Owlv2 With Labskills, 4 Terms (24 Months) Printed Access Card For Williamson/masters' Macroscale And Microscale Organic Experiments, 7th
7th Edition
ISBN: 9781305884168
Author: Williamson, Kenneth L.; Masters, Katherine M.
Publisher: Cengage Learning
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Chapter 5, Problem 10Q
Interpretation Introduction
Interpretation:
The reason for the more efficiency of the packed column as compared to the unpacked column should be determined.
Concept introduction:
A technique used to separate various components or a fraction from mixture based on their volatilities is called fractional distillation. The fractional distillation is used to separate different components of the mixture if boiling point difference is less than
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Chapter 5 Solutions
Owlv2 With Labskills, 4 Terms (24 Months) Printed Access Card For Williamson/masters' Macroscale And Microscale Organic Experiments, 7th
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- 5. Use the MS data to answer the questions on the next page. 14.0 1.4 15.0 8.1 100- MS-IW-5644 26.0 2.8 27.0 6.7 28.0 1.8 29.0 80 4.4 38.0 1.0 39.0 1.5 41.0 1.2 42.0 11.2 43.0 100.0 44.0 4.3 79.0 1.9 80.0 2.6 Relative Intensity 40 81.0 1.9 82.0 2.5 93.0 8.7 20- 95.0 8.2 121.0 2.0 123.0 2.0 136.0 11.8 0 138.0 11.5 20 40 8. 60 a. Br - 0 80 100 120 140 160 180 200 220 m/z Identify the m/z of the base peak and molecular ion. 2 b. Draw structures for each of the following fragments (include electrons and charges): 43.0, 93.0, 95.0, 136.0, and 138.0 m/z. C. Draw a reasonable a-fragmentation mechanism for the fragmentation of the molecular ion to fragment 43.0 m/z. Be sure to include all electrons and formal charges. 6. Using the values provided in Appendix E of your lab manual, calculate the monoisotopic mass for the pyridinium ion (CsH6N) and show your work.arrow_forwardNonearrow_forwardStereochemistry: Three possible answers- diastereomers, enantiomers OH CH₂OH I -c=0 21108 1101 41745 HOR CH₂OH IL Но CH₂OH TIL a. Compounds I and III have this relationship with each other: enantiomers b. Compounds II and IV have this relationship with each other: c. Compounds I and II have this relationship with each other: d. *Draw one structure that is a stereoisomer of II, but neither a diastereomer nor an enantiomer. (more than one correct answer)arrow_forward
- Don't used Ai solutionarrow_forwardDon't used Ai solutionarrow_forwardIn mass spectrometry, alpha cleavages are common in molecules with heteroatoms. Draw the two daughter ions that would be observed in the mass spectrum resulting from an alpha cleavage of this molecule. + NH2 Q Draw Fragment with m/z of 72arrow_forward
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