a) Interpretation: The molecular formula and the structure of an unknown compound to be predicted using spectrum details. Concept introduction: Molecular formula: It represents the types of atoms with their total number present in a given molecule. Mass spectroscopy: It is a form of spectroscopic technique which is used for the elucidation of the molecular formula and molecular weight of the compound, depending upon the mass of the molecule. Molecular ion peak (M) +. : It is defined as the heaviest peak in the IR spectrum of the molecule which represents the largest molecular ion in the given molecule with greater m/z value. The (M+1) +. peak: It denotes the peak that arises next to molecular ion peak in the mass spectrum. The peak arises due to the presence of the isotope of carbon ( 13 C). (M+1) +. peak in mass spectroscopy is used to explain the number of carbon atoms present in a molecule depending on the abundance of (M+1) +. peak. 1 HNMR: The 1 HNMR spectrum gives information on the different electronic environment of protons. The number of signal (proton types) generated in 1 HNMR are predicted by performing symmetry operations (rotation or reflection symmetry). The 13 CNMR spectrum gives information on the different electronic environments of carbon. As like 1 HNMR, the number of signals generated in 13 CNMR are predicted by performing symmetry operations (rotation or reflection symmetry). Only chemical shift values are reported in the spectrum but not the multiplicity and integration values because the coupling between two neighboring 13 C- 13 C nuclei are weakly involved due to the low abundance of 13 C isotopes of carbon atom. To Identify: The molecular formula to be identified.

Question

1 N2H4 (l) + 3 O2(g) > 2 NO2 (g) + 2 H2O (g) If 75.0 kg of hydrazine are reacted with 75.0 kg of oxygen, which is the limiting reactant?

Answer 1

Question

Chapter 13.SE, Problem 68GP

Interpretation Introduction

a)

Interpretation:

The molecular formula and the structure of an unknown compound to be predicted using spectrum details.

Concept introduction:

Molecular formula:

It represents the types of atoms with their total number present in a given molecule.

Mass spectroscopy:

It is a form of spectroscopic technique which is used for the elucidation of the molecular formula and molecular weight of the compound, depending upon the mass of the molecule.

Molecular ion peak (M)^+.:

It is defined as the heaviest peak in the IR spectrum of the molecule which represents the largest molecular ion in the given molecule with greater m/z value.

The (M+1)^+. peak:

It denotes the peak that arises next to molecular ion peak in the mass spectrum. The peak arises due to the presence of the isotope of carbon (¹³C).

(M+1)^+. peak in mass spectroscopy is used to explain the number of carbon atoms present in a molecule depending on the abundance of (M+1)^+. peak.

¹HNMR: The ¹HNMR spectrum gives information on the different electronic environment of protons. The number of signal (proton types) generated in ¹HNMR are predicted by performing symmetry operations (rotation or reflection symmetry).

The ¹³CNMR spectrum gives information on the different electronic environments of carbon. As like ¹HNMR, the number of signals generated in ¹³CNMR are predicted by performing symmetry operations (rotation or reflection symmetry). Only chemical shift values are reported in the spectrum but not the multiplicity and integration values because the coupling between two neighboring ¹³C-¹³ C nuclei are weakly involved due to the low abundance of ¹³C isotopes of carbon atom.

To Identify:

The molecular formula to be identified.

Interpretation Introduction

b)

Interpretation:

The molecular formula and the structure of an unknown compound to be predicted using spectrum details.

Concept introduction:

Molecular formula:

It represents the types of atoms with their total number present in a given molecule.

Mass spectroscopy:

It is a form of spectroscopic technique which is used for the elucidation of the molecular formula and molecular weight of the compound, depending upon the mass of the molecule.

Molecular ion peak (M)^+.:

It is defined as the heaviest peak in the IR spectrum of the molecule which represents the largest molecular ion in the given molecule with greater m/z value.

The (M+1)^+. peak:

It denotes the peak that arises next to molecular ion peak in the mass spectrum. The peak arises due to the presence of the isotope of carbon (¹³C).

(M+1)^+. peak in mass spectroscopy is used to explain the number of carbon atoms present in a molecule depending on the abundance of (M+1)^+. peak.

¹HNMR: The ¹HNMR spectrum gives information on the different electronic environment of protons. The number of signal (proton types) generated in ¹HNMR are predicted by performing symmetry operations (rotation or reflection symmetry).

The ¹³CNMR spectrum gives information on the different electronic environments of carbon. As like ¹HNMR, the number of signals generated in ¹³CNMR are predicted by performing symmetry operations (rotation or reflection symmetry). Only chemical shift values are reported in the spectrum but not the multiplicity and integration values because the coupling between two neighboring ¹³C-¹³ C nuclei are weakly involved due to the low abundance of ¹³C isotopes of carbon atom.

To Identify:

The structure to be predicted for C₅H₁₀O.

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1 N2H4 (l) + 3 O2(g) > 2 NO2 (g) + 2 H2O (g) If 75.0 kg of hydrazine are reacted with 75.0 kg of oxygen, which is the limiting reactant?

PQ-10. What is the major product of this reaction? (A) (C) 930 Me HO O=S=O O-8-CF, C 어 Me H+ OH 270 O 0-5-0 O=S=O O-S-CF CF3 2

Predict the major organic product(s) of the following reactions. Include stereochemistry when necessary. Write NR if no reaction, try to explain.

Answer 2

Question

Chapter 13.SE, Problem 68GP

Interpretation Introduction

a)

Interpretation:

The molecular formula and the structure of an unknown compound to be predicted using spectrum details.

Concept introduction:

Molecular formula:

It represents the types of atoms with their total number present in a given molecule.

Mass spectroscopy:

It is a form of spectroscopic technique which is used for the elucidation of the molecular formula and molecular weight of the compound, depending upon the mass of the molecule.

Molecular ion peak (M)^+.:

It is defined as the heaviest peak in the IR spectrum of the molecule which represents the largest molecular ion in the given molecule with greater m/z value.

The (M+1)^+. peak:

It denotes the peak that arises next to molecular ion peak in the mass spectrum. The peak arises due to the presence of the isotope of carbon (¹³C).

(M+1)^+. peak in mass spectroscopy is used to explain the number of carbon atoms present in a molecule depending on the abundance of (M+1)^+. peak.

¹HNMR: The ¹HNMR spectrum gives information on the different electronic environment of protons. The number of signal (proton types) generated in ¹HNMR are predicted by performing symmetry operations (rotation or reflection symmetry).

The ¹³CNMR spectrum gives information on the different electronic environments of carbon. As like ¹HNMR, the number of signals generated in ¹³CNMR are predicted by performing symmetry operations (rotation or reflection symmetry). Only chemical shift values are reported in the spectrum but not the multiplicity and integration values because the coupling between two neighboring ¹³C-¹³ C nuclei are weakly involved due to the low abundance of ¹³C isotopes of carbon atom.

To Identify:

The molecular formula to be identified.

Interpretation Introduction

b)

Interpretation:

The molecular formula and the structure of an unknown compound to be predicted using spectrum details.

Concept introduction:

Molecular formula:

It represents the types of atoms with their total number present in a given molecule.

Mass spectroscopy:

It is a form of spectroscopic technique which is used for the elucidation of the molecular formula and molecular weight of the compound, depending upon the mass of the molecule.

Molecular ion peak (M)^+.:

It is defined as the heaviest peak in the IR spectrum of the molecule which represents the largest molecular ion in the given molecule with greater m/z value.

The (M+1)^+. peak:

It denotes the peak that arises next to molecular ion peak in the mass spectrum. The peak arises due to the presence of the isotope of carbon (¹³C).

(M+1)^+. peak in mass spectroscopy is used to explain the number of carbon atoms present in a molecule depending on the abundance of (M+1)^+. peak.

¹HNMR: The ¹HNMR spectrum gives information on the different electronic environment of protons. The number of signal (proton types) generated in ¹HNMR are predicted by performing symmetry operations (rotation or reflection symmetry).

The ¹³CNMR spectrum gives information on the different electronic environments of carbon. As like ¹HNMR, the number of signals generated in ¹³CNMR are predicted by performing symmetry operations (rotation or reflection symmetry). Only chemical shift values are reported in the spectrum but not the multiplicity and integration values because the coupling between two neighboring ¹³C-¹³ C nuclei are weakly involved due to the low abundance of ¹³C isotopes of carbon atom.

To Identify:

The structure to be predicted for C₅H₁₀O.

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Answer 3

Question

Chapter 13.SE, Problem 68GP

Interpretation Introduction

a)

Interpretation:

The molecular formula and the structure of an unknown compound to be predicted using spectrum details.

Concept introduction:

Molecular formula:

It represents the types of atoms with their total number present in a given molecule.

Mass spectroscopy:

It is a form of spectroscopic technique which is used for the elucidation of the molecular formula and molecular weight of the compound, depending upon the mass of the molecule.

Molecular ion peak (M)^+.:

It is defined as the heaviest peak in the IR spectrum of the molecule which represents the largest molecular ion in the given molecule with greater m/z value.

The (M+1)^+. peak:

It denotes the peak that arises next to molecular ion peak in the mass spectrum. The peak arises due to the presence of the isotope of carbon (¹³C).

(M+1)^+. peak in mass spectroscopy is used to explain the number of carbon atoms present in a molecule depending on the abundance of (M+1)^+. peak.

¹HNMR: The ¹HNMR spectrum gives information on the different electronic environment of protons. The number of signal (proton types) generated in ¹HNMR are predicted by performing symmetry operations (rotation or reflection symmetry).

The ¹³CNMR spectrum gives information on the different electronic environments of carbon. As like ¹HNMR, the number of signals generated in ¹³CNMR are predicted by performing symmetry operations (rotation or reflection symmetry). Only chemical shift values are reported in the spectrum but not the multiplicity and integration values because the coupling between two neighboring ¹³C-¹³ C nuclei are weakly involved due to the low abundance of ¹³C isotopes of carbon atom.

To Identify:

The molecular formula to be identified.

Interpretation Introduction

b)

Interpretation:

The molecular formula and the structure of an unknown compound to be predicted using spectrum details.

Concept introduction:

Molecular formula:

It represents the types of atoms with their total number present in a given molecule.

Mass spectroscopy:

It is a form of spectroscopic technique which is used for the elucidation of the molecular formula and molecular weight of the compound, depending upon the mass of the molecule.

Molecular ion peak (M)^+.:

It is defined as the heaviest peak in the IR spectrum of the molecule which represents the largest molecular ion in the given molecule with greater m/z value.

The (M+1)^+. peak:

It denotes the peak that arises next to molecular ion peak in the mass spectrum. The peak arises due to the presence of the isotope of carbon (¹³C).

(M+1)^+. peak in mass spectroscopy is used to explain the number of carbon atoms present in a molecule depending on the abundance of (M+1)^+. peak.

¹HNMR: The ¹HNMR spectrum gives information on the different electronic environment of protons. The number of signal (proton types) generated in ¹HNMR are predicted by performing symmetry operations (rotation or reflection symmetry).

The ¹³CNMR spectrum gives information on the different electronic environments of carbon. As like ¹HNMR, the number of signals generated in ¹³CNMR are predicted by performing symmetry operations (rotation or reflection symmetry). Only chemical shift values are reported in the spectrum but not the multiplicity and integration values because the coupling between two neighboring ¹³C-¹³ C nuclei are weakly involved due to the low abundance of ¹³C isotopes of carbon atom.

To Identify:

The structure to be predicted for C₅H₁₀O.

Expert Solution & Answer

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Answer 4

Question

Chapter 13.SE, Problem 68GP

Interpretation Introduction

a)

Interpretation:

The molecular formula and the structure of an unknown compound to be predicted using spectrum details.

Concept introduction:

Molecular formula:

It represents the types of atoms with their total number present in a given molecule.

Mass spectroscopy:

It is a form of spectroscopic technique which is used for the elucidation of the molecular formula and molecular weight of the compound, depending upon the mass of the molecule.

Molecular ion peak (M)^+.:

It is defined as the heaviest peak in the IR spectrum of the molecule which represents the largest molecular ion in the given molecule with greater m/z value.

The (M+1)^+. peak:

It denotes the peak that arises next to molecular ion peak in the mass spectrum. The peak arises due to the presence of the isotope of carbon (¹³C).

(M+1)^+. peak in mass spectroscopy is used to explain the number of carbon atoms present in a molecule depending on the abundance of (M+1)^+. peak.

¹HNMR: The ¹HNMR spectrum gives information on the different electronic environment of protons. The number of signal (proton types) generated in ¹HNMR are predicted by performing symmetry operations (rotation or reflection symmetry).

The ¹³CNMR spectrum gives information on the different electronic environments of carbon. As like ¹HNMR, the number of signals generated in ¹³CNMR are predicted by performing symmetry operations (rotation or reflection symmetry). Only chemical shift values are reported in the spectrum but not the multiplicity and integration values because the coupling between two neighboring ¹³C-¹³ C nuclei are weakly involved due to the low abundance of ¹³C isotopes of carbon atom.

To Identify:

The molecular formula to be identified.

Interpretation Introduction

b)

Interpretation:

The molecular formula and the structure of an unknown compound to be predicted using spectrum details.

Concept introduction:

Molecular formula:

It represents the types of atoms with their total number present in a given molecule.

Mass spectroscopy:

It is a form of spectroscopic technique which is used for the elucidation of the molecular formula and molecular weight of the compound, depending upon the mass of the molecule.

Molecular ion peak (M)^+.:

It is defined as the heaviest peak in the IR spectrum of the molecule which represents the largest molecular ion in the given molecule with greater m/z value.

The (M+1)^+. peak:

It denotes the peak that arises next to molecular ion peak in the mass spectrum. The peak arises due to the presence of the isotope of carbon (¹³C).

(M+1)^+. peak in mass spectroscopy is used to explain the number of carbon atoms present in a molecule depending on the abundance of (M+1)^+. peak.

¹HNMR: The ¹HNMR spectrum gives information on the different electronic environment of protons. The number of signal (proton types) generated in ¹HNMR are predicted by performing symmetry operations (rotation or reflection symmetry).

The ¹³CNMR spectrum gives information on the different electronic environments of carbon. As like ¹HNMR, the number of signals generated in ¹³CNMR are predicted by performing symmetry operations (rotation or reflection symmetry). Only chemical shift values are reported in the spectrum but not the multiplicity and integration values because the coupling between two neighboring ¹³C-¹³ C nuclei are weakly involved due to the low abundance of ¹³C isotopes of carbon atom.

To Identify:

The structure to be predicted for C₅H₁₀O.

Expert Solution & Answer

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Answer 5

Chapter 13.SE, Problem 68GP

Interpretation Introduction

a)

Interpretation:

The molecular formula and the structure of an unknown compound to be predicted using spectrum details.

Concept introduction:

Molecular formula:

It represents the types of atoms with their total number present in a given molecule.

Mass spectroscopy:

It is a form of spectroscopic technique which is used for the elucidation of the molecular formula and molecular weight of the compound, depending upon the mass of the molecule.

Molecular ion peak (M)^+.:

It is defined as the heaviest peak in the IR spectrum of the molecule which represents the largest molecular ion in the given molecule with greater m/z value.

The (M+1)^+. peak:

It denotes the peak that arises next to molecular ion peak in the mass spectrum. The peak arises due to the presence of the isotope of carbon (¹³C).

(M+1)^+. peak in mass spectroscopy is used to explain the number of carbon atoms present in a molecule depending on the abundance of (M+1)^+. peak.

¹HNMR: The ¹HNMR spectrum gives information on the different electronic environment of protons. The number of signal (proton types) generated in ¹HNMR are predicted by performing symmetry operations (rotation or reflection symmetry).

The ¹³CNMR spectrum gives information on the different electronic environments of carbon. As like ¹HNMR, the number of signals generated in ¹³CNMR are predicted by performing symmetry operations (rotation or reflection symmetry). Only chemical shift values are reported in the spectrum but not the multiplicity and integration values because the coupling between two neighboring ¹³C-¹³ C nuclei are weakly involved due to the low abundance of ¹³C isotopes of carbon atom.

To Identify:

The molecular formula to be identified.

Interpretation Introduction

b)

Interpretation:

The molecular formula and the structure of an unknown compound to be predicted using spectrum details.

Concept introduction:

Molecular formula:

It represents the types of atoms with their total number present in a given molecule.

Mass spectroscopy:

It is a form of spectroscopic technique which is used for the elucidation of the molecular formula and molecular weight of the compound, depending upon the mass of the molecule.

Molecular ion peak (M)^+.:

It is defined as the heaviest peak in the IR spectrum of the molecule which represents the largest molecular ion in the given molecule with greater m/z value.

The (M+1)^+. peak:

It denotes the peak that arises next to molecular ion peak in the mass spectrum. The peak arises due to the presence of the isotope of carbon (¹³C).

(M+1)^+. peak in mass spectroscopy is used to explain the number of carbon atoms present in a molecule depending on the abundance of (M+1)^+. peak.

¹HNMR: The ¹HNMR spectrum gives information on the different electronic environment of protons. The number of signal (proton types) generated in ¹HNMR are predicted by performing symmetry operations (rotation or reflection symmetry).

The ¹³CNMR spectrum gives information on the different electronic environments of carbon. As like ¹HNMR, the number of signals generated in ¹³CNMR are predicted by performing symmetry operations (rotation or reflection symmetry). Only chemical shift values are reported in the spectrum but not the multiplicity and integration values because the coupling between two neighboring ¹³C-¹³ C nuclei are weakly involved due to the low abundance of ¹³C isotopes of carbon atom.

To Identify:

The structure to be predicted for C₅H₁₀O.

Answer 6

Chapter 13.SE, Problem 68GP

Interpretation Introduction

a)

Interpretation:

The molecular formula and the structure of an unknown compound to be predicted using spectrum details.

Concept introduction:

Molecular formula:

It represents the types of atoms with their total number present in a given molecule.

Mass spectroscopy:

It is a form of spectroscopic technique which is used for the elucidation of the molecular formula and molecular weight of the compound, depending upon the mass of the molecule.

Molecular ion peak (M)^+.:

It is defined as the heaviest peak in the IR spectrum of the molecule which represents the largest molecular ion in the given molecule with greater m/z value.

The (M+1)^+. peak:

It denotes the peak that arises next to molecular ion peak in the mass spectrum. The peak arises due to the presence of the isotope of carbon (¹³C).

(M+1)^+. peak in mass spectroscopy is used to explain the number of carbon atoms present in a molecule depending on the abundance of (M+1)^+. peak.

¹HNMR: The ¹HNMR spectrum gives information on the different electronic environment of protons. The number of signal (proton types) generated in ¹HNMR are predicted by performing symmetry operations (rotation or reflection symmetry).

The ¹³CNMR spectrum gives information on the different electronic environments of carbon. As like ¹HNMR, the number of signals generated in ¹³CNMR are predicted by performing symmetry operations (rotation or reflection symmetry). Only chemical shift values are reported in the spectrum but not the multiplicity and integration values because the coupling between two neighboring ¹³C-¹³ C nuclei are weakly involved due to the low abundance of ¹³C isotopes of carbon atom.

To Identify:

The molecular formula to be identified.

Answer 7

Chapter 13.SE, Problem 68GP

Interpretation Introduction

a)

Interpretation:

The molecular formula and the structure of an unknown compound to be predicted using spectrum details.

Concept introduction:

Molecular formula:

It represents the types of atoms with their total number present in a given molecule.

Mass spectroscopy:

It is a form of spectroscopic technique which is used for the elucidation of the molecular formula and molecular weight of the compound, depending upon the mass of the molecule.

Molecular ion peak (M)^+.:

It is defined as the heaviest peak in the IR spectrum of the molecule which represents the largest molecular ion in the given molecule with greater m/z value.

The (M+1)^+. peak:

It denotes the peak that arises next to molecular ion peak in the mass spectrum. The peak arises due to the presence of the isotope of carbon (¹³C).

(M+1)^+. peak in mass spectroscopy is used to explain the number of carbon atoms present in a molecule depending on the abundance of (M+1)^+. peak.

¹HNMR: The ¹HNMR spectrum gives information on the different electronic environment of protons. The number of signal (proton types) generated in ¹HNMR are predicted by performing symmetry operations (rotation or reflection symmetry).

The ¹³CNMR spectrum gives information on the different electronic environments of carbon. As like ¹HNMR, the number of signals generated in ¹³CNMR are predicted by performing symmetry operations (rotation or reflection symmetry). Only chemical shift values are reported in the spectrum but not the multiplicity and integration values because the coupling between two neighboring ¹³C-¹³ C nuclei are weakly involved due to the low abundance of ¹³C isotopes of carbon atom.

To Identify:

The molecular formula to be identified.

Answer 8

Interpretation Introduction

b)

Interpretation:

The molecular formula and the structure of an unknown compound to be predicted using spectrum details.

Concept introduction:

Molecular formula:

It represents the types of atoms with their total number present in a given molecule.

Mass spectroscopy:

It is a form of spectroscopic technique which is used for the elucidation of the molecular formula and molecular weight of the compound, depending upon the mass of the molecule.

Molecular ion peak (M)^+.:

It is defined as the heaviest peak in the IR spectrum of the molecule which represents the largest molecular ion in the given molecule with greater m/z value.

The (M+1)^+. peak:

It denotes the peak that arises next to molecular ion peak in the mass spectrum. The peak arises due to the presence of the isotope of carbon (¹³C).

(M+1)^+. peak in mass spectroscopy is used to explain the number of carbon atoms present in a molecule depending on the abundance of (M+1)^+. peak.

¹HNMR: The ¹HNMR spectrum gives information on the different electronic environment of protons. The number of signal (proton types) generated in ¹HNMR are predicted by performing symmetry operations (rotation or reflection symmetry).

The ¹³CNMR spectrum gives information on the different electronic environments of carbon. As like ¹HNMR, the number of signals generated in ¹³CNMR are predicted by performing symmetry operations (rotation or reflection symmetry). Only chemical shift values are reported in the spectrum but not the multiplicity and integration values because the coupling between two neighboring ¹³C-¹³ C nuclei are weakly involved due to the low abundance of ¹³C isotopes of carbon atom.

To Identify:

The structure to be predicted for C₅H₁₀O.

Answer 9

Interpretation Introduction

b)

Interpretation:

The molecular formula and the structure of an unknown compound to be predicted using spectrum details.

Concept introduction:

Molecular formula:

It represents the types of atoms with their total number present in a given molecule.

Mass spectroscopy:

It is a form of spectroscopic technique which is used for the elucidation of the molecular formula and molecular weight of the compound, depending upon the mass of the molecule.

Molecular ion peak (M)^+.:

It is defined as the heaviest peak in the IR spectrum of the molecule which represents the largest molecular ion in the given molecule with greater m/z value.

The (M+1)^+. peak:

It denotes the peak that arises next to molecular ion peak in the mass spectrum. The peak arises due to the presence of the isotope of carbon (¹³C).

(M+1)^+. peak in mass spectroscopy is used to explain the number of carbon atoms present in a molecule depending on the abundance of (M+1)^+. peak.

¹HNMR: The ¹HNMR spectrum gives information on the different electronic environment of protons. The number of signal (proton types) generated in ¹HNMR are predicted by performing symmetry operations (rotation or reflection symmetry).

The ¹³CNMR spectrum gives information on the different electronic environments of carbon. As like ¹HNMR, the number of signals generated in ¹³CNMR are predicted by performing symmetry operations (rotation or reflection symmetry). Only chemical shift values are reported in the spectrum but not the multiplicity and integration values because the coupling between two neighboring ¹³C-¹³ C nuclei are weakly involved due to the low abundance of ¹³C isotopes of carbon atom.

To Identify:

The structure to be predicted for C₅H₁₀O.

Answer 10

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Answer 21

Ch. 13.1 - Prob. 1P Ch. 13.1 - Prob. 2P Ch. 13.2 - Prob. 3P Ch. 13.3 - The following 1H NMR peaks were recorded on a...Ch. 13.3 - When the 1Î— NMR spectrum of acetone, CH3COCH3, is...Ch. 13.4 - Each of the following compounds has a single 1H...Ch. 13.4 - Identify the different types of protons in the...Ch. 13.5 - How many peaks would you expect in the 1H NMR...Ch. 13.6 - Predict the splitting patterns you would expect...Ch. 13.6 - Draw structures for compounds that meet the...

Solution Summary: The author explains the molecular formula and the structure of an unknown compound to be predicted using spectrum details.

Chapter 13 Solutions