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6.05 Ignitable Liquids (50 Points)
Recovering Ignitable Liquids
Gather information about at least three methods investigators use to identify the presence
of ignitable liquids. Describe how the method is used and some advantages and
disadvantages of that method.
Method to identify
ignitable liquids
(1
point each)
Describe how it is
used
(2 points each)
Advantages
(2 points
each)
Disadvantages
(2
points each)
1. GC
It is used to separate
and analyze
components in
mixture
chromatographically
Spped of analysis
high sensitivity
Limited to volatile
sample
Does not react with
column
2. MS
Analyzed substance
for suspected drugs
by toxicologists
Sensitivity
specificity
Not good of
identifying
Carbons that
produce similar ions
3. UV
The band of
wavelengths between
visible light and x
rays that can’t be
seen by humans
The pour patterns
are identified and this
means it accelerate
long after its order is
discernible.
Sun burn the eyes
and burn the skin
Long exposure times
4. As an investigator, which method would you choose to search for ignitable liquids at the scene
of a recent apartment fire? Explain your reasoning.
(2 points)
A UV light because uv lights are
a really kind of special unique light and it can get the smoke out of the aparments.
Select three of the following types of evidence and describe the process for collecting them
during a fire investigation.
Types of evidence: carpet, tile, cement, linoleum, sand or soil, wood flooring
Type of evidence
Best portion/location to
collect from
(2 points)
How to collect
(2 points)
5. carpet
Under furniture
It’s a long process to collect
but to make it simple
photograph if it is damaged
and if a suspect area is
identified cut a long strip of
© ACCESS Virtual Learning 2020
carpet for further analyzing
6. wood flooring
Floor patterns where
wood gained is aligned
vertically
It is a long process but to
make it simple use a wood
chisel and hand sledge to
cut the slivers from both
sides of the joined board
seams and after this further
analyze.
7. linoleum
Sampling from
different materials and
using the right tools.
It is a long process but to
make it simple identify the
edge of the pool. Cut long
strips of flooring along the
periphery zone and further
analyze.
8. Which of these types of material will likely contain the most useful amount of ignitable liquid
evidence? Explain.
(2 points)
wood flooring because many arsonists or fire starters pour
liquids that are flammable/ignitable on floors or walls and stairs.
9. What type of container is best for packaging these types of evidence?
(2 points)
An evidence
can
11. Explain what a reference sample is and why it is collected.
(3 points)
It is for comparison
and elimination reasons.
Analyzing Evidence
11. What two methods are utilized to analyze ignitable liquids after they are collected and
transported to the lab?
(2 points)
Mass spectrometry and gas chromatography
Examine the graph below and answer the following questions.
© ACCESS Virtual Learning 2020
(
https://www.osha.gov/dts/sltc/methods/partial/pv2028/gasolinefig1.gif
)
12. What method was utilized to prepare this graph?
Explain your reasoning.
(2 point)
gas
chromatograpghy and because it has two phases
13. Which of the labeled components of this sample was most attracted to the stationary phase?
Explain your reasoning.
(2 points)
C and this is because it exits out of the column
14. Which of the labeled components of this sample was present in the greatest abundance in the
mixture? Explain your reasoning.
(2 points)
A and this is because it reaches the maximum
© ACCESS Virtual Learning 2020
C
A
B
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Standardization of Sodium Hydroxide (NaOH) Solution
Mass of KHP used (g)
Initial buret reading (mL)
Final Buret reading (mL)
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Initial buret reading (mL)
Final buret reading (mL)
Volume of base used (mL)
Molarity of the Acetic Acid in the Vinegar (M) HINT: Use as the M of base
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0.7138
1.15
18.97
Try 1: ✔ 17.82
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NG 6
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Trial 1
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Chemistry
please neat writing!
13.28
Pick an appropriate solvent(s) from table to
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Common Polar
Common Nonpolar Solvents
Solvents
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hexane
(H₂O)
(C6H12)
acetone
diethyl ether
(CH3CH₂OCH2CH3)
(CH3COCH3)
methyl alcohol
(CH3OH)
toluene
(C7H8)
Part A
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Express your answer as a chemical formula. If there is more than one answer, separate
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ΑΣΦ
?
Part B
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Express your answer as a chemical formula. If there is more than one answer, separate
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?
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Express your answer as a chemical formula. If there is more than one answer, separate
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ΑΣΦ
?
Part D
sodium nitrate (ionic)
Express your answer as a chemical formula. If there is more than one answer, separate
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2= | ΑΣΦ
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Na₂CO3(aq)
Na₂CO3 (aq)
Na₂CO3 (aq)
Na2CO3 (aq)
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