(a) Interpretation: From the given spectra, the structure of the molecule is to be determined and mechanism is to be drawn. Concept introduction: Various spectroscopies are the primary method for determining the structure of compounds. If the molecule is not too large or complex, the determination should be very accurate. These are simply done and rapid. For overlapping information, they can be combined. According to the structure of the molecule, the molecules absorb specific frequencies of light. The IR spectroscopy theory utilizes this concept. Mass spectroscopy (MS) measures the mass to charge the ratio of ions. In order to determine the structure of the molecule, Proton nuclear magnetic resonance (1H NMR) is used.

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Answer 1

Question

Chapter 21, Problem 21.96P

Interpretation Introduction

(a)

Interpretation:

From the given spectra, the structure of the molecule is to be determined and mechanism is to be drawn.

Concept introduction:

Various spectroscopies are the primary method for determining the structure of compounds. If the molecule is not too large or complex, the determination should be very accurate. These are simply done and rapid. For overlapping information, they can be combined. According to the structure of the molecule, the molecules absorb specific frequencies of light. The IR spectroscopy theory utilizes this concept. Mass spectroscopy (MS) measures the mass to charge the ratio of ions. In order to determine the structure of the molecule, Proton nuclear magnetic resonance (1H NMR) is used.

Interpretation Introduction

(b)

Interpretation:

From the given spectra, the structure of the molecule is to be determined and mechanism is to be drawn.

Concept introduction:

Various spectroscopies are the primary method for determining the structure of compounds. If the molecule is not too large or complex, the determination should be very accurate. These are simply done and rapid. For overlapping information, they can be combined. According to the structure of the molecule, the molecules absorb specific frequencies of light. The IR spectroscopy theory utilizes this concept. Mass spectroscopy (MS) measures the mass to charge the ratio of ions. In order to determine the structure of the molecule, Proton nuclear magnetic resonance (1H NMR) is used.

Interpretation Introduction

(c)

Interpretation:

From the given spectra, the structure of the molecule is to be determined and mechanism is to be drawn.

Concept introduction:

Various spectroscopies are the primary method for determining the structure of compounds. If the molecule is not too large or complex, the determination should be very accurate. These are simply done and rapid. For overlapping information, they can be combined. According to the structure of the molecule, the molecules absorb specific frequencies of light. The IR spectroscopy theory utilizes this concept. Mass spectroscopy (MS) measures the mass to charge the ratio of ions. In order to determine the structure of the molecule, Proton nuclear magnetic resonance (1H NMR) is used.

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Part VII. Below are the 'HNMR, 13 C-NMR, COSY 2D- NMR, and HSQC 2D-NMR (similar with HETCOR but axes are reversed) spectra of an organic compound with molecular formula C6H1003 - Assign chemical shift values to the H and c atoms of the compound. Find the structure. Show complete solutions. Predicted 1H NMR Spectrum 4.7 4.6 4.5 4.4 4.3 4.2 4.1 4.0 3.9 3.8 3.7 3.6 3.5 3.4 3.3 3.2 3.1 3.0 2.9 2.8 2.7 2.6 2.5 2.4 2.3 2.2 2.1 2.0 1.9 1.8 1.7 1.6 1.5 1.4 1.3 1.2 1.1 f1 (ppm) Predicted 13C NMR Spectrum 100 f1 (ppm) 30 220 210 200 190 180 170 160 150 140 130 120 110 90 80 70 -26 60 50 40 46 30 20 115 10 1.0 0.9 0.8 0 -10

Answer 2

Question

Chapter 21, Problem 21.96P

Interpretation Introduction

(a)

Interpretation:

From the given spectra, the structure of the molecule is to be determined and mechanism is to be drawn.

Concept introduction:

Various spectroscopies are the primary method for determining the structure of compounds. If the molecule is not too large or complex, the determination should be very accurate. These are simply done and rapid. For overlapping information, they can be combined. According to the structure of the molecule, the molecules absorb specific frequencies of light. The IR spectroscopy theory utilizes this concept. Mass spectroscopy (MS) measures the mass to charge the ratio of ions. In order to determine the structure of the molecule, Proton nuclear magnetic resonance (1H NMR) is used.

Interpretation Introduction

(b)

Interpretation:

From the given spectra, the structure of the molecule is to be determined and mechanism is to be drawn.

Concept introduction:

Various spectroscopies are the primary method for determining the structure of compounds. If the molecule is not too large or complex, the determination should be very accurate. These are simply done and rapid. For overlapping information, they can be combined. According to the structure of the molecule, the molecules absorb specific frequencies of light. The IR spectroscopy theory utilizes this concept. Mass spectroscopy (MS) measures the mass to charge the ratio of ions. In order to determine the structure of the molecule, Proton nuclear magnetic resonance (1H NMR) is used.

Interpretation Introduction

(c)

Interpretation:

From the given spectra, the structure of the molecule is to be determined and mechanism is to be drawn.

Concept introduction:

Various spectroscopies are the primary method for determining the structure of compounds. If the molecule is not too large or complex, the determination should be very accurate. These are simply done and rapid. For overlapping information, they can be combined. According to the structure of the molecule, the molecules absorb specific frequencies of light. The IR spectroscopy theory utilizes this concept. Mass spectroscopy (MS) measures the mass to charge the ratio of ions. In order to determine the structure of the molecule, Proton nuclear magnetic resonance (1H NMR) is used.

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Answer 3

Question

Chapter 21, Problem 21.96P

Interpretation Introduction

(a)

Interpretation:

From the given spectra, the structure of the molecule is to be determined and mechanism is to be drawn.

Concept introduction:

Various spectroscopies are the primary method for determining the structure of compounds. If the molecule is not too large or complex, the determination should be very accurate. These are simply done and rapid. For overlapping information, they can be combined. According to the structure of the molecule, the molecules absorb specific frequencies of light. The IR spectroscopy theory utilizes this concept. Mass spectroscopy (MS) measures the mass to charge the ratio of ions. In order to determine the structure of the molecule, Proton nuclear magnetic resonance (1H NMR) is used.

Interpretation Introduction

(b)

Interpretation:

From the given spectra, the structure of the molecule is to be determined and mechanism is to be drawn.

Concept introduction:

Various spectroscopies are the primary method for determining the structure of compounds. If the molecule is not too large or complex, the determination should be very accurate. These are simply done and rapid. For overlapping information, they can be combined. According to the structure of the molecule, the molecules absorb specific frequencies of light. The IR spectroscopy theory utilizes this concept. Mass spectroscopy (MS) measures the mass to charge the ratio of ions. In order to determine the structure of the molecule, Proton nuclear magnetic resonance (1H NMR) is used.

Interpretation Introduction

(c)

Interpretation:

From the given spectra, the structure of the molecule is to be determined and mechanism is to be drawn.

Concept introduction:

Various spectroscopies are the primary method for determining the structure of compounds. If the molecule is not too large or complex, the determination should be very accurate. These are simply done and rapid. For overlapping information, they can be combined. According to the structure of the molecule, the molecules absorb specific frequencies of light. The IR spectroscopy theory utilizes this concept. Mass spectroscopy (MS) measures the mass to charge the ratio of ions. In order to determine the structure of the molecule, Proton nuclear magnetic resonance (1H NMR) is used.

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Answer 4

Question

Chapter 21, Problem 21.96P

Interpretation Introduction

(a)

Interpretation:

From the given spectra, the structure of the molecule is to be determined and mechanism is to be drawn.

Concept introduction:

Various spectroscopies are the primary method for determining the structure of compounds. If the molecule is not too large or complex, the determination should be very accurate. These are simply done and rapid. For overlapping information, they can be combined. According to the structure of the molecule, the molecules absorb specific frequencies of light. The IR spectroscopy theory utilizes this concept. Mass spectroscopy (MS) measures the mass to charge the ratio of ions. In order to determine the structure of the molecule, Proton nuclear magnetic resonance (1H NMR) is used.

Interpretation Introduction

(b)

Interpretation:

From the given spectra, the structure of the molecule is to be determined and mechanism is to be drawn.

Concept introduction:

Various spectroscopies are the primary method for determining the structure of compounds. If the molecule is not too large or complex, the determination should be very accurate. These are simply done and rapid. For overlapping information, they can be combined. According to the structure of the molecule, the molecules absorb specific frequencies of light. The IR spectroscopy theory utilizes this concept. Mass spectroscopy (MS) measures the mass to charge the ratio of ions. In order to determine the structure of the molecule, Proton nuclear magnetic resonance (1H NMR) is used.

Interpretation Introduction

(c)

Interpretation:

From the given spectra, the structure of the molecule is to be determined and mechanism is to be drawn.

Concept introduction:

Various spectroscopies are the primary method for determining the structure of compounds. If the molecule is not too large or complex, the determination should be very accurate. These are simply done and rapid. For overlapping information, they can be combined. According to the structure of the molecule, the molecules absorb specific frequencies of light. The IR spectroscopy theory utilizes this concept. Mass spectroscopy (MS) measures the mass to charge the ratio of ions. In order to determine the structure of the molecule, Proton nuclear magnetic resonance (1H NMR) is used.

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Answer 5

Chapter 21, Problem 21.96P

Interpretation Introduction

(a)

Interpretation:

From the given spectra, the structure of the molecule is to be determined and mechanism is to be drawn.

Concept introduction:

Various spectroscopies are the primary method for determining the structure of compounds. If the molecule is not too large or complex, the determination should be very accurate. These are simply done and rapid. For overlapping information, they can be combined. According to the structure of the molecule, the molecules absorb specific frequencies of light. The IR spectroscopy theory utilizes this concept. Mass spectroscopy (MS) measures the mass to charge the ratio of ions. In order to determine the structure of the molecule, Proton nuclear magnetic resonance (1H NMR) is used.

Interpretation Introduction

(b)

Interpretation:

From the given spectra, the structure of the molecule is to be determined and mechanism is to be drawn.

Concept introduction:

Various spectroscopies are the primary method for determining the structure of compounds. If the molecule is not too large or complex, the determination should be very accurate. These are simply done and rapid. For overlapping information, they can be combined. According to the structure of the molecule, the molecules absorb specific frequencies of light. The IR spectroscopy theory utilizes this concept. Mass spectroscopy (MS) measures the mass to charge the ratio of ions. In order to determine the structure of the molecule, Proton nuclear magnetic resonance (1H NMR) is used.

Interpretation Introduction

(c)

Interpretation:

From the given spectra, the structure of the molecule is to be determined and mechanism is to be drawn.

Concept introduction:

Various spectroscopies are the primary method for determining the structure of compounds. If the molecule is not too large or complex, the determination should be very accurate. These are simply done and rapid. For overlapping information, they can be combined. According to the structure of the molecule, the molecules absorb specific frequencies of light. The IR spectroscopy theory utilizes this concept. Mass spectroscopy (MS) measures the mass to charge the ratio of ions. In order to determine the structure of the molecule, Proton nuclear magnetic resonance (1H NMR) is used.

Answer 6

Chapter 21, Problem 21.96P

Interpretation Introduction

(a)

Interpretation:

From the given spectra, the structure of the molecule is to be determined and mechanism is to be drawn.

Concept introduction:

Various spectroscopies are the primary method for determining the structure of compounds. If the molecule is not too large or complex, the determination should be very accurate. These are simply done and rapid. For overlapping information, they can be combined. According to the structure of the molecule, the molecules absorb specific frequencies of light. The IR spectroscopy theory utilizes this concept. Mass spectroscopy (MS) measures the mass to charge the ratio of ions. In order to determine the structure of the molecule, Proton nuclear magnetic resonance (1H NMR) is used.

Answer 7

Chapter 21, Problem 21.96P

Interpretation Introduction

(a)

Interpretation:

From the given spectra, the structure of the molecule is to be determined and mechanism is to be drawn.

Concept introduction:

Various spectroscopies are the primary method for determining the structure of compounds. If the molecule is not too large or complex, the determination should be very accurate. These are simply done and rapid. For overlapping information, they can be combined. According to the structure of the molecule, the molecules absorb specific frequencies of light. The IR spectroscopy theory utilizes this concept. Mass spectroscopy (MS) measures the mass to charge the ratio of ions. In order to determine the structure of the molecule, Proton nuclear magnetic resonance (1H NMR) is used.

Answer 8

Interpretation Introduction

(b)

Interpretation:

From the given spectra, the structure of the molecule is to be determined and mechanism is to be drawn.

Concept introduction:

Various spectroscopies are the primary method for determining the structure of compounds. If the molecule is not too large or complex, the determination should be very accurate. These are simply done and rapid. For overlapping information, they can be combined. According to the structure of the molecule, the molecules absorb specific frequencies of light. The IR spectroscopy theory utilizes this concept. Mass spectroscopy (MS) measures the mass to charge the ratio of ions. In order to determine the structure of the molecule, Proton nuclear magnetic resonance (1H NMR) is used.

Answer 9

Interpretation Introduction

(b)

Interpretation:

From the given spectra, the structure of the molecule is to be determined and mechanism is to be drawn.

Concept introduction:

Various spectroscopies are the primary method for determining the structure of compounds. If the molecule is not too large or complex, the determination should be very accurate. These are simply done and rapid. For overlapping information, they can be combined. According to the structure of the molecule, the molecules absorb specific frequencies of light. The IR spectroscopy theory utilizes this concept. Mass spectroscopy (MS) measures the mass to charge the ratio of ions. In order to determine the structure of the molecule, Proton nuclear magnetic resonance (1H NMR) is used.

Answer 10

Interpretation Introduction

(c)

Interpretation:

From the given spectra, the structure of the molecule is to be determined and mechanism is to be drawn.

Concept introduction:

Various spectroscopies are the primary method for determining the structure of compounds. If the molecule is not too large or complex, the determination should be very accurate. These are simply done and rapid. For overlapping information, they can be combined. According to the structure of the molecule, the molecules absorb specific frequencies of light. The IR spectroscopy theory utilizes this concept. Mass spectroscopy (MS) measures the mass to charge the ratio of ions. In order to determine the structure of the molecule, Proton nuclear magnetic resonance (1H NMR) is used.

Answer 11

Interpretation Introduction

(c)

Interpretation:

From the given spectra, the structure of the molecule is to be determined and mechanism is to be drawn.

Concept introduction:

Various spectroscopies are the primary method for determining the structure of compounds. If the molecule is not too large or complex, the determination should be very accurate. These are simply done and rapid. For overlapping information, they can be combined. According to the structure of the molecule, the molecules absorb specific frequencies of light. The IR spectroscopy theory utilizes this concept. Mass spectroscopy (MS) measures the mass to charge the ratio of ions. In order to determine the structure of the molecule, Proton nuclear magnetic resonance (1H NMR) is used.

Answer 12

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Answer 14

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Answer 15

Ch. 21 - Prob. 21.1P Ch. 21 - Prob. 21.2P Ch. 21 - Prob. 21.3P Ch. 21 - Prob. 21.4P Ch. 21 - Prob. 21.5P Ch. 21 - Prob. 21.6P Ch. 21 - Prob. 21.7P Ch. 21 - Prob. 21.8P Ch. 21 - Prob. 21.9P Ch. 21 - Prob. 21.10P

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Chapter 21 Solutions