OWLv2 with LabSkills for Gilbert/Martin's Experimental Organic Chemistry: A Miniscale & Microscale Approach, 6th Edition, [Instant Access], 4 terms (24 months)
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Chapter 3.3, Problem 22E

a)

Interpretation Introduction

Interpretation:Difference in melting points of sample with sample tube has height of 2 mm than that of 5 mm should be explained.

Concept introduction:Melting point is temperature that involves conversion of substance from solid to liquid state. Both liquid and solid phases are present in equilibrium with each other at this temperature.

b)

Interpretation Introduction

Interpretation:Source of error in measurement of melting point of 130135 °C should be determined.

Concept introduction:Melting point is temperature that involves conversion of substance from solid to liquid state. Both liquid and solid phases are present in equilibrium with each other at this temperature.

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2. The goal behind suction filtration is to remove soluble impurities that are on the surface of the crystals. Therefore, why can't you simply use suction filtration instead of recrystallization to purify an impure solid?
You were tasked to separate the components of a mixture containing silica, sodium chloride and charcoal. TNāCI dissolves in water while silica and charcoal are not water-soluble. Only charcoal dissolves in carbon disulfide. a. Write a short experimental procedure to carry out the separation of the mixture. b. Given the following data, determine the percentage of charcoal, sodium chloride and silica. Mass (g) Mass of beaker 100.000 Mass of beaker + mixture 110.000 mass of evaporating dish 62.000 mass of evaporating dish + solid after evaporation of water 65.000 Mass of beaker + charcoal + silica after evaporation of excess water 117.000 mass of beaker + silica after decanting dissolved charcoal and drying 113.545
What is the main purpose of recrystallisation? A. Chemists recrystallise solids when they want to change big crystals into small crystals. B. Chemists recrystallise solids that are contaminated with impurities. If done properly, the solid will then recrystallise in a purer form. C. Chemists recrystallise solids when they want to change small crystals into big crystals.
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