Hcsent The student attmped to peaty The Aroduet by columo Chamatagraphy wih Slia gel column and ethyl 94tate as the eluant- The studn't Collected 1o fractiuns and ran g TLC of cnch fraction 4 8 9 10 cunclude about the Separatión ? (whch fractiun s What Can yoy Contained which compund? Are there mixed fract win s?)OBr a) Heptanamide 1) (Me),CuLi b) MeHC-CHCOMC 2) H;O - OH (aq) c) 2 Acetaldehyde Benzene d) Valeramide SOCI. Heat c) 2-Octanone (Ph)sP-CH2
- Data: Nitration of methyl benzoate: Weight of filler paper: 0.682g Mp product: 76-77 C Nitration of Acetanilide: Weight of filler paper: 0.691g Weight of filler paper product: 1.232g Mp product: 212-214 C Compound MM (g/mol) ortho mp (oC) meta mp (oC) para mp (oC) Nitroacetanilide 180.16 94 155 214-217 Methyl nitrobenzoate 181.15 -13 78-80 94-96 Draw all the resonance forms for the arenium ion formed during the nitration of acetanilide.Data: Nitration of methyl benzoate: Weight of filler paper: 0.682g Mp product: 76-77 C Nitration of Acetanilide: Weight of filler paper: 0.691g Weight of filler paper product: 1.232g Mp product: 212-214 C Compound MM (g/mol) ortho mp (oC) meta mp (oC) para mp (oC) Nitroacetanilide 180.16 94 155 214-217 Methyl nitrobenzoate 181.15 -13 78-80 94-96 Based on the table above , determine the regiochemistry of your nitroacetanilide and draw the structure. Draw all the resonance forms for the arenium ion (cation intermediate) formed during the nitration of methyl benzoate.(in Consider the tolluiing reactun hat is the theorechial yıcld Product if -50g of Startiny inaturial and o. grams) KoH arc use1? 0:50g f KOH Mdcular wughts 5611 Chemial fomala;(8 Hyo 4olecalar waghts :20-15 Mukalar cuclght:222.29
- Q write mechansim Two reactions: (1) 1., H (1 equiv.) 2. a) LiAlH b) H2O work - up 3. H (final product only ) 1. 2. CH¸ MgBr 3. CH₂OH,H* Gwrite mechansim Two reactions: 0 ② CN 1. HO. OH H+ (1 equiv.) H 2. a) LiAlH4 b) H₂O work-up 3. H+ 1. HO (1 equiv.) H 2. CH3MgBr 3. CH3OH, H+ OH, H+ (final product only) OCH3 (±)Org. Chem. 1. EA21Q22