Macroscale and Microscale Organic Experiments
Macroscale and Microscale Organic Experiments
7th Edition
ISBN: 9781305577190
Author: Kenneth L. Williamson, Katherine M. Masters
Publisher: Brooks Cole
Question
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Chapter 4, Problem 1Q
Interpretation Introduction

Interpretation:

The gray color of the naphthalene obtained after the usual purification procedure should be explained.

Concept introduction:

Recrystallization is a technique that is used to purify the impure compounds. It is based on the principle that the solubility of substances increases with the increase in temperature.

Following are some of the types of recrystallization:

  1. Single-solvent recrystallization
  2. Multi-solvent recrystallization
  3. Hot filtration-recrystallization

Expert Solution & Answer
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Answer to Problem 1Q

The gray color of naphthalene is due to the impurity of charcoal.

Explanation of Solution

The change in color of naphthalene indicates the presence of an impurity in it. But this impurity neither lowers the melting point of the sample nor widens the melting point range. So this is not a normal small-sized impurity and it shows only color change in the sample. The color of the sample changes from white to gray so the impurity may be charcoal (black) that is used in the recrystallization process.

Conclusion

Due to the impurity of charcoal, naphthalene found to have grayish color.

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