(a)
Interpretation:
The standard solution of methyl vinyl
Concentration MVK, mmol/L | Relative Peak Area |
0.500 | 3.76 |
1.50 | 9.16 |
2.50 | 15.03 |
3.50 | 20.42 |
4.50 | 25.33 |
5.50 | 31.97 |
The slope and the intercept of the least square line are to be determined.
Concept introduction:
The slope of a line is also known as a gradient of line which is used to define the direction and steepness of the line.
The intercept line is the y-axis of a line at which point it crosses the X −axis.
(b)
Interpretation:
The graph for the least square line as well as experimental points is to be plotted.
Concept introduction:
The least-square method is a method in which the best result is obtained for the set data point by minimizing the sum of offset or residuals from the plot of curve statistically.
(c)
Interpretation:
The relative peak area of the sample containing MVK is 10.3. The concentration of MVK in the solution is to be determined.
Concept introduction:
The slope of a line is also known as a gradient of line which is used to define the direction and steepness of the line.
The intercept line is the y-axis of a line at which point it crosses the X −axis.
(d)
Interpretation:
It is considered that the result obtained from (d) is representing the single measurement as well as the mean of four measurements. The respective absolute and relative standard deviation is to be determined.
Concept introduction:
The standard deviation method is used for the quantification of the amount of variation or for the dispersion for the set of the data values.
(e)
Interpretation:
The calculation for the section (c) and (d) is to be repeated when the peak area of the sample is 22.8.
Concept introduction:
The standard deviation method is used for the quantification of the amount of variation or for the dispersion for the set of the data values.

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Chapter A1 Solutions
PRINCIPLES OF INSTRUMENTAL ANALYSIS
- What is the missing reactant R in this organic reaction? + R H3O+ + • Draw the structure of R in the drawing area below. • Be sure to use wedge and dash bonds if it's necessary to draw one particular enantiomer. Click and drag to start drawing a structure.arrow_forwardWhat would be the best choices for the missing reagents 1 and 3 in this synthesis? 1 1. PPh3 2. n-BuLi 2 • Draw the missing reagents in the drawing area below. You can draw them in any arrangement you like. • Do not draw the missing reagent 2. If you draw 1 correctly, we'll know what it is. • Note: if one of your reagents needs to contain a halogen, use bromine. Click and drag to start drawing a structure.arrow_forwardThe product on the right-hand side of this reaction can be prepared from two organic reactants, under the conditions shown above and below the arrow. Draw 1 and 2 below, in any arrangement you like. 1+2 NaBH₂CN H+ N Click and drag to start drawing a structure. X $arrow_forward
- Explain what is the maximum absorbance of in which caffeine absorbs?arrow_forwardExplain reasons as to why the amount of caffeine extracted from both a singular extraction (5ml Mountain Dew) and a multiple extraction (2 x 5.0ml Mountain Dew) were severely high when compared to coca-cola?arrow_forwardProtecting Groups and Carbonyls 6) The synthesis generates allethrolone that exhibits high insect toxicity but low mammalian toxicity. They are used in pet shampoo, human lice shampoo, and industrial sprays for insects and mosquitos. Propose detailed mechanistic steps to generate the allethrolone label the different types of reagents (Grignard, acid/base protonation, acid/base deprotonation, reduction, oxidation, witting, aldol condensation, Robinson annulation, etc.) III + VI HS HS H+ CH,CH,Li III I II IV CI + P(Ph)3 V ༼ Hint: no strong base added VI S VII IX HO VIII -MgBr HgCl2,HgO HO. isomerization aqeuous solution H,SO, ༽༽༤༽༽ X MeOH Hint: enhances selectivity for reaction at the S X ☑arrow_forward
- Draw the complete mechanism for the acid-catalyzed hydration of this alkene. esc 田 Explanation Check 1 888 Q A slock Add/Remove step Q F4 F5 F6 A བྲA F7 $ % 5 @ 4 2 3 & 6 87 Click and drag to start drawing a structure. © 2025 McGraw Hill LLC. All Rights Reserved. Terms of Use | Privacy Ce W E R T Y U S D LL G H IK DD 요 F8 F9 F10 F1 * ( 8 9 0 O P J K L Z X C V B N M H He commandarrow_forwardExplanation Check F1 H₂O H₂ Pd 1) MCPBA 2) H3O+ 1) Hg(OAc)2, H₂O 2) NaBH4 OH CI OH OH OH hydration halohydrin formation addition halogenation hydrogenation inhalation hydrogenation hydration ☐ halohydrin formation addition halogenation formation chelation hydrogenation halohydrin formation substitution hydration halogenation addition Ohalohydrin formation subtraction halogenation addition hydrogenation hydration F2 80 F3 σ F4 F5 F6 1 ! 2 # 3 $ 4 % 05 Q W & Å © 2025 McGraw Hill LLC. All Rights Reserved. F7 F8 ( 6 7 8 9 LU E R T Y U A F9arrow_forwardShow the mechanism steps to obtain the lowerenergy intermediate: *see imagearrow_forward
- Soap is made by the previous reaction *see image. The main difference between one soap and another soap isthe length (number of carbons) of the carboxylic acid. However, if a soap irritates your skin, they mostlikely used too much lye.Detergents have the same chemical structure as soaps except for the functional group. Detergentshave sulfate (R-SO4H) and phosphate (R-PO4H2) functional groups. Draw the above carboxylic acidcarbon chain but as the two variants of detergents. *see imagearrow_forwardWhat are the reactions or reagents used? *see imagearrow_forwardWhat are the reactions or reagents used? *see imagearrow_forward
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