Principles of Instrumental Analysis
7th Edition
ISBN: 9781305577213
Author: Douglas A. Skoog, F. James Holler, Stanley R. Crouch
Publisher: Cengage Learning
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Chapter 25, Problem 25.14QAP
Interpretation Introduction
Interpretation:
The titration curve should be developed in spreadsheet format and the limiting current versus the volume of titrant should be plotted.
Concept introduction:
In Amperometric titrations, equivalence point is determined by measuring the
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Record the amounts measured and
calculate the percent yield for Part 2
in the table below.
Dicyclopentadiene
measured in volume
Cyclopentadiene
measured in grams
0
Measured
Calculated
Mol
Yield
Mass (g) or Volume (mL)
Mass (g) or Volume (ml)
0.6
2.955
Part 2 Measurements and Results
Record the amounts measured and calculate the percent yield for Part 2 in the table below.
0.588
0.0044
2.868
0.0434
N/A
Table view List view
Measured
Calculated
Mol
$ Yield
Melting Point (C)
Mass (g) or Volume (ml)
Mass (g) or Volume (ml.)
Cyclopentadiene
0.1
0.08
0.001189
measured in volume
Maleic Anhydride
0.196
N/A
cis-norbornene-5,6-endo-
dicarboxylic anhydride
0.041
0.0002467
N/A
N/A
N/A
0.002
N/A
N/A
128
Draw the condensed structural formula and line-angle formula for each:
2,3-dimethylheptane
3-bromo-2-pentanol
3-isopropyl-2-hexene
4-chlorobutanoic acid
Record the IUPAC names for each of the structures shown below.
a)
b)
c)
OH
d)
OH
e)
Chapter 25 Solutions
Principles of Instrumental Analysis
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