EBK ORGANIC CHEMISTRY-STUD.SOLNS.MAN+SG
EBK ORGANIC CHEMISTRY-STUD.SOLNS.MAN+SG
4th Edition
ISBN: 9781119659525
Author: Klein
Publisher: WILEY CONS
Question
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Chapter 26, Problem 49PP

(a)

Interpretation Introduction

Interpretation:

Isoprene units in the given set of compounds need to be circled.

Concept introduction:

Terpenes are naturally occurring compounds which share a common feature.  All terpenes are thought to be assembled from isoprene units having five carbon atoms.  So the structure of terpenes has the carbon atoms in multiples of five only.

EBK ORGANIC CHEMISTRY-STUD.SOLNS.MAN+SG, Chapter 26, Problem 49PP , additional homework tip  1

The isoprene units are identified by following few steps namely,

  • Identify the number of isoprene units
  • Look for methyl group
  • Trial and error to find isoprene unit

To identify: the isoprene units in bisabolene

(b)

Interpretation Introduction

Interpretation:

Isoprene units in the given set of compounds need to be circled.

Concept introduction:

Terpenes are naturally occurring compounds which share a common feature.  All terpenes are thought to be assembled from isoprene units having five carbon atoms.  So the structure of terpenes has the carbon atoms in multiples of five only.

EBK ORGANIC CHEMISTRY-STUD.SOLNS.MAN+SG, Chapter 26, Problem 49PP , additional homework tip  2

The isoprene units are identified by following few steps namely,

  • Identify the number of isoprene units
  • Look for methyl group
  • Trial and error to find isoprene unit

To identify: the isoprene units in flexibilene

(c)

Interpretation Introduction

Interpretation:

Isoprene units in the given set of compounds need to be circled.

Concept introduction:

Terpenes are naturally occurring compounds which share a common feature.  All terpenes are thought to be assembled from isoprene units having five carbon atoms.  So the structure of terpenes has the carbon atoms in multiples of five only.

EBK ORGANIC CHEMISTRY-STUD.SOLNS.MAN+SG, Chapter 26, Problem 49PP , additional homework tip  3

The isoprene units are identified by following few steps namely,

  • Identify the number of isoprene units
  • Look for methyl group
  • Trial and error to find isoprene unit

To identify: the isoprene units in humulene

(d)

Interpretation Introduction

Interpretation:

Isoprene units in the given set of compounds need to be circled.

Concept introduction:

Terpenes are naturally occurring compounds which share a common feature.  All terpenes are thought to be assembled from isoprene units having five carbon atoms.  So the structure of terpenes has the carbon atoms in multiples of five only.

EBK ORGANIC CHEMISTRY-STUD.SOLNS.MAN+SG, Chapter 26, Problem 49PP , additional homework tip  4

The isoprene units are identified by following few steps namely,

  • Identify the number of isoprene units
  • Look for methyl group
  • Trial and error to find isoprene unit

To identify: the isoprene units in vitamin A

(e)

Interpretation Introduction

Interpretation:

Isoprene units in the given set of compounds need to be circled.

Concept introduction:

Terpenes are naturally occurring compounds which share a common feature.  All terpenes are thought to be assembled from isoprene units having five carbon atoms.  So the structure of terpenes has the carbon atoms in multiples of five only.

EBK ORGANIC CHEMISTRY-STUD.SOLNS.MAN+SG, Chapter 26, Problem 49PP , additional homework tip  5

The isoprene units are identified by following few steps namely,

  • Identify the number of isoprene units
  • Look for methyl group
  • Trial and error to find isoprene unit

To identify: the isoprene units in geraniol

 (f)

Interpretation Introduction

Interpretation:

Isoprene units in the given set of compounds need to be circled.

Concept introduction:

Terpenes are naturally occurring compounds which share a common feature.  All terpenes are thought to be assembled from isoprene units having five carbon atoms.  So the structure of terpenes has the carbon atoms in multiples of five only.

EBK ORGANIC CHEMISTRY-STUD.SOLNS.MAN+SG, Chapter 26, Problem 49PP , additional homework tip  6

The isoprene units are identified by following few steps namely,

  • Identify the number of isoprene units
  • Look for methyl group
  • Trial and error to find isoprene unit

To identify: the isoprene units in sabinene

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On the next page is an LC separation of the parabens found in baby wash. Parabens are suspected in a link to breast cancer therefore an accurate way to quantitate them is desired. a. In the chromatogram, estimate k' for ethyl paraben. Clearly indicate what values you used for all the terms in your calculation. b. Is this a "good" value for a capacity factor? Explain. c. What is the resolution between n-Propyl paraben and n-Butyl paraben? Again, indicate clearly what values you used in your calculation. MAU | Methyl paraben 40 20 0 -2 Ethyl paraben n-Propyl paraben n-Butyl paraben App ID 22925 6 8 min
d. In Figure 4, each stationary phase shows some negative correlation between plate count and retention factor. In other words, as k' increases, N decreases. Explain this relationship between k' and N. Plate Count (N) 4000 3500 2500 2000 1500 1000 Figure 4. Column efficiency (N) vs retention factor (k') for 22 nonionizable solutes on FMS (red), PGC (black), and COZ (green). 3000 Eluent compositions (acetonitrile/water, A/W) were adjusted to obtain k' less than 15, which was achieved for most solutes as follows: FMS (30/70 A/W), PGC (60/40), COZ (80/20). Slightly different compositions were used for the most highly retained solutes. All columns were 50 mm × 4.6 mm id and packed with 5 um particles, except for COZ, which was packed with 3 um particles. All other chromatographic conditions were constant: column length 5 cm, column j.§. 4.6 mm, flow rate 2 mL/min, column temperature 40 °C, and injection volume 0.5 μL Log(k'x/K'ethylbenzene) FMS 1.5 1.0 0.5 0.0 ཐྭ ཋ ཤྩ བྷྲ ; 500 0 5 10…
f. Predict how the van Deemter curve in Figure 7 would change if the temperature were raised from 40 °C to 55 °C. Figure 7. van Desmter curves in reduced coordinates for four nitroalkane homologues (nitropropane, black; nitrobutane, red; nitropentane, blue; and nitrohexane, green) separated on the FMS phase. Chromatographic conditions: column dimensions 50 mm × 4.6 mm id, eluent 30/70 ACN/water, flow rates 0.2-5.0 mL/min, injection volume 0.5 and column temperature 40 °C. No corrections to the plate heights have been made to account for extracolumn dispersion. Reduced Plate Height (h) ° 20 40 60 Reduced Velocity (v) 8. (2) A water sample is analyzed for traces of benzene using headspace analysis. The sample and standard are spiked with a fixed amount of toluene as an internal standard. The following data are obtained: Ppb benzene Peak area benzene Peak area toluene 10.0 252 376 Sample 533 368 What is the concentration of benzene in the sample?
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