EBK CHEMISTRY: THE MOLECULAR NATURE OF
7th Edition
ISBN: 9781119513216
Author: HYSLOP
Publisher: JOHN WILEY+SONS INC.
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Textbook Question
Chapter 0, Problem 8RQ
Some large biological molecules rely on molecular shape for their function. Can you describe one of these?
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You have now performed a liquid-liquid extraction protocol in Experiment 4. In doing so, you
manipulated and exploited the acid-base chemistry of one or more of the compounds in your
mixture to facilitate their separation into different phases. The key to understanding how liquid-
liquid extractions work is by knowing which layer a compound is in, and in what protonation state.
The following liquid-liquid extraction is different from the one you performed in Experiment
4, but it uses the same type of logic. Your task is to show how to separate apart Compound
A and Compound B.
. Complete the following flowchart of a liquid-liquid extraction. Handwritten work is
encouraged.
•
Draw by hand (neatly) only the appropriate organic compound(s) in the boxes.
.
Specify the reagent(s)/chemicals (name is fine) and concentration as required in Boxes 4
and 5.
•
Box 7a requires the solvent (name is fine).
•
Box 7b requires one inorganic compound.
• You can neatly complete this assignment by hand and…
b) Elucidate compound D w) mt at 170 nd shows c-1 stretch at 550cm;'
The compound has the ff electronic transitions: 0%o* and no a*
1H NMR Spectrum
(CDCl3, 400 MHz)
3.5
3.0
2.5
2.0
1.5
1.0
0.5 ppm
13C{H} NMR Spectrum
(CDCl3, 100 MHz)
Solvent
80
70
60
50
40
30
20
10
0 ppm
ppm
¹H-13C me-HSQC Spectrum
ppm
(CDCl3, 400 MHz)
5
¹H-¹H COSY Spectrum
(CDCl3, 400 MHz)
0.5
10
3.5
3.0
2.5
2.0
1.5 1.0
10
15
20
20
25
30
30
-35
-1.0
1.5
-2.0
-2.5
3.0
-3.5
0.5
ppm
3.5
3.0
2.5
2.0
1.5
1.0
0.5
ppm
Show work with explanation. don't give Ai generated solution
Chapter 0 Solutions
EBK CHEMISTRY: THE MOLECULAR NATURE OF
Ch. 0 - Practice Exercise 0.1
Using the chapter titles...Ch. 0 - Prob. 2PECh. 0 - Prob. 3PECh. 0 - Prob. 4PECh. 0 - Prob. 5PECh. 0 - Prob. 6PECh. 0 - Prob. 7PECh. 0 - Prob. 8PECh. 0 - Prob. 9PECh. 0 - Practice Exercise 0.10 Aluminum atoms have a mass...
Ch. 0 - Practice Exercise 0.11 How much heavier is the...Ch. 0 - Practice Exercise 0.12 The definition of the size...Ch. 0 - Practice Exercise 0.13 Naturally occurring boron...Ch. 0 - Practice Exercise 0.14
Neon, the gas used in neon...Ch. 0 - Prob. 1RQCh. 0 - 0.2 Knowing what we know today, which of the...Ch. 0 - 0.3 In what ways does the atomic theory affect the...Ch. 0 - Shake a few crystals of salt into your hand and...Ch. 0 - Are there any examples of crystals in nature that...Ch. 0 - 0.6 Heat is one form of energy. If a reaction...Ch. 0 - Can you think of a chemical reaction that starts...Ch. 0 - 0.8 Some large biological molecules rely on...Ch. 0 - 0.9 What elements were formed (a) during the first...Ch. 0 - Prob. 10RQCh. 0 - 0.11 What is the predominant element in the solar...Ch. 0 - Prob. 12RQCh. 0 - What physical factors caused elements and minerals...Ch. 0 - Is this separation still occurring on the earth?Ch. 0 - 0.15 What measuring devices did early chemists...Ch. 0 - 0.16 In your own words, describe how Daltons...Ch. 0 - Which of the laws of chemical combination is used...Ch. 0 - Prob. 18RQCh. 0 - Where in an atom is nearly all of its mass...Ch. 0 - What is a nucleon? Which ones have we studied?Ch. 0 - 0.21 How was the charge-to-mass ratio of the...Ch. 0 - 0.22 How did Robert Millikan determine the charge...Ch. 0 - How was the proton discovered?Ch. 0 - What experiment did Rutherford carry out to...Ch. 0 - Why dont we count the electrons when determining...Ch. 0 - Define the terms atomic number and mass number....Ch. 0 - Prob. 27RQCh. 0 - Write the symbols of the isotopes that contain the...Ch. 0 - What is wrong with the following statement? The...Ch. 0 - 0.30 The atomic number of silver, Ag, is 47 and it...Ch. 0 - A certain element X forms a compound with oxygen...Ch. 0 - Nitrogen reacts with a metal to form a compound in...Ch. 0 - Give the numbers of neutrons, protons, and...Ch. 0 - 0.34 Give the numbers of electrons, protons, and...Ch. 0 - Iodine-131 is used to treat overactive thyroids;...Ch. 0 - Prob. 36RQCh. 0 - 0.37 One chemical substance in natural gas is a...Ch. 0 - 0.38 Carbon tetrachloride contains one carbon and...Ch. 0 - If an atom of carbon-12 had been assigned a...Ch. 0 - 0.40 One atom of has a mass that is 9.0754 times...Ch. 0 - Naturally occurring copper is composed of 69.17%...Ch. 0 - Naturally occurring magnesium (one of the elements...Ch. 0 - N2O is often called nitrous oxide or laughing gas,...Ch. 0 - An element has 24 protons in its nucleus. (a)...Ch. 0 - Iron is composed of four isotopes with the...Ch. 0 - 0.46 What color are the protons, neutrons, and...Ch. 0 - 0.47 Immediately after the big bang, helium and...Ch. 0 - Prob. 48RQCh. 0 - Scientists often validate measurements, such as...Ch. 0 - Sir James Chadwick, discovered the neutron. The...
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- Redraw the flowchartarrow_forwardredraw the flowchart with boxes and molecules written in themarrow_forwardPart I. a) Elucidate the structure of compound A using the following information. • mass spectrum: m+ = 102, m/2=57 312=29 • IR spectrum: 1002.5 % TRANSMITTANCE Ngg 50 40 30 20 90 80 70 60 MICRONS 5 8 9 10 12 13 14 15 16 19 1740 cm M 10 0 4000 3600 3200 2800 2400 2000 1800 1600 13 • CNMR 'H -NMR Peak 8 ppm (H) Integration multiplicity a 1.5 (3H) triplet b 1.3 1.5 (3H) triplet C 2.3 1 (2H) quartet d 4.1 1 (2H) quartet & ppm (c) 10 15 28 60 177 (C=0) b) Elucidate the structure of compound B using the following information 13C/DEPT NMR 150.9 MHz IIL 1400 WAVENUMBERS (CM-1) DEPT-90 DEPT-135 85 80 75 70 65 60 55 50 45 40 35 30 25 20 ppm 1200 1000 800 600 400arrow_forward
- • Part II. a) Elucidate The structure of compound c w/ molecular formula C10 11202 and the following data below: • IR spectra % TRANSMITTANCE 1002.5 90 80 70 60 50 40 30 20 10 0 4000 3600 3200 2800 2400 2000 1800 1600 • Information from 'HAMR MICRONS 8 9 10 11 14 15 16 19 25 1400 WAVENUMBERS (CM-1) 1200 1000 800 600 400 peak 8 ppm Integration multiplicity a 2.1 1.5 (3H) Singlet b 3.6 1 (2H) singlet с 3.8 1.5 (3H) Singlet d 6.8 1(2H) doublet 7.1 1(2H) doublet Information from 13C-nmR Normal carbon 29ppm Dept 135 Dept -90 + NO peak NO peak 50 ppm 55 ppm + NO peak 114 ppm t 126 ppm No peak NO peak 130 ppm t + 159 ppm No peak NO peak 207 ppm по реак NO peakarrow_forwardCould you redraw these and also explain how to solve them for me pleasarrow_forwardNonearrow_forward
- Draw the curved-arrow mechanism with the drawings of the molecules, not just abbreviations. -NO₂ Sn, HCl (aq) E D H (CH3CO)₂O -NH2 CH3arrow_forwardWhat is/are the product(s) of the following reaction? Select all that apply. * HI A B C OD OH A B OH D Carrow_forwardIn the image, the light blue sphere represents a mole of hydrogen atoms, the purple or teal spheres represent a mole of a conjugate base. A light blue sphere by itself is H+. Assuming there is 2.00 L of solution, answer the following: The Ka of the left & right solution is? The pH of the left & right solution is? The acid on the left & right is what kind of acid?arrow_forward
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