103 IR LUU 13C NMR ppm 209.13 178.49 50 42.35 32.95 29.87 18.64 4 D00 3000 1000 e000 1500 S00 HAVENUMBERI -l 1Η NMR 200 180 160 140 120 100 80 60 40 20 Cos-04-320 ppm Assign. Shift(ppm) Exchanges w/ D20 A 11.24 В 2.53 2.41 D 2.16 E 1.91 TMS 1 2 2 12 11 10 8. 3 2
103 IR LUU 13C NMR ppm 209.13 178.49 50 42.35 32.95 29.87 18.64 4 D00 3000 1000 e000 1500 S00 HAVENUMBERI -l 1Η NMR 200 180 160 140 120 100 80 60 40 20 Cos-04-320 ppm Assign. Shift(ppm) Exchanges w/ D20 A 11.24 В 2.53 2.41 D 2.16 E 1.91 TMS 1 2 2 12 11 10 8. 3 2
Chemistry
10th Edition
ISBN:9781305957404
Author:Steven S. Zumdahl, Susan A. Zumdahl, Donald J. DeCoste
Publisher:Steven S. Zumdahl, Susan A. Zumdahl, Donald J. DeCoste
Chapter1: Chemical Foundations
Section: Chapter Questions
Problem 1RQ: Define and explain the differences between the following terms. a. law and theory b. theory and...
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B. explain each step with words on how to get the structure.
Step 1: Calculate the Index of Hydrogen Deficiency (IHD).
Step 2: Use IR to determine obvious
Step 3: Use 1H-NMR to determine structural details.
Step 4: Confirm the final structure using 13C-NMR.
Transcribed Image Text:2) CH1,O3
IR
LUD
13C NMR
ppm
209.13
178.49
42.35
32.95
29.87
18.64
4000
3000
2000
1500
100
HAVENUMBERI -l
1Η ΝMR
200
180
160
140
120
100
80
60
40
20
CoS-04-320
ppm
TT
Assign. Shift(ppm)
Exchanges
w/ D20
A
11.24
2.53
C
2.41
2.16
2
V
1.91
TMS
1
2
2
12
11
10
8
7
6.
4
2
1
TRANSHITTANCEIXI
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